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1992-0818_TRULIS, THOMAS / JASMINE_Agreement MEMORANDUM TO: Memo to File FROM: Dawn M. Schanderl, Deputy City Clerk DATE: August 18, 1992 SUBJECT: Soils Reports - Solag Property Douglas Dumhart, Management Assistant 1, gave our office the one and only copy of the soils report for the Solag Disposal Maintance Yard. DO NOT CHECK OUT. If someone would like a copy we will send out to have a copy made. The citizen will be charge the amount for copying. If a person would like to review it will be done in this office only. • • • • PRELIMINARY SUBSURFACE SOIL ASSESSMENT for SOLAG DISPOSAL MAINTENANCE YARD • at 31731 Paseo Adelanto San Juan Capistrano, California • Job Number 6409 • Prepared by • AMERICAN ENVIRONMENTAL MANAGEMENT CORPORATION 10960 Boatman Way Stanton, California 90680 (714) 826-6320 • April 1, 1992 • ncevxcowrcx • TABLE OF CONTENTS • 1.0 INTRODUCTION 2 2.0 DESCRIPTION OF FACILITY 2 • 2.1 REGIONAL GEOLOGIC AND HYDROLOGIC SETTING 3 3.0 DESCRIPTION OF FIELD ACTIVITIES 4 4.0 CONCLUSIONS AND RECOMMENDATIONS 7 • APPENDIX A BORING LOGS APPENDIX B LABORATORY ANALYTICAL RESULTS AND CHAIN OF CUSTODY DOCUMENTATION • • • • • • aEcn¢o rvEa • Pmhmtr gSmsudare SoilA Msm nl W.g Dispo M..(e n YW 1.0 INTRODUCTION • American Environmental Management Corporation (AEMC) has been contracted by Solag Disposal to perform a preliminary subsurface soil assessment at its San Juan Capistrano Maintenance Yard. The purpose of this assessment was to provide a preliminary evaluation of the chemical • quality of the soils beneath the subject property. This assessment was limited to the soils beneath a gravel/road base cover, which varied in thickness from 6 inches to 3 feet, and above groundwater saturated soils, encountered between 16 and 19 feet below ground surface. • This subsurface soil assessment consisted of drilling ten shallow soil boreholes in readily accessible areas of the subject property that potentially could have been exposed to various hazardous materials used • in the maintenance of vehicles and equipment. The following sections of this report describe the assessment activities and the subsequent laboratory analytical results. • 2.0 DESCRIPTION OF FACILITY The subject property is located at 31731 Paseo Adelanto in the City of San Juan Capistrano, California, as shown in the Site Location Map, Figure 1. The site is rectangularly shaped and is used as a maintenance and storage • yard for Solag Disposal's household solid waste removal company. The site is primarily occupied by several temporary office buildings and a large vehicle maintenance area. The remainder of the site consists of unpaved • parking and storage areas. The subject property currently houses a 10,000-gallon underground diesel storage tank, a 1,500-gallon above ground diesel storage tank, a 1,000- gallon above ground waste oil storage tank, and many other small • containers (i.e. 55-gallon drums or less) of various chemicals used for the maintenance of the Solag vehicles. The hazardous materials used at this site primarily consist of petroleum products such as diesel fuel, oil, greases and lubricants, and hydraulic oil, and other chemicals and materials used • for vehicle maintenance such as battery acid, paints, antifreeze, and brake fluid. • M&MWR01(4/92) 2 Cry gECY¢FO PMfP • Pml=nwy Sd urta Sod A m=nt So g Dispoaat Mainte YW According to a Preliminary Site Assessment Report prepared by Hekimian • and Associates, Inc. dated June 19, 1991, the subject facility was first occupied in early 1970 and was formerly accessed from the east through an entrance on Los Rios Street. This assessment report describes the surface of the subject property as displaying considerable evidence of fuel • and lubricant spills originating from poor maintenance and operation practices. This investigation was performed in the areas either displaying ground surface staining or in hazardous material storage areas. • 2.1 REGIONAL GEOLOGIC AND HYDROLOGIC SETTING The subject property is located within the northwestern end of the Peninsular Ranges Geomorphic Province of Southern California. The subject property is located in an area of the western foothills of • the Santa Ana Mountains. This area primarily consists of a series of marine terraces comprised of marine sedimentary rocks of Miocene and Pliocene age. California Division of Mines and Geology mapping of the site indicated that it is underlain by artificial fill which • overlays Quaternary (recent) stream alluvial deposits composed of sand, silt, clay, and some gravel. Erosion and alluvial deposition along with landsliding is currently taking place in this area. The soils encountered in the site assessment boreholes, drilled to a maximum • depth of 19 feet, primarily consisted of silt and sand and some fine gravels. The site is located on the eastern bank of the Trabuco Creek in an • area several hundred feet north of where it joins the San Juan Creek, which flows south into the Pacific Ocean. The site is located within the San Juan Groundwater Basin. Groundwater in the San Juan Groundwater Basin is contained within alluvial material, in • unconfined conditions, and receives recharge from direct infiltration of stream flow and rainfall, subsurface inflow from sedimentary bedrock, and agricultural return flows. Groundwater flow in the basin is generally directed to the south or southwest similar to the • surface flow of the San Juan and Trabuco Creeks. According to the Capistrano Valley Water District, there is a water well within several • RB& R01(4/92) 3 HY BftYfLfO YWEP • Pm imivry SubcuAace Soil 6aseasmem Solag Dvgl l Maiole"=Yard hundred feet north of the subject property. The depth to water at • that well is approximately 17 feet below ground surface. Groundwater was encountered at 16 to 19 feet below the subject property during AEMC's soil borehole drilling. • 3.0 DESCRIPTION OF FIELD ACTIVITIES Prior to the commencement of any site assessment field activities, AEMC prepared a Site Health and Safety Plan. The Health and Safety Plan • outlined the safety procedures that were followed by AEMC during the soil borehole drilling. Daily tailgate health and safety meetings were conducted by AEMC each day field work was performed, in order to implement the Health and Safety Plan requirements. All field activities were performed under the direct supervision of Mr. Kevin Sheridan, Project Geologist for AEMC, working under the supervision of Mr. Richard Harness, Engineering Division Manager for AEMC, (Registered • Professional Engineer #41339). Additionally, the borehole drilling was witnessed by Ms. Beth Padon, M.S. Archaeologist for LSA Associates, Inc. due to the site's proximity to historically sensitive areas such as the San Juan Capistrano Mission. • On March 12, 1992, ten soil boreholes were drilled to evaluate the unsaturated subsurface soil conditions. The ten boreholes were drilled to depths of 16 to 19 feet below ground surface (i.e. until groundwater was encountered). The boreholes were sampled at five-foot intervals, starting at 5 feet below ground surface. The soil borehole locations are shown in Figure 2. • The boreholes were drilled using a truck-mounted drilling rig (Mobile B-53) provided by Drill Line Industries of Norwalk, California. Drill Line Industries has a C-57 contractors license for drilling and well installation. The boreholes were drilled with six-inch outside diameter hollow stem augers. • The borehole soil samples were collected in stainless steel 18-inch split- barrel samplers fitted with three six-inch brass sample liners. The center • R3&6 R91(4/92) 4 eecrcLE9 vuee • Prclimiwy Subcurfaa Soil Acrenmcm Solag DiaWcal Maiataa Yard sample liner was retained for analysis. The ends of the center sample liner • were covered with aluminum foil, capped with plastic caps, and labeled. All soil samples collected from the boreholes were shipped to AEMC's state-certified laboratory to Rancho Cordova, California, using standard • chain of custody documentation. All of the borehole soil samples were analyzed by EPA Method 8015 for total petroleum hydrocarbons (TPH) as gasoline and diesel and 8240 for volatile organic compounds (VOC). Additionally, the 5-foot sample from each borehole was also analyzed by • EPA Method 9040 for pH, EPA Method 8080 for polychlorinated biphenyls (PCB's) and Title 22 metals for total threshold metal concentrations. The borehole lithologies were logged on a boring log by an AEMC • geologist utilizing the Unified Soil Classifications Systems (USCS). Boring logs are included with this report in Appendix A. Upon conclusion of the soil borehole drilling, the boreholes were backfilled • with a six-sack concrete slurry mix. All generated soil cuttings were placed in 55-gallon drums and currently remain on-site. All sampling and drilling equipment was properly cleaned to minimize the • potential for cross-contamination. The augers and drilling equipment were steam cleaned off-site prior to their use. The sampling equipment was washed in tap water with alconox, and then rinsed in distilled water between sample. • The laboratory analytical results of the soil borehole drilling are summarized below in Table 1 and contained in full in Appendix B. • • • 0&6 MR91(4j92) 5 PELYLLEO MffP • PrclimiLLary Subsurface SoilAaeasmenSofas U qe lM.nt.".Yud • TABLE 1 SUMMARY OF SOIL BOREHOLE SAMPLES LABORATORY ANALYTICAL RESULTS SOLAG DISPOSAL-SAN JUAN DISPOSAL • Sample I.D. EPA Method EPA Method EPA Method EPA Method Borehole# 8240 8015 8080 9040 Depth (feet) VOC's (ppb) TPH (ppm) PCB's (ppm) pH • BH1-1 ND ND ND 7.9 BH1-10 ND ND - BH7-15 ND ND - BI-12-5 ND ND ND 8.7 • BH2-10 ND ND - BH2-15 ND ND - BI-13-5 ND NO NO 8.5 BH3-10 ND ND - BH3-15 ND NO • BI-14-5 ND ND ND 8.7 BI4-10 ND NO BI-14-15 ND NO BI-15-5 ND ND ND 8.6 • BH5-10 ND NO BH5-15 ND ND BH6-5 ND ND ND 8.7 BI-16-10 NO ND BH6-15 ND ND - • BH7-5 ND ND ND 7.5 BH7-10 ND ND - BH8-5 ND ND ND 7.9 BI-18-10 NO NO - • BHB-15 ND ND - BH9-5 ND ND ND 7.5 131-19-10 NO NO - BH9-15 ND ND • F38:6f09R01(4/92) 6 Cp PELTCLFDM1ffl • PreLmine,y SWsurfnm Soil prsettmcm S Ng D.P.1 wmt'ante Ynrd • TABLE 1 (continued) SUMMARY OF SOIL BOREHOLE SAMPLES LABORTORY ANALYTICAL RESULTS SOLAG DISPOSAL-SAN JUAN DISPOSAL • Sample I.D. EPA Method EPA Method EPA Method EPA Method Borehole# 8240 8015 8080 9040 Depth (feet) VOC's (ppb) TPH (ppm) PCB's (ppm) pH BH10-5 ND ND ND 7.8 BH10-10 ND ND - BH10-15 ND ND • ND = NOT DETECTED - = NOT TESTED Metals analyses not reported in table, however all TTLC values were below 10 times the STLC value • The laboratory analytical results reported in Table 1 indicate that the soils encountered in the boreholes do not contain detectable amounts of • VOC's, TPH, or PCB's, and have a normal range of pH values. Additionally, the TTLC metals analyses appear to be attributable to typical background soil concentrations that do not require further analyses or soluble content determinations. • 4.0 CONCLUSIONS AND RECOMMENDATIONS Based on the soil sampling activities and the subsequent laboratory • analytical testing described in this report, AEMC concludes the following: There were no TPH, VOC's or PCB's detected in the borehole soil samples. Additionally, pH and metal • concentrations appeared to be within normal ranges. • F3&6109R01(A/92) 7 eC flFLmLEwKfl • Prtlivtiaary Sab.0 Soil Assessment S9 g Disp9 MainEee Ye There was six inches to three feet of a crushed rock/gravel • road base mix on the majority of the ground surface of the subject property. This road base appears oil stained in many areas; however, it was not evaluated in the scope of work for this project. • Areas that were not readily accessible to drilling equipment, or that were occupied by a structure or concrete pavement were not evaluated in the scope of work for this project. • Additionally, a leak detection investigation for the underground storage tank was not performed. Groundwater was encountered at 16 to 19 feet below ground • surface in the soil boreholes; however, groundwater was not evaluated in the scope of work for this project. The site's compliance with existing environmental regulations • was not evaluated in the scope of work for this project. • • • • • F38 MWM1(</92) 8 CO flELYCEfD PVffl Pr ..Y SQA.rt S fl Aeseumevt Solas Diapoml Maivtemv Yard Report Prepared By: Kevin Sheridan Project Manager Report Reviewed By: � a Richard L. Harness Engineering Division Manager 066109RD1(4/92) 9 ®flFLYCIEp VPRfl • 0 N A i it N N1 • VACANTLOT s m X x- % ppppERT uNE X _- -QX /TIRE INSTALLATION AND PAINTING AREA I BH10+ X E � Q x • UNPAVED I — 4!1 HS STORAGE YARD SUBSURFACE---- BH6 {� X x � DUMPSTER 4 RAMP VEHICLE MAINTENANCE AREA BHS WITH CONCRETE PAD • �8H1 X t BH3+ 4 20 ^co ®a® 65% Bli9 X�_X PARKING BH2 '1 � o J FUELING STATION gHq+ +BH7 X r�X • 0400 —� X FENCE f 10,000-GALLON DIESEL UNDERGROUND STORAGE TANK o0o X --------- — X X X —X 1,000-GALLON WASTE OIL ABOVEGROUND STORAGE TANK X'— FRESH LUBRICANT FRESH MOTOR OIL AND DIESEL ABOVEGROUND STORAGE TANK • 1,500-GALLON DIESEL ABOVEGROUND STORAGE TANK(NOT USED) %G 0 TN LEGEND: O PROPOSED BORING LOCATION • 0�� STORAGE YARD 0 STORAGE CONTAINERS AND TRAILERS Z TEMPORARY OFFICE$AND PARTS STORAGE B114S O • N BORING LOCATION MAP UNIFIED SOIL CLASSIFICATION SYSTEM MAJOR DIVISIONS SYMBOL TYPICAL NAMES GW . . :: WELL GRADED GRAVELS,GRAVELS,GRAVEL-SAND MIXTVRE9 CLEAN GRAVELS GRAVELS WITH LITTLE OR NO FINES• GP `�"- ;1::: POORLY GRADED GRAVELS,GRAVEL-SAND MIXTURES MORE THAN HALF J COARSE FRACTION O 0 IS LARGER THAN GM SILTY GRAVELS,POORLY GRADED GRAVEL-SANG-SILT MIXTURES U) NO.4 SIEVE SIZE GRAVELS WITH p OVER 12%FINES W /+! CLAYEY GRAVELS,POORLY GRADED GRAVEL-SANG . Z ¢ GC CLAY MDMRES Qw tY CLEAN SANDS SW L WELL GRADED SANDS,GRAVELLY SANDS LL SANDS WITH LITTLE OR cr cr NO FINES SP POORLY GRADED SANDS,GRAVELLY SANDS Oi MORE THAN HALF COARSE FRACTION S M SILTY SANDS,POORLY GRADED SAND-SILT MD(TURES IS SMALLER THAN SANDS WITH NO.4 SIEVE SIZE OVER 12%FINES SC CLAYEY SANDS,POORLY GRADED SANDCLAY MLXTURES . INORGANIC SILTS AND VERY FINE SANDS,ROCK ML FLOUR,SILTY OR CLAYEY FINE SANDS,OR CLAYEY SILTS WITH SLIGHT PIASTOTY 5mQ SILTS AND CLAYSNOHGNICMVCLAYS OF LOW TO MEDIUM PLASTICITY y CL GELLYCLAYS,SANDY CLAYS,SILTY CLAYS, LIQUID LIMIT LESS THAN 50 LEAN CLAYS Lu OL1;1p1 I I ORGANIC CLAYS AND ORGANIC SILTY CLAYS OF 1 I LOW PLASTICT(Y z H A A I..I INORGANIC SILTS,MICACEOUS OR DIATOMACIOUS cc IYI FINE SANDY OR SILTY SOILS,ELASTIC SILTS ul SILTS AND CLAYS Z CILLL INORGANIC CLAYS OF HIGH PLASTICITY, FAT CLAYS Ll Wa LIQUID LIMIT GREATER THAN 50 3 OH /// ORGANIC CLAYS OF MEDIUM TO HIGH PLASTICITY/// ORGANIC SILTS HIGHLY ORGANIC SOILS PT PEAT AND OTHER HIGHLY ORGANIC SOILS SOIL CLASSIFICATION CHART AMERICAN 3Solag 1731 Disposal 31731 Paseo Adelanto ENVIRONMENTAL MANAGEMENT CORP. San Juan Capistrano, Calitomia PROJECT NUMBER DATE: PM FIGURE 6409 3/92 • Boring Location: SEE SITE PLAN Elevation and Datum: GROUND SURFACE Drilling Company. DRILL LINE INDUSTRIES Date Started: 3/12/92 Date Finished: 3/12/92 S Drilling Equipment: MOBIL B53 /6-INCH HOLLOW STEM AUGER Date Developed/Sampled: NA Type/Diameter of Casing: NA Completion Depth: 16.0-FEET Type of Perforation: NA Number of Samples: 3 Type of Perforation Backfill: NA Water Depth: APPROXIMATELY 15.0-FEET • Type of Seal: CEMENT GROUT Logged By: Mi Checked By: Graphic Log Samples Description $ E S Remarks a • z � # b _ Unpaved at surface Road base to 2V c!;!E 5 SAND-light grey brown,dominantly medium grained, SP 70 s.o- a++-5 sub-angular,damp,very dense,odorless 6.0 • 10 GRAVELLY SAND-light grey brown,20%gravel,well sw 58 +e. BII+-+o graded,predominantly medium grained,subrounded,to ++'e subangular,moist,very dense,odorless • 15 SILTY SAND-light orange brown,medium coarse, SP subrounded,moist,trace silt,vary dense,odorless +e.o Drilling terminated at 15.64eet. • 20- 25- 30 • LOG OF BORING BH1 AMERICAN 3Solag 1731 Disposal 31731 Paseo Adelanto ENVIRONMENTAL MANAGEMENT CORP. San Juan Capistrano, Calffomia • PnomcrNUMBER DATE: PM 6409 3/92 PAGE 1 OF 1 • Boring Location: SEE SITE PLAN Elevation and Datum: GROUND SURFACE Drilling Company: DRILL LINE INDUSTRIES Date Started: 3/12/92 Date Finished: 3/12/92 Drilling Equipment: MOBIL B53 /6-INCH HOLLOW STEM AUGER Date Developed/Sampled: NA f Type/Diameter of Casing: NA Completion Depth: 16.0-FEET Type of Perforation: NA Number of Samples: 3 Type of Perforation Backfill: NA water Depth: APPROXIMATELY 15.0-FEET • Type of Seal: CEMENT GROUT Logged By: MJ Checked By: Graphic Log Samples s 8 Description S EE 4 8 Remarks � a o z y m E • � b 3 � b � s z' Unpaved at surface 1: Road base to 24' to 5— SAND-grey brown,fine to coarse grained,moist,medium SP 30 5.0- BH2-5 dense,odorless 6.0 10 SILTY SAND-yellow brown,20%silt,fine to medium SM 25 ro.a BM-10 grained,moist,medium dense,odorless ri.o • 15 SILT-olive brown,trace sand and Gay,very moist,wet, ML 55 u.a BH2-15 very dense,odorless 1 16.0 Drilling terminated at 15.0-feet. • 02530 20- 25- 30 LOG OF BORING BI-112 Solag AMERICAN 31731 Disposal 31731 Paseo Adelanto CNVIRONMENTAL MANAGCMENT CORP. San.Juan Capistrano,California • MOJECTNUMUM DAM PM PAGE 1 OF 1 6409 3/92 • Boring Location: SEE SITE PLAN Elevation and Datum: GROUND SURFACE Drilling Company: DRILL LINE INDUSTRIES Date Started: 3/12/92 Data Fniahed: 3/12/92 Drilling Equipment: MOBIL B53 /6-INCH HOLLOW STEM AUGER Date Developed/Sampled: NA • Type/Diameter of Casing: NA Completion Depth: 16.0-FEET Type of Perforation: NA Number of Samples: 3 Type of Perforation Backfill: NA Water Depth: APPROXIMATELY 16.0-FEET • Type of Seal: CEMENT GROUT Logged By; Mi Checked By: Graphic Log Samples 8 Description $ Ea 8 Remarks a C3 m $ m M b is s z Unpaved at surface r:>a Road base to 18' S SAND-grey brown,fine to coarse,dominantly coarse, Sw 24 e.a BN9s subangular to subrounded,moist,medium dense, 7'0 odorless 10— SAND-light orange brown,trace fine gravel,coarse to sw eo 10.0 BNs-1e . medium,well graded,subrounded to subangular,moist, 1'0 very dense,odorless I, SAND-light orange brown,trace fine gravel,coarse to 15 medium,well graded,subrounded,wet,very dense, sw W/s• 1s.0. BH3.15 odorless +e.c Drilling terminated at 15.0-feet. • 02530 20- 25- 30 LOG OF BORING BH3 AMERICAN 3Solag 1731 Disposal 31731 Paseo Adelanto ENVIRONMENYAL MANAGEMENT CORP. San Juan Capistrano, California PROJECT NUMBER DATE PM 6409 3/92 PAGE 1 OF 1 • Boring Location: SEE SITE PLAN Elevation and Datum: GROUND SURFACE Drilling Company: DRILL LINE INDUSTRIES Date Started: 3/12/92 Date Finished: 3/12/92 i Drilling Equipment: MOBIL B53/6-INCH HOLLOW STEM AUGER Date Developed/Sampled: NA Type/Diameter of Casing: NA Completion Depth: 16.0-FEET Type of Perforation: NA Number of Samples: 3 Type of Perforation Backfill: NA Water Depth: APPROXIMATELY 15.0-FEET • Type of Seal: CEMENT GROUT Logged By: MJ Checked By: Graphic Log Samples n Description53 a S y ¢ i Remarks. e E 0— unpaved at surface Roadbase to 18' 5 GRAVELLY SAND-grey brown, 15%gravel,fine to coarse, Sw 35 5.a eHa5 well graded,subangular to subrounded,moist,dense, 6.0 odorless 10 SAND-trace gravel,light orange brown,well graded, sw nio.o BH4.10 subangular,moist,medium dense,odorless 15— SANDY SILT-olive brown,20%sand,wet,medium dense, ML 0 15.0- er4.15 i ododess 16.0 Drilling terminated at 15.0-11eeL 20- 25 30 LOG OF BORING BH4 AMERICAN 3Solag 1731 Disposal 31731 Paseo Adelanto ENVIRONMENTAL MANAGEMENT CORP. San Juan Capistrano, California PnOJECr NUMBER DATE nM 6409 3/92 PAGE 1 OF 1 • Boring Location: SEE SITE PLAN Elevation and Datum: GROUND SURFACE Drilling Company: DRILL LINE INDUSTRIES Date Started: 3/12/92 Date Finished: 3/12/92 • Drilling Equipment: MOBIL B53 /6-INCH HOLLOW STEM AUGER Date Developed/Sampled: NA Type/Diameter of Casing: NA Completion Depth: 16.0-FEET Type of Perforation: NA Number of Samples: 3 Type of Perforation Backfill: NA Water Depth: APPROXIMATELY 16.0-FEET • Type of Seal' CEMENT GROUT Logged By: MJ Checked By: Graphic Log Samples s Description $ o a Remarks • a - E 3 a a .1; z 0— Unpaved at surface Roadbase to 18" • 5— SAND-grey brown,medium grained,moist,dense, SP +0 5.o- BH5-5 odorless 8.0 10 SAND-grey brown,fine to costae,trace gravel, SP e5 iao BH5-10 subangular,moist,very dense,odorless 15 SANDY SILT,-olive brown,trace clay,moist,medium ML 32 Tao- BH5-15 dense,odorless 180 V Drilling terminated at 15.0-feet. • • 20- S3025- 30 LOG OF BORING BH5 AMERICAN 3Solag 1731 Disposal 31731 Paseo Adelanto ENVIRONMENTAL MANAGEMENT CORP. San Juan Capistrano, California PPMEM NUMSM Mie: PM 6409 3/92 PAGE 1 OF 1 Boring Location: SEE SITE PLAN Elevation and Datum: GROUND SURFACE Drilling Company: DRILL LINE INDUSTRIES Date Started: 3/12/92 Date Finished: 3/12/92 . Drilling Equipment: MOBIL B53 /6-INCH HOLLOW STEM AUGER Date Developed/Sampled: NA Type/Diameter of Casing: NA Completion Depth: 16.0-FEET Type of Perforation: NA Number of Samples: 3 Type of Perforation Backfill: NA Water Depth: APPROXIMATELY 15.0-FEET Type of Seal: CEMENT GROUT MJ Logged By: Checked By: _ Graphic Log Samples d CL Descriptlon S E 8 Remarks _ a m 8 ° a Z E 3 s Z. 0 Unpaved at surfaceT1!. Roadbase to 30' 0 6 SAND-gray brown,trace gravel,Tine to coarse, SP V 5.a BH" subangular,moist,medium dense,odorless s'0 10— SAND-grey brown,fine to coarse dominantly medium, SP 35 Io.o BHS-ro . moist,dense,odorless 1 GRAVELLY SAND-light orange brown,15%gravel, V 15 medium to coarse,subangular,very moist,wet,very SP 70 15.0- BM&15 dense,ododeas I Ire.o Drilling terminated at 16.0-feet. 02530 20- 25- 30 LOG OF BORING BH6 Solag AMERICAN 31731 Disposal 31731 Paseo Adelanto ENVIRONMENTAL MANAGEMENT CORP. San Juan Capistrano, Califomia i PF*JEM NUMBER DATE: PM 6409 3/92 PAGE 1 OF 1 • Boring Location' SEE SITE PLAN Elevation and Datum: GROUND SURFACE Drilling Company: DRILL LINE INDUSTRIES Date Started: 3/12/92 Date Finished: 3/12/92 • Drilling Equipment: MOBIL B53 /6-INCH HOLLOW STEM AUGER Date Developed/Sampled: NA Type/Diameter of Casing: NA Completion Depth: 15.0-FEET Type of Perforation: NA Number of Samples: 2 Type of Perforation Backfill: NA Water Depth: APPROXIMATELY 15.0-FEET • Type of Seal: CEMENT GROUT Logged By: Mi Checked By: Graphic Log Samples IT � c Description $ 4 $ Remarks • $ o 3 3 b 2 0 Unpaved at surface Roadbase to 12" 5 SILTY SAND-20%to 30%sit,dark olive brown,fine SM n 5.o- SH7-5 grained,from medium,medium dense,moist,odorless 8.0 • 10 GRAVELLY SAND-grey to grey brown,15%to 20% SP 32 Io.o- BH7-I0 gravel,fine to coarse,subrounded,moist,dense,odorless I'0 r 55 Iao- ern-u su.IPI.EnTttalrrEo 18.0 00 FECovERvl 15Drilling terminated at 15.0-feat. • 20- • 25 • 30 LOG OF BORING BI-117 Solag AMERICAN 31731 Disposal 31731 Paseo Adeianto . CNVIRONMENTAL MANAGEMENT CORP. San Juan Capistrano, California Pnr rEMNUMBER DATE: PM 6409 3/92 PAGE 1 OF 1 Boring location: SEE SITE PLAN Elevation and Datum: GROUND SURFACE Drilling Company: DRILL LINE INDUSTRIES Date Started: 3/12/92 Date Finished: 3/12/92 i Drilling Equipment: MOBIL B53 /6-INCH HOLLOW STEM AUGER Date Developed/Sampled: NA Type/biameter of Casing: NA Completion Depth: 16.0-FEET Type of Perforation: NA Number of Samples: 3 Type of Perforation Backfill: NA Water Depth: APPROXIMATELY 15.0-FEET Type of Seal: CEMENT GROUT Logged By: MJ Checked By: Graphic Log Samples s Description $ E a 8 Remarks 8 9 a 2 E • 3 e df s z 0 Unpaved at surface Roadbase to 24' 5— SAND-dark grey brown to dark brown,fine grained, SP 25 5.o- SHe-5 . moist,medium dense,odorless 6.0 10 SAND-dark grey brown,trace sift fine to coarse grained, SP as mo. BH&I O dominantly fine,trace fine gravel,slightly moist,dense, 11'0 odorless GRAVELLY SAND-grey to grey brown,20%to 30%fine 15 gravel,fine to coarse,subrounded,very moist to wet, SP 35 15.o- BHe-15 V dense,odorless 16.0 Drilling terminated 15.0-feet. 20- 24 30 LOG OF BORING BI-118 AMERICAN 3Solag 1731 Disposal 31731 Paseo Adelanto ENVIRONMENTAL MANAGEMENT CORP. San Juan Capistrano, California PROJECT NUMBER DAM PM 6409 3/92 PAGE 1 OF 1 • Boring Location: SEE SITE PLAN Elevation and Datum: GROUND SURFACE Drilling Company: DRILL LINE INDUSTRIES Date Started: 3/12/92 Date Finished: 3/12/92 • Drilling Equipment: MOBIL B53/6-INCH HOLLOW STEM AUGER Date Developed/Sampled: NA Type/Diameter of Casing: NA Completion Depth: 3 Type of Perforation: NA Number of Samples: 16.0-FEET • Type of Perforation Backfill: NA water Depth: APPROXIMATELY 15.0-FEET Type of Seal: CEMENT GROUT Logged By: MJ Checked By: Graphic Log Samples W • 8 Description SE E Remarks a 0 c 2 0 Unpaved at surface Roadbese to 12. 40 5 SAND-gray brown,fine to medium grained,quartz, SP 35 5.0- BHa5 feldspar and rock fragments,dense,moist,odorless 6.0 • 10— SM 37 too- BHo-10 SILTY SAND-dark grey brown,10%to 20%silt,fine to 11a medium grained,subrounded,moist,dense,odorless GRAVELLY SAND-grey brown,1 D%to 20%fine gravel, 15 dominantly coarse grained,very moist to wet,dense, sP e5 t5.o- BHa1s — odorless 1 116.0 Drilling terminated at 15.0-feet. I• 02530 20- 25- 30 LOG OF BORING BH9 AMERICAN 3Solag 1731 Disposal 31731 Paseo Adelanto • ENVIRONMENTAL MANAGEMENT CORP. San Juan Capistrano, Calffomla PRD.IECr NUMBER LUTE: 6409 3/92 PAGE 1 OF 1 Boring Location: SEE SITE PLAN Elevation and Datum: GROUND SURFACE Drilling Company: DRILL LINE INDUSTRIES Date Started: 3/12/92 7e Fnlshed: 3/12/92 Drilling Equipment: MOBIL B53/6-INCH HOLLOW STEM AUGER Date Developed/Sampled: NA • Type/Diameter of Casing: NA Completion Depth: 19.5-FEET Type of Perforation: NA Number of Samples: 3 Type of Perforation Backfill: NA water Depth: APPROXIMATELY 19.5-FEET Type of Seal: CEMENT GROUT Logged By: KS Checked By: Graphic Log Samples Description S E 4 8 Remarks a a 8 3 E i D Unpaved at surface t; Roadbase to tY 'i.• �—SILTY SAND-oil"brown,20%to 30%silt,fine grained, sM w s.o- BHIo-5 massive,slightly moist,medium dense,odorless 8.0 10— SAND-grey brown,fine to coarse grained,dominantly SP as io.o- BHIP10 medium grained,subrounded,dominantly quartz 10 feldspar,slightly moist,dense,odorless 15 SILTY SAND-dark grey to black,10%to 20%silt,fine to sM re.o- BHIP15 coarse grained,high organic content(roots,etc), teo subrounded,very moist,dense,odorless V 20Drilling terminated at 19.5-feet. 25 30 LOG OF BORING BH10 Solag jAILMERICAN 31731 Disposal 31731 Paseo Adelanto ENVIRONMENTAL MANAGCMENT CORP. San Juan Capistrano, California . PRC.IECTNUMBER wre PM 6409 3/92 PAGE 1 OF 1 • • • • APPENDIX B • LABORATORY ANALYTICAL RESULTS AND CHAIN OF CUSTODY DOCUMENTATION • • • Cp PEfY0.f0 V1MP / CLIENT JOB NUMBER ANALYSIS REQUESTED DESTINATION LABORATORY •► i 1KF AELC 3249 �L •. i •RD. • i RANCHO CORDOVA,GA. 95742 OTHER JOB DESCRIPTION w 1 SITE LOCATION ' TURN A"WIR TV9 NOTE/FIELD HEADINGS DATE I TIME ioerunFlCnT1aN © ®® ®®®® ■wpm mm.■MENEM 1101111 milli ■.nnnnn■■■■ ■■n ■ ■3■■■■■■■moil Nil■Ine©■■■■�■ ISO 00■■■■1■i■■1■I■■■■■■.■. ■■� �i■■■■■■■■1■1■■1 I■■■■MIN ME In 11 1 M ■■■■. ■■� I . ON IN ■■111■■■.■ME BEEN! in1111111 .■.■ ■■ mom 11111111 ■■ll.111011101 ©©■■ ■■■C NO MM NE RELINQUISHED BY(SIGN) I PRINT NAME/COMPANY DATE/TIME I RECD N) I PRINT NAMRLPAMPANY,~' a /V. WO-) �� . . _ d/ _ . .WN. .. SHIPPED VIA )�� • AMERICAN CHAIN OF CUSTODY OJVIRONMi11RAL LA.oRYL,oRRS CORR � �y6 S- LOG No. 24919 CLIENTNAME�'dL� �( D •: FIELD CONDITIONS: cLoob\ ADDRE57 q pASEO F1'DB CA I"` �/ 45,9, •-:, N "W --o ^Kn I 6c, oIII �'TY`• :L)U A-I V \1/-L't'6 s�/'-/11�L� G O _' � _ O COMPOSITE: PROJECT NAME�L� QX� JU# I�AELC y d RAN HO CORDO .0 m n / , O„ S PROJECT MANAGER P D PHONEY RANCHOCORDOV9572 on_) nJ e OTHER SAMPLED BY � ALkSQN! Q SPECIAL JOB DESCRIPTION Prta 0I0 E'Silo w Solt- 0 DK c<I1! APb -SAPA90IS& SITE LOCATION ' TUM , .•OR TIME, NOTE I FIELD READINGS SR►� JtlA►� o�P)S�R�a � �� � a � � � �, L F � v0 W NW F; q � CONTAINER > � O_ O � DEPTH METHOD TYPE NO. = 3 L I arts X X x X X p ;;Y r16 -ro` Io c s I31�S -S s g: :✓3HS'yor Ib K x Iv. qo to tt SUSPECTED CONSTITUENTS SAMPLE RETENTION TIME PRESERVATIVES: (1)HCL (3)=COLD (2)HNO3 (4) V. 3 7-17-17-7771 AT BV: DATE/TIME: CONDITIONS/COMM NTS: r (ncle� - - 15-!00 / , !t c •• ! ❑ FED XUPS ❑ OTHER_ AIRBILL 4 �532_tCL -- 3.36 AMERICAN CHAIN OF CUSTODY ..YwRONMiNTALLAYYT]RATOR�i CORR ��96 LOG No. 2 4 9 2 0 CLIENT NAME . TED FIELD CONDITIONS: 50 L' DtSPo R �- . ADDRESS res P_x O' =:k at -.i.h ti'e 9 W cz-oVOy �Q J V t 5 6O AELC < O 0 COMPOSITE: PROJECT NAME_dL -50 _ r ✓�+ 3249 FITZGERALD RD. .D.( PROJECT MANA E PHONEY RANCHO CORDOV957 2 mD N SAMPLED BY tis p` r (-AC✓� .1 ❑ OTHER ti G NU • SPECIAL INSTRUCTIONS: JOB DESCRIPTION SOIL. L-k SITE LOCATION ri,; TON ARONR TWF NOTE FIELD READINGS A-d WiSTgAfU1Z W Z m uF Y N o o �W N NO • CONTAINER = _ ?� 3 i • DEPTH METHOD TYPE NO. S 12 I I t zo :? }12 1+5A Sots, t1 ;2.3 02 — /p+c ro D - Lvmo 1t :�I Bif'I �to to fd� k SUSPECTED CONSTITUENTS SAMPLE RETENTION TIME PRESERVATIVES: (1)HCL (3)-COLD (2)HNO3 (4) RELIN • • • •. • : MRkyN 3 hCK-50d ke 3-rz-az zP fyi R TLAB DATEITIME: CONDITI S/COMMENTS: S w •• . ❑ FED X UPS ❑ OTHER AIRBILL N �$33 _ Lq�_ j AMERICAN ENVIRONMENTAL LABORATORIES CORP. • AEMC 03/27/92 10960 Boatman Way Stanton, CA 90680 Attention: Kevin Sheridan • Reference: Analytical Results Project Name: Solag - San Juan AELC ID No. : L8465 Pro]'ect No. : 6409 AELC Job No. : 6409 Date Received: 03/13/92 Chain Of Custody: 24918 - 24920 The following analyses were performed on the above referenced project: No. of Turnaround Samples Time Analysis Description 10 14 Days CAM Metals, TTLC, EPA Method 6010/7000 29 14 Days TPH Volatiles by DHS Method - EPA M8015 29 14 Days TPH as Diesel by DHS Method - M8015 10 14 Days PCB's in Soil, Sludge or Other Oil 29 14 Days Volatile Organic Compounds by GC/MS 10 14 Days pH measurement, electrometric These samples were received by American Environmental Laboratories in a chilled, intact state and accompanied by a valid chain of custody document. Analytical results are attached to this letter. Please call if we can provide additional assistance. Sincere y ' George Hampton Laboratory Director 3e •,mru.ww 3249 Fitzgerald Rood•Rarcho C=ovo.CA 95742•Fox 1916)638-4510-(9161638-7301 AMERICAN ENVIRONMENTAL LABORATORIES CORP. Positive Analytical Results Summary The purpose of the attached data summary is to supplement -- rather than replace -- the comprehensive analytical report. Much of the information contained only in the full report -- including sample collection, receipt and analysis dates; chain of custody documentation; reporting limits; identification of analytes which were tested for but not detected; and QA/QC data including method blank results and surrogate standard and matrix spike compound recoveries -- is essential to a responsible evaluation of the analytical results summarized here. PAA.Su*'L920305 3249 902r.leraid Road•Rancno CardOva.CA 95742•Fcx(910)o38-4510•1916 6387301 AMERICAN ENVIAONMEE LAHICAIES CORP. CA DOHS ELAP Accreditation/Aegiatratlan Number 1233 POSITIVE ANALYTICAL RESULTS SUMMARY Client: AEMC Boatman Project No. : 6409 10960 Boatman Wap Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Received: 03/13/92 COC Log No. : 24918 - 24920 Date Reported: 03/31/92 AELC ID No. : L8465 POSITIVE RESULTS Sample I.D. Client AELC Analyte CAS No. Value BH10-5 1A pH N/A 7.8 Standard Units As (((Arsenic) 7440-38-2 6 . 3 mg/kg Ba (Barium) 7440-39-3 63 mg/kg Cr ((Chromium) 7440-47-3 12 mg/kg Co Cobalt) 7440-48-4 6.8 mg/kg Cu (Copper) 7440-50-8 16 mg/kg Ni (Nickel) 7440-02-0 11 mg/kg Pb (Lead) 7439-92-1 20 mg/kg V (Vanadium) 7440-62-2 27 mg/kg Zn (Zinc) 7440-66-6 47 mg/kg BH9-5 4ApH N/A 7.5 Standard Units As (Arsenic) 7440-38-2 2.5 mg/kg Ba (Barium) 7440-39-3 16 mg/kg Cu (Cop er) 7440-50-8 9 .9 mg/kg Ni (Nickel) 7440-02-0 6.2 mg/kg Pb (Lead) 7439-92-1 7.3 mg/kg V (Vanadium) 7440-62-2 8.0 mg/kg Zn (Zinc) 7440-66-6 32 mg/kg BH8-5 7A pH N/A 7.9 Standard Units As (Arsenic) 7440-38-2 1.8 mg/kg Ba (Barium) 7440-39-3 27 mg/kg Cr (Chromium) 7440-47-3 6.2 mg/kg Cu (Copper) 7440-50-8 17 mg/kg Ni Nickel) 7440-02-0 6.9 mg/kg Pb Lead) 7439-92-1 11 mg/kg V Vanadium) 7440-62-2 15 mg/kg Zn Zinc) 7440-66-6 30 mg/kg BH7-5 l0A pH N/A 7.6 Standard Units As (Arsenic) 7440-38-2 1.1 mg/kg Ba (Barium) 7440-39-3 41 mg/kg Cr Chromium) 7440-47-3 7.1 mg/kg Cu Copper) 7440-50-8 19 mg/kg Ni Nickel) 7440-02-0 7.8 mg/kg Pb Lead) 7439-92-1 19 mg/kg V Vanadium) 7440-62-2 15 mg/kg Zn Zinc) 7440-66-6 38 mg/kg y BH6-5 12A pH N/A 8. 7 Standard Units As (Arsenic) 7440-38-2 2.1 mg/kg Ba (Barium) 7440-39-3 22 mg/kg Cu 7440-50-8 11 mg/kg Ni JCI:IpKer) Nicel) 7440-02-0 7 .2 mg/kg Pb Lead) 7439-92-1 7.9 mg/kg V Vanadium) 7440-62-2 14 mg/kg Zn (Zinc) 7440-66-6 29 mg/kg BH5-5 15A pH N/A 8.6 Standard Units � W- 3249 fihnerald Road•Rancro CJlQOYQ.CA 95742•=ax(o tb]638d$t0.1976)bJ9-7707 AMERICAN 6N"RON GNTAL LABORATORIES CORM CA DOHS FLAP Accreditation/Registration Number 1233 POSITIVE ANALYTICAL RESULTS SUMMARY Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Received: 03/13/92 COC Log No. : 24918 - 24920 Date Reported: 03/31/92 AELC ID No. : L8465 POSITIVE RESULTS(cont.) Sample I.D. Client AELC Analyte CAS No. Results As (Arsenic) 7440-38-2 1.8 mg/kg Ba (Barium) 7440-39-3 21 mg/kg Cu (Copper) 7440-50-8 18 mg/kg Ni (Nickel) 7440-02-0 7.7 mg/kg Pb (Lead) 7439-92-1 10 mg/kg V ((Vanadium) 7440-62-2 12 mg/kg Zn Zinc) 7440-66-6 29 mg/kg BH4-5 18A pH N/A 8.7 Standard Units As (Arsenic) 7440-38-2 1.0 mg/kg Be (Barium) 7440-39-3 17 mg/kg Cu Copper) 7440-50-8 8.7 mg/kg Ni Nickel) 7440-02-0 5.4 mg/kg Pb Lead) 7439-92-1 7 .4 mg/kg V Vanadium) 7440-62-2 8 .2 mg/kg Zn Zinc) 7440-66-6 27 mg/kg BH3-5 21ApH N/A 8.5 Standard Units As Arsenic) 7440-38-2 1.4 mg/kg Be Barium) 7440-39-3 14 mg/kg Cu Copper) 7440-50-8 13mg/kg Ni Nickel) 7440-02-0 6 .2 mg/kg Pb Lead) 7439-92-1 7 .2 mg/kg V Vanadium) 7440-62-2 9 .8 mg/kg . Zn Zinc) 7440-66-6 28 mg/kg BH2-5 24A pH N/A 8.7 Standard Units As (Arsenic) 7440-38-2 2.5 mg/kg Be (Barium) 7440-39-3 25 mg/kg Cr (Chromium) 7440-47-3 6.1 mg/kg Cu (Copper) 7440-50-8 14 mg/kg Ni I Nickel) 7440-02-0 6.6 mg/kg Pb Lead) 7439-92-1 12 mg/ g V Vanadium) 7440-62-2 15 mg/kg Zn Zinc) 7440-66-6 30 mg/kg BH1-5 27A pH N/A 7 .9 Standard Units As (Arsenic) 7440-38-2 5.5 mg/kg Be SIS Barium) 7440-39-3 43 mg/kg Cr Chromium) 7440-47-3 10 mg/kg Cu Copper) 7440-50-8 11 mg/kg Ni (Nickel) 7440-02-0 7.0 mg/kg Pb (Lead) 7439-92-1 i7 mg/kg V (Vanadium) 7440-62-2 20 mg/kg Zn (Zinc) 7440-66-6 34 mg/kg s$ •„an,P.o 3249 Fiageralo Road-Poncho Cordova.CA 95742•Far(9161638-4510•(916)638-7301 AMERICAN ENVIRONMENTAL LABORATORIES CORM CA DOHS ELAP AccreditatLon/Reaiatration Number 1233 Analysis Report: Total Petroleum Hydrocarbons by GC/MS, DHS TPH Draft Procedure Purge and Trap, EPA Method 5030/8260 C14ent: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465 Date Extracted: 03/1&/92 Batch No. : 8943 Date Analyzed: 03/18/92 Matrix: SOIL Date Reported: 03/29/92 ANALYTE Sample I.D. TPH as Gasoline Client AELC (mg/kg) BH10-5 lA ND BH10-10 2A ND BH10-15 3A ND BH9-5 4A ND BH9-10 5A ND BH9-15 6A ND BH8-5 7A ND BH8-10 8A ND BH8-15 9A ND BH7-5 10A ND Rep. Limit 1.0 ND - Not detected at or above indicated Reporting Limit Rep. Limit - Reporting Limit unless otherwise indicated in parentheses. r i. 04 +vai[o wnw 3249 Fitzgerald Road•Poncho Cordova,CA 95742•Fax(916)638-4.510•(916(638-7301 AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOES SLAP AccreditationlRegistration N=ber 1233 Analysis Report: Total Petroleum Hydrocarbons by GC/MS, DHS TPH Draft Procedure Purge and Trap, EPA Method 5030/8260 Client: &EMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Extracted: 03/18/92 COC Lo No. : 24918 - 24920 Date Analyzed: 03/18/92 AELC ID No. : L8465 Date Reported: 03/21/92 Batch No. : 8943 Matrix: SOIL METHOD BLANK Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) TPH as Gasoline N/A ND 1.0 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • on + ,,n.,.. 3249 Fitgeroid Road•Rancho Cordova,CA 45742•'-cx(916)638-4510•(416)638.7301 AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DONS SLAP Aecreditation/Reaiatratlon N=ber 1233 Analysis Report: Total Petroleum Hydrocarbons by GC/MS, DHS TPH Draft Procedure Purge and Trap, EPA Method 5030/8260 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Extracted: 03/18/92 COC Log No. : 24918 - 24920 Date Analyzed., 03/18/92 AELC ID No. : L8465 Date Reported: 03/25/92 Batch No. : 8943 Matrix: SOIL MATRIX SPIKE MS MS Gone. Recovery Analyte CAS No. (mg/kg) (percent) Gasoline N/A 2.0 106 MATRIX SPIKE DUPLICATE MSD MSD Gone. Recovery Analyte CAS No. (mg/kg) (percent) Gasoline N/A 2.0 99 RELATIVE % DIFFERENCE Relative Percent Difference Analyte CAS No. (percent) Gasoline N/A 7 , II� i �° •r„wo 3249 Fitzgerald POW•?ancno Cordova.CA 95,742•Fax(916)639-4510•(916)638-7301 AMERICAN ENVIPONMENTAL LABORATORIES CORP. CA DOHS ELAP Accreditation/Registration Number 1233 Analysis Report: Total Petroleum H drocarbons by GC/MS, DHS TPH Draft Procedure Purge and Trap, EPA Method 5030/8260 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Reported: 03/29/92 COC Log No. : 24918 - 24920 AELC ID No. : L8465 Batch No. : 8943 Matrix: SOIL LAB CONTROL STANDARD LCS LCS Conc. Recovery Analyte CAS No. (mg/L) (percent) Gasoline N/A 0.4 114 '4 -FC`1roo—w 3249 Fingeraid Roaa•Rancno Corcova.CA 95742•=ox(016)6384510•(916)638-7301 AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOSE ELAP ACCreditati./Registratlan N=ber 1233 Analysis Report: Total Petroleum Hdrocarbons by GS/MS, DHS TPH Draft Procedure Purge and Trap, EPA Method 5030/8260 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465 Date Extracted: 03/19/92 Batch No. : 8944 Date Analyzed: 03/19/92 Matrix: SOIL Date Reported: 03/29/92 ANALYTE Sample Z.D. TPH as Gasoline Client AELC (mg/kg) BH7-10 11A ND BH6-5 12A ND BH6-10 13A ND BH6-15 14A ND BH5-5 15A ND BH5-10 16A ND BH5-15 17A ND BH4-5 18A ND BH4-10 19A ND BH4-15 20A ND Rep. Limit 1.0 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. 4 . 1',1— 3240 Fitzgerald Road•Rancho Cordova.CA 95742•Fax(9+61 638-4510•(916)638-7301 AMERICAN ENVIRONMENTAL LASOPATORIE9 COPP. CA D09S ELAP Aeereditat ion/Reg Is trat ion Nomber 1233 Analysis Report: Total Petroleum Hydrocarbons by GS/MS, DHS TPH Draft Procedure Purge and Trap, EPA Method 5030/8260 Client: AEMC Boatman Project No. : 6409 10960 Boatman Wap Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Extracted: 03/19/92 COC Lo No. : 24918 - 24920 Date Analyzed: 03/19/92 AELC lD No. : L8465 Date Reported: 03/29/92 Batch No. : 8944 Matrix: SOIL METHOD BLANK Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) TPH as Gasoline N/A ND 1. 0 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses . 3249 Fitzgerald Road-Rancho Cordova.CA 95742•`ax(9161 o38-4510-(916)638-7301 AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DONS ELAP Aeeraditac Lon/RagL-t-ati— N=ber 1233 Analysis Report: Total Petroleum Hydrocarbons by GS/MS, DHS TPH Draft Procedure Purge and Trap, EPA Method 5030/8260 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan _ AELC Contact: John Arndt Job No. : 6409 Date Extracted: 03/19/92 COC Lo No. : 24918 - 24920 Date Analyzed: 03/19/92 AELC ID No. : L8465 Date Reported: 03/2S/92 Batch No. : 8944 Matrix: SOIL MATRIX SPIKE MS MS Conc. Recovery Analyte CAS No. (mg/kg) (percent) Gasoline N/A 2.0 99 MATRIX SPIKE DUPLICATE MSD MSD Conc. Recovery Analyte CAS No. (mg/kg) (percent) Gasoline N/A 2.0 101 RELATIVE % DIFFERENCE Relative Percent Difference Analyte CAS No. (percent) Gasoline N/A 2 d 3209 Fitgercld Road•Rancno Ccracva.CA 95:02•Fox X916)n38-4510-f916)638-7301 AMERICAN ENVIAONMEE IABICAlES CORP. CA DORS ELAP Aaareditatian)Registratian N=ber 1233 Analysis Report: Total Petroleum Hydrocarbons by GS/MS, DHS TPH Draft Procedure Purge and Trap, EPA Method 5030/8260 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Reported: 03/31/92 COCLo No. : 24918 - 24920 AELC ID No. : L8465 Batch No. : 8944 Matrix: SOIL LAB CONTROL STANDARD LCS LCS Conc. Recovery Analyte CAS No. (mg/L) (percent) Gasoline N/A 0.4 114 ,0 0 3249 Fitzgerald Road•Rancho Cordova.CA 95742•Fax(916)638-4510•(916)638-7301 • oMERICAORATORIES N ENVIRONMWCA DOGS ELAP Accreditation/Registration Number 1233 Analysis Report: Total Petroleum Hydrocarbons by GC/MS, DHS TPH Draft Procedure • Purge and Trap, EPA Method 5030/8260 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465 Date Extracted: 03/2C/92 Batch No. : 8945 Date Analyzed: 03/20/92 Matrix: SOIL Date Reported: 03/30/92 • ANALYTE Sample I.D. TPH as Gasoline Client AELC (mg/kg) BH3-5 21A ND • BH3-10 22A ND BH3-15 23A ND BH2-5 24A NO BH2-10 25A ND • BH2-15 26A NO BH1-5 27A ND BHI-10 28A ND BHI-15 29A ND r•. Rep. Limit 1.0 ND — Not detected at or above indicated Reportin Limit Rep. Limit — Reporting Limit unless otherwise in�icated in parentheses. • • • Q$ rnaEo wn+ 3249 Fitzgerald Road•Rancho Cordova,CA 95742•Fax(916)638-4510-(9161638-7301 • AMERICAN ENVIRONMENTAL LABORATORilES CORP. CA DOHS ELAP Accreditation/Registratlon Number 1233 Analysis Report: Total Petroleum Hydrocarbons by GC/MS, DHS TPH Draft Procedure 0 Purge and Trap, EPA Method 5030/8260 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt 0 Job No. : 6409 Date Extracted: 03/20/92 COC Lo No. : 24918 - 24920 Date Analyzed: 03/20/92 AELC ID No. : L8465 Date Reported: 03/30/92 Batch No. : 8945 Matrix: SOIL METHOD BLANK Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) TPH as Gasoline N/A ND 1.0 ND — Not detected at or above indicated ReportingLimit Rep. Limit — Reporting Limit unless otherwise inicated in parentheses . 9 Le . ..„>., 3249 Fitzgerald Road•Rancho Cordova.CA 95742•fax(Q16)638-4510•(9161638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. G DOHS FLAP Aaaredltatlan/Registration Number 1233 Analysis Report: Total Petroleum Hydrocarbons by GC/MS, DHS TPH Draft Procedure • Purge and Trap, EPA Method 5030/8260 Client: A$MC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Sola& - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Extracted: 03/20/92 COC Lo No. : 24918 - 24920 Date Analyzed: 03/20/92 AELC ID No. : L8465 Date Reported: 03/30/92 Batch No. : 8945 Matrix: SOIL • MATRIX SPIKE MS MS Conc. Recovery Analyte CAS No. (mg/kg) (percent) Gasoline N/A 2.0 106 :• MATRIX SPIKE DUPLICATE MSD MSD Cont. Recovery Analyte CAS No. (mg/kg) (percent) Gasoline N/A 2.0 99 • RELATIVE % DIFFERENCE Relative Percent Difference Analyte CAS ,No. (percent) '• Gasoline N/A 7 • • i • • 3249 Fitzgerald Road•Rancho Cordova.CA 95742•Fox N161 038-451 0•(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOHS ELAP Accreditation/Registration Number 1233 Analysis Report: Total Petroleum Hydrocarbons by GC/MS, DHS TPH Draft Procedure • Purge and Trap, EPA Method 5030/8260 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 • Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Reported: 03/30/92 COC Log No. : 24918 - 24920 AELC ID No. : L8465 Batch No. : 8945 Matrix: SOIL LAB CONTROL STANDARD • LCS LCS Conc. Recovery Analyte CAS No. (mg/L) (percent) Gasoline N/A 0.4 114 • • • a 32,19 Fitzgerald Road•Rancno Cordova,CA 957,12•�ox[9161638-4510• 916)o38-7301 AMERICAN ENVIRONMENTAL LA801ATORIES CORP. rA DOHS ELAP Accreditation/Reg iatrat ion Number 1233 Analysis Report: Total Petroleum Hydrocarbons, EPA Method 8015 Shaker, DOHS LUFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Sampled: 03/12/92 COC Lo No. : 24918 - 24920 Date Received: 03/13/92 AELC l� No. : L8465 Date Extracted: 03/17/92 Batch No. : 8927 Date Analyzed: 03/23/92 Matrix: SOIL Date Reported: 03/29/92 ANALYTE Sample I.D. TPH as Diesel Client AELC (mg/kg) BH10-5 lA ND BH10-10 2A ND BH9-5 4A ND BH9-10 5A ND BH9-15 6A ND BH8-5 7A ND Rep. Limit 10 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise inicated in parentheses. �$oencuvno 3249 Fikgerola Road•RanC09 Cordova,CA 95742•Fax(916)638-4510•(9161638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES COPD. CA DOHS ELAP ACCredltatlonlReglstratl.n Number 1233 • Analysis Report: Total Petroleum Hydrocarbons, EPA Method 8015 Shaker, DOHS LUFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Extracted: 03/17/92 COC Lo No. : 24918 - 24920 Date Analyzed: 03/23/92 AELC ID No. : L8465 Date Reported: 03/29/92 Batch No. : 8927 Matrix: SOIL • METHOD BLANK Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) TPH as Diesel N/A ND 10 ND — Not detected at or above indicated Reporting Limit • Rep. Limit Reporting Limit unless otherwise in in parentheses . • • 3249 Firgeraid Rood•Rdncno Cordova.CA 95742•=Cx(0161 038-4510•1916)638-7 301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOHS ELAP Accreditation/Registration N=ber 1233 Analysis Report: Total Petroleum Hydrocarbons, EPA Method 8015 • Shaker, DOHS LUFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Extracted: 03/17/92 COC Log No. : 24918 - 24920 Date Analyzed: 03/23/92 AELC ID No. : L8465 Date Reported: 03/29;x92 Batch No. : 8927 Matrix: SOIL MATRIX SPIKE • MS MS Conc. Recovery Analyte CAS No. (mg/kg) (percent) Diesel N/A 100 83 MATRIX SPIKE DUPLICATE MSD Analyte CAS No. MSD ( Conc. mg/kg) (percent) Diesel N/A 100 82 • RELATIVE % DIFFERENCE Relative Percent Difference Analyte CAS No. (percent) Diesel N/A 1 • • • 3°e n.•.,m o.nw 32d9 Fitzgerald Road•Rancnc Cordo c.CA 95742•Fax(9151 o38-4510•(916)o38-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. rA DONS ELAP Acrred1tat1on1Reg13trat Lan Number 1233 • Analysis Report: Total Petroleum Hydrocarbons, EPA Method 8015 Shaker, DOHS LUFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Reported: 03/29/92 COC Log No. : 24918 - 24920 AELC ID No. : L8465 Batch No. : 8927 Matrix: SOIL • LAB CONTROL STANDARD LCS LCS Conc. Recovery Analyte CAS No. (mg/L) (percent) Diesel N/A 1000 102 • • • • • • &u[na.. 3249 Fingeraid Road•Rancno Cordova.CA 95742•Fox R16)638-4.510-(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOES ELAP Accredltatlon/Reglstratlon Number 1233 • Analysis Report: Total Petroleum Hydrocarbons, EPA Method 8015 Shaker, DOHS LUFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 COC Lo No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465 Date Extracted: 03/17/92 Batch No. : 8928 Date Analyzed: 03/23/92 Matrix: SOIL Date Reported: 03/29/92 • ANALYTE Sample I.D. TPH as Diesel Client AELC (mg/kg) BH8-10 8A ND • BH8-15 9A ND BH7-5 10A ND BH7-10 11A ND BH6-5 12A ND • BH6-10 13A ND BH6-15 14A ND Rep. Limit 10 ND - Not detected at or above indicated ReportingLimit * Rep. Limit m Reporting Limit unless otherwise inicated in parentheses. a i 0 r 3249 Fitzgerald Road•Rarcno Cordova,CA 05742•Fax(016)038-4510•(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DONS ELAP Ac.red1taticn1HGgiatrat10n Number 1233 • Analysis Report: Total Petroleum Hydrocarbons, EPA Method 8015 Shaker, DOHS LUFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Extracted: 03/17/92 COC Lo No. : 24918 - 24920 Date Analyzed: 03/23/92 AELC ID No. : L8465 Date Reported: 03/29/92 Batch No. : 8928 Matrix: SOIL • METHOD BLANK Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) TPH as Diesel N/A ND 10 ND — Not detected at or above indicated Reporting Limit • Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • • • • • • Ain:,m+me 3249 Fitzgerald Road•Rancho Cordova,CA 95742-;ox(9161638-4510•(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOHS ELAP Accreditation/Registration N=ber 1233 Analysis Report: Total Petroleum Hydrocarbons, EPA Method 8015 Shaker, DOHS LUFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Extracted: 03/17/92 COC Log No. : 24918 - 24920 Date Analyzed: 03/23/92 AELC ID No. : L8465 Date Reported: 03/29/92 Batch No. : 8928 Matrix: SOIL • MATRIX SPIKE MS MS Conc. Recovery Analyte CAS No. (mg/kg) (percent) Diesel N/A 200 91 MATRIX SPIKE DUPLICATE MSD Analyte CAS No. MSD ( Conc. mg/kg) (percent) Diesel N/A 100 85 RELATIVE % DIFFERENCE Relative Percent Difference Analyte CAS No. (percent) • Diesel N/A 7 ,o„n 3249 Fingeroid Rood•Rancro Cereova.CA 95742•Fdx 016)638-4510•(9161638-7301 • AMERICAN ENVIRONMENTAL LA®ORATORIlS COR0. CA DOES ELAP AccraditationlRagiatration N=bar 1233 Analysis Report: Total Petroleum Hydrocarbons, EPA Method 8015 • Shaker, DOHS LUFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Reported: 03/29/92 COC Log No. : 24918 - 24920 AELC ID No. : L8465 Batch No. : 8928 Matrix: SOIL • LAB CONTROL STANDARD LCS LCS Conc. Recovery Analyte CAS No. (mg/L) (percent) Diesel N/A 1000 102 • • • • 3$ ,Ennvo rmn 3249 Filzgeral0 Road•Rancho Cordova,CA 95742•fax(916)638-4510•(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP CA DOHS ELAP Accred Ltation(Reglstration Number 1233 Analysis Report: Total Petroleum Hydrocarbons, EPA Method 8015 • Shaker, DOHS LOFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 • Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465 Date Extracted: 03/11/92 Batch No. : 8929 Date Analyzed: 03/23/92 Matrix: SOIL Date Reported: 03/29/92 • ANALYTE Sample I.D. TPH as Diesel Client AELC (mg/kg) BH5-5 15A ND BH5-10 16A NO BH5-15 17A ND BH4-5 18A ND BH4-10 19A ND • BH4-15 20A ND Rep. Limit 10 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • • • • • ca•!.[o awx 3249 Fingeraid Road•Rancho Cordova.CA 95742•Fax(916)638-4510•(916)638-7301 • AMERICAN AL CORR CA Does ELAP Accreditation/Registration N.ber 1233 Analysis Report: Total Petroleum Hydrocarbons, EPA Method 8015 • Shaker, DOHS LUFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Extracted: 03/17/92 COC Log No. : 24918 - 24920 Date Analyzed: 03/23/92 AELC ID No. : L8465 Date Reported: 03/29/92 Batch No. : 8929 Matrix: SOIL METHOD BLANK • Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) TPH as Diesel N/A NO 10 ND - Not detected at or above indicated ReportingLimit • Rep. Limit Reporting Limit unless otherwise inicated in parentheses. 49 ,• • • • • 3249 Fitzgerald Road•Raa ho Cordova.CA 95742•Fax(916)638-4510•(916)6384301 • AMERICAN ENVIRONMENTAL LA801ATORIEE CORP. to DOES SLAP Accreditation/Registration Number 1233 • Analysis Report: Total Petroleum Hydrocarbons, EPA Method 8015 Shaker, DOHS LUFT Method Client: ARMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Extracted: 03/17/92 COC Log No. : 24918 - 24920 Date Analyzed: 03/23/92 AELC ID No. : L8465 Date Reported: 03/29/92 Batch No. : 8929 Matrix: SOIL • MB SPIKE MBS MBS Conc. Recovery Analyte CAS No. (mg/kg) (percent) Diesel N/A 100 117 :• MB SPIKE DUPLICATE MBSD MBSD Conc. Recovery Analyte CAS No. (mg/kg) (percent) • Diesel N/A 100 117 MB SPIKE RPD MBS Relative Percent Difference Analyte CAS No. (percent) Diesel N/A 0 • • • 3249 Fitzgerald Road-Rancno Cordova.CA 95742•Fax(916)638-4510.1916)638-7301 AMERICAORATORIES N ENVIRONMECA DOES ELAP Accreditation/Registration Number 1233 Analysis Report: Total Petroleum Hydrocarbons, EPA Method 8015 • Shaker, DOHS LUFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 • Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Reported: 03/29/92 COC Log No. : 24918 - 24920 AELC ID No. : L8465 Batch No. : 8929 Matrix: SOIL LAB CONTROL STANDARD • LCS LCS Conc. Recovery Analyte CAS No. (mg/L) (percent) Diesel N/A 1000 111 • • • • • • • J$ 3249 Fitzgerald Road•Roncho Cordova.CA 95742•;cx(9161636-4510•(916)638-7301 • AMERICAN ENVIRONMENTAL LA901ATORIES CORR CA DOES ELAP Accreditation/Reglatratlon Number 1233 Analysis Report: Total Petroleum Hydrocarbons, EPA Method 8015 0 Shaker, DOHS LUFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt 0 Job No. : 6409 Date Sampled: 03/12/92 COC Lo No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465 Date Extracted: 03/17/92 Batch No. : 8930 Date Analyzed: 03/23/92 Matrix: SOIL Date Reported: 03/29/92 ANALYTE Sample I.D. TPH as Diesel Client AELC (mg/kg) BH3-10 22A ND BH3-15 23A ND BH2-5 24A ND BH2-10 25A ND BH2-15 26A ND • BHI-5 27A ND BH1-10 28A ND BH1-15 29A ND Rep. Limit 10 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. 0 0 atonmrwn 3249 Fitzgerald Road•Roncho Cordova.CA 95742•Fax(916)638-4510.[916)638-7301 • AMERICAN ENVIRONMENTAL LAEORATORfES CORP. CA DOHS ELAP Aerredltation/Registration Number 1233 Analysis Report: Total Petroleum Hydrocarbons, EPA Method 8015 • Shaker, DOHS LUFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 • Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Extracted: 03/17/92 COC Log No. : 24918 - 24920 Date Analyzed: 03/23/92 AELC ID No. : L8465 Date Reported: 03/29/92 Batch No. : 8930 Matrix: SOIL METHOD BLANK • Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) TPH as Diesel N/A ND 10 ND = Not detected at or above indicated Reporting Limit Rep. Limit Reporting Limit unless otherwise indicated in parentheses . • • • • • • 4 nrnnw..n+ 3249 Fingerado Road•Ran ho Cordma.CA 95742•Fax(916)6380.510•(916)638-7301 • AMERICAN ENV RONMiNTAL LABORATORIES CORP. CA DOSS ELAP ACQred1t.t106)REg1]Lr.t10n Number 1233 Analysis Report: Total Petroleum Hydrocarbons, EPA Method 8015 • Shaker, DOHS LUFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Ray Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 + Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Extracted: 03/17/92 COC Lo No. : 24918 - 24920 Date Analyzed: 03/23/92 AELC I No. : L8465 Date Reported: 03/29/92 Batch No. : 8930 Matrix: SOIL MB SPIKE • MBS MBS Conc. Recovery Analyte CAS No. (mg/kg) (percent) Diesel N/A 100 117 • MB SPIKE DUPLICATE MBSD MBSD Conc. Recovery Analyte CAS No. (mg/kg) (percent) Diesel N/A 100 118 • MB SPIKE RPD MBS Relative Percent Difference Analyte CAS No. (percent) • Diesel N/A 1 • • • • 3249 Fitzgerald Road•RanchO Cordova.CA 95742•Foz(916)638-4510•(9161638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES COR0. CA DOES ELAP AccredLtation/Registration Number 1233 Analysis Report: Total Petroleum Hydrocarbons, EPA Method 8015 • Shaker, DOHS LUFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Reported: 03/29/92 COC Log No. : 24918 - 24920 AELC ID No. : L8465 Batch No. : 8930 Matrix: SOIL LAB CONTROL STANDARD • LCS LCS Conc. Recovery Analyte CAS No. (mg/L) (percent) Diesel N/A 1000 111 • • • • • • • nenaunrrw. 3249 Fitzgerald Rood•Par ho COrdO Q.CA 95742•for(916)638-4510•(916)638-7301 • AMERICAN ENVIRONMENTAL LAGORATORIES CORP. CA DOHS ELAP Accred Ltation/Regiatrat Lon Number 1233 Analysis Report: CAM Metals, TTLC, EPA Methods 6010/7000 • Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 CDC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : 1.8465-1A Date Digested: 03/18/92 Batch No. : 53688 Date Analyzed: 03/19/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH10-5 • Sample: BH10-5 Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) Method Ag (Silver) 7440-22-4 ND 2.5 6010 1 As (Arsenic) 7440-38-2 6.3 0.50 7060 Ba (Barium) 7440-39-3 63 5 .0 6010 Be (Beryllium) 7440-41-7ND 0.50 6010 Cd (Cadmium) 7440-43-9 ND 0. 50 6010 • Cr (Chromium) 7440-47-3 12 5 .0 6010 Co (Cobalt) 7440-48-4 6 .8 5 .0 6010 Cu (Copper) 7440-50-8 16 5 .0 6010. Hg (Mercury) 7439-97-6 ND 0.050 7471 • Mo (Molybdenum) 7439-98-7 ND 5 .0 6010 Ni (Nickel) 7440-02-0 11 5.0 6010 Pb (Lead) 7439-92-1 20 5.0 6010 Sb (Antimony) 7440-36-0 ND 25 6010 • Se (Selenium) 7783-00-8 ND 0.50 7740 Tl (Thallium) 7440-28-0 ND 25 6010 V (Vanadium) 7440-62-2 27 5.0 6010 Zn (Zinc) 7440-66-6 47 5.0 6010 ND — Not detected at or above indicated Reporting Limit • Rep. Limit y Reporting Limit unless otherwise indicated in parentheses . • ,nnm ana 3249 Fifzgeraio Road•Rancho Coroova,CA 95742•=ax X9161 638-4510-19161638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOHS ELAP Accreditation/Regietrat Lon Number 1233 • Analysis Report: CAM Metals, TTLC, EPA Methods 6010/7000 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-4A Date Digested: 03/18/92 Batch No. : 53688 Date Analyzed: 03/19/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH9-5 • Sample: BH9-5 Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) Method Ag (Silver) 7440-22-4 ND 2.5 6010 • As (Arsenic) 7440-38-2 2.5 0.50 7060 Ba (Barium) 7440-39-3 16 5.0 6010 Be (Beryllium) 7440-41-7 ND 0.50 6010 Cd (Cadmium) 7440-43-9 ND 0. 50 6010 • Cr (Chromium) 7440-47-3 ND 5.0 6010 Cc (Cobalt) 7440-48-4 ND 5.0 6010 Cu (Copper) 7440-50-8 9 .9 5.0 6010 Hg (Mercury) 7439-97-6 ND 0.050 7471 • Mo (Molybdenum) 7439-98-7 ND 5.0 6010 Ni (Nickel) 7440-02-0 6.2 5.0 6010 Pb (Lead) 7439-92-1 7. 3 5.0 6010 Sb (Antimony) 7440-36-0 ND 25 6010 • Se (Selenium) 7783-00-8 ND 0.50 7740 Tl (Thallium) 7440-28-0 ND 25 6010 V (Vanadium) 7440-62-2 8.0 5.0 6010 Zn (Zinc) 7440-66-6 32 5.0 6010 ND - Not detected at or above indicated ReportingLimit • Rep. Limit - Reporting Limit unless otherwise inicated in parentheses. • • 4d u,nntonna 3249 Fingeraio Roca•Rancho Cordovc.CA 95742•Fax t916)638--Z10-(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOHS ELAP Ateredltation/ReBlntrat Lon N=ber 1233 • Analysis Report: CAM Metals, TTLC, EPA Methods 6010/7000 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-7A Date Digested: 03/18/92 Batch No. : 53688 Date Analyzed: 03/19/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH8-5 • Sample: BHS-5 Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) Method Ag (Silver) 7440-22-4 ND 2.5 6010 As (Arsenic) 7440-38-2 1.8 0.50 7060 Ba (Barium) 7440-39-3 27 5 .0 6010 Be (Beryllium) 7440-41-7 ND 0.50 6010 Cd (Cadmium) 7440-43-9 ND 0.50 6010 Cr (Chromium) 7440-47-3 6.2 5 .0 6010 Co (Cobalt) 7440-48-4 ND 5.0 6010 Cu (Copper) 7440-50-8 ' 17 5.0 6010 Hg (Mercury) 7439-97-6 ND 0.050 7471 Mo (Molybdenum) 7439-98-7 ND 5 .0 6010 Ni (Nickel) 7440-02-0 6.9 5.0 6010 Pb (Lead) 7439-92-1 11 5.0 6010 Sb (Antimony) 7440-36-0 ND 25 6010 + Se (Selenium) 7783-00-8 ND 0.50 7740 T1 (Thallium) 7440-28-0 NO 25 6010 V (Vanadium) 7440-62-2 15 5.0 6010 Zn (Zinc) 7440-66-6 30 5.0 6010 i ND - Not detected at or above indicated ReportingLimit Rep. Limit - Reporting Limit unless otherwise inicated in parentheses . 3249 Fingerald Raad•Rondho Cordova.CA 95742•;ax 1916;638-45510•(V61638-730f • /o►MEt�1�/4N ENVIRONMHE IABOgATOFilES COFP. CA DOHS FLAP Accred1tat1on1Reg1atrat1on N.ber 1233 • Analysis Report: CAM Metals, TTLC, EPA Methods 6010/7000 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Lo No. : 24918 - 24920 Date Received: 03/13/92 AELC ZD No. : L8465-10A Date Digested: 03/18/92 Batch No. : 53688 Date Analyzed: 03/19!92 Matrix: SOIL Date Reported: 03//29/92 Client ID No. : BH7-5 • Sample: BH7-5 Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) Method Ag (Silver) 7440-22-4 ND 2.5 6010 • As (Arsenic) 7440-38-2 1.1 0. 50 7060 Ba (Barium) 7440-39-3 41 5 .0 6010 Be (Beryllium) 7440-41-7 ND 0.50 6010 Cd (Cadmium) 7440-43-9 ND 0.50 6010 • Cr (Chromium) 7440-47-3 7.1 5 .0 6010 Co (Cobalt) 7440-48-4 ND 5.0 6010 Cu (Copper) 7440-50-8 19 5.0 6010 Hg (Mercury) 7439-97-6 ND 0.050 7471 Mo (Molybdenum) 7439-98-7 ND 5 .0 6010 Ni (Nickel) 7440-02-0 7 .8 5.0 - 6010 Pb (Lead) 7439-92-1 19 5.0 6010 Sb (Antimony) 7440-36-0 NO 25 6010 • Se (Selenium) 7783-00-8 ND 0.50 7740 Tl (Thallium) 7440-28-0 ND 25 6010 V (Vanadium) 7440-62-2 15 5.0 6010 Zn (Zinc) 7440-66-6 38 5.0 6010 NO — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • • i» onnm o•vc 32d9 Fitzgerald Road•Rancno COrdOVO.CA 95742•Fax(Q161638-4510-(916)638-7301 • AMERICAN ONMEN LABR CORP. CA DONS SLAP Accreditation!Registration Number 1233 • Analysis Report: CAM Metals, TTLC, EPA Methods 6010/7000 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Lo No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-12A Date Digested: 03/18/92 Batch No. : 53688 Date Analyzed: 03/10/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH6-5 • Sample: BH6-5 Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) Method Ag (Silver) 7440-22-4 ND 2.5 6010 • As (Arsenic) 7440-38-2 2. 1 0.50 7060 Ba (Barium) 7440-39-3 22 5 .0 6010 Be (Beryllium) 7440-41-7 ND 0. 50 6010 Cd (Cadmium) 7440-43-9 ND 0.50 6010 • Cr (Chromium) 7440-47-3 ND 5.0 6010 Co (Cobalt) 7440-48-4 ND 5 .0 6010 Cu (Copper) 7440-50-8 11 5.0 6010 Hg (Mercury) 7439-97-6 ND 0.050 7471 Mo (Molybdenum) 7439-98-7 ND 5 .0 6010 Ni (Nickel) 7440-02-0 7.2 5.0 6010 Pb (Lead) 7439-92-1 7.9 5.0 6010 Sb (Antimony) 7440-36-0 ND 25 6010 • Se (Selenium) 7783-00-8 ND 0.50 7740 T1 (Thallium) 7440-28-0 ND 25 6010 V (Vanadium) 7440-62-2 14 5.0 6010 Zn (Zinc) 7440-66-6 29 5.0 6010 • ND a Not detected at or above indicated Reporting Limit Rep. Limit a Reporting Limit unless otherwise indicated in parentheses. • • ,r.,,Eu r•+x 3249 Firzgerdd Rood•Rancho Cofdovc.CA 95742•Fox 1916)638-4510•(9161638-7301 • AMERICAN ENVIRONMENTAL LA60RATORIES CORP. CA DONS ELAP Aoered1tat1on1Reg1.trat1on Number 1233 • Analysis Report: CAM Metals, TTLC, EPA Methods 6010/7000 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 CDC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-15A Date Digested: 03/18/92 Batch No. : 53688 Date Analyzed: 03/19/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH5-5 • Sample: BH5-5 Results Rep, Limit Analyte CAS No. (mg/kg) (mg/kg) Method Ag (Silver) 7440-22-4 ND 2. 5 6010 • As (Arsenic) 7440-38-2 1. 8 0.50 7060 Ba (Barium) 7440-39-3 21 5.0 6010 Be (Beryllium) 7440-41-7 NO 0.50 6010 Cd (Cadmium) 7440-43-9 ND 0.50 6010 • Cr (Chromium) 7440-47-3 ND S .0 6010 Co (Cobalt) 7440-48-4 ND 5.0 6010 Cu (Copper) 7440-50-8 18 5.0 6010 Hg (Mercury) 7439-97-6 ND 0.050 7471 Mo (Molybdenum) 7439-98-7 ND 5.0 6010 Ni (Nickel) 7440-02-0 7.7 5.0 6010 Pb (Lead) 7439-92-1 10 5 .0 6010 Sb (Antimony) 7440-36-0 ND 25 6010 • Se (Selenium) 7783-00-8 ND 0.50 7740 Tl (Thallium) 7440-28-0 ND 25 6010 V (Vanadium) 7440-62-2 12 5.0 6010 Zn (Zinc) 7440-66-6 29 5.0 6010 • ND - Not detected at or above indicated Reporting Limit Rep. Limit - Reporting Limit unless otherwise indicated in parentheses. • • 3249 Fi2gercic Road•Roncho CordOVd,CA 95742•Fcx 916)638-4510•(916)638.7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOHS ELAP Aeeteditation/Registration Number 1233 • Analysis Report: CAM Metals, TTLC, EPA Methods 6010/7000 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-ISA Date Digested: 03/18/92 Batch No. : 53688 Date Analyzed: 03/19/92 Matrix: SOIL Date Repported: 03/29/92 Client ID No. : BH4-5 • Sample: BH4-5 Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) Method Ag (Silver) 7440-22-4 ND 2.5 6010 • As (Arsenic) 7440-38-2 1.0 0.50 7060 Ba (Barium) 7440-39-3 17 5.0 6010 Be (Beryllium) 7440-41-7 ND 0.50 6010 Cd (Cadmium) 7440-43-9 ND 0.50 6010 Cr (Chromium) 7440-47-3 ND 5.0 6010 Co (Cobalt) 7440-48-4 ND 5 .0 6010 Cu (Copper) 7440-50-8 8.7 5.0 6010 Hg (Mercury) 7439-97-6 ND 0.050 7471 • Mo (Molybdenum) 7439-98-7 ND 5.0 6010 Ni (Nickel)' 7440-02-0 5.4 5.0 6010 Pb (Lead) 7439-92-1 7.4 5.0 6010 Sb (Antimony) 7440-36-0 ND 25 6010 • Se (Selenium) 7783-00-8 ND 0.50 7740 T1 (Thallium) 7440-28-0 ND 25 6010 V (Vanadium) 7440-62-2 8.2 5.0 6010 Zn (Zinc) 7440-66-6 27 5 .0 6010 ND - Not detected at or above indicated Reporting Limit Rep. Limit - Reporting Limit unless otherwise indicated in parentheses. R • • +vmito v.nx 3249 Fitzgerald Road•RoMho Cordow.CA 95742•Fox(916)638-4510•(916)6387301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOHS ELAP Aetreditat Lon/Registration Number 1233 Analysis Report: CAM Metals, TTLC, EPA Methods 6010/7000 • Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ZD No. : L8465-21A Date Digested: 03/18/92 Batch No. : 53688 Date Analyzed: 03/19/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH3-5 • Sample: BH3-5 Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) Method Ag (Silver) 7440-22-4 ND 2.5 6010 • As (Arsenic) 7440-38-2 1.4 0.50 7060 Ba (Barium) 7440-39-3 14 5.0 6010 Be (Beryllium) 7440-41-7 ND 0.50 6010 Cd (Cadmium) 7440-43-9 ND 0. 50 6010 Cr (Chromium) 7440-47-3 ND 5.0 6.010 Co (Cobalt) 7440-48-4 ND 5.0 6010 Cu (Copper) 7440-50-8 13 5,0 6010 Hg (Mercury) 7439-97-6 ND 0.050 7471 '• Mo (Molybdenum) 7439-98-7 ND 5.0 6010 Ni (Nickel) 7440-02-0 6.2 5.0 6010 Pb (Lead) 7439-92-1 7.2 5.0 6010 Sb (Antimony) 7440-36-0 ND 25 6010 Se (Selenium) 7783-00-8 ND 0.50 7740 T1 (Thallium) 7440-28-0 ND 25 6010 V (Vanadium) 7440-62-2 9.8 5.0 6010 Zn (Zinc) 7440-66-6 28 5.0 6010 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. 3244 fiRgeraid Road•Rancno Cordova.CA 95742•%Cx(016)638 4510•19161638.7301 • AMERICAN ENVIRONMENTAL LABORATORIES COgP. CA 0085 FLAP Accreditatlon/Registration Number 1233 • Analysis Report: CAM Metals, TTLC, EPA Methods 6010/7000 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Lo No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-24A Date Digested: 03/18/92 Batch No. : 53688 Date Analyzed: 03/19/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH2-5 • Sample: BH2-5 Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) Method Ag (Silver) 7440-22-4 ND 2.5 6010 • As (Arsenic) 7440-38-2 2.5 0.50 7060 Ba (Barium) 7440-39-3 25 5.0 6010 Be (Beryllium) 7440-41-7 ND 0.50 6010 Cd (Cadmium) 7440-43-9 ND 0.50 6010 • Cr (Chromium) 7440-47-3 6. 1 5.0 6010 Co (Cobalt) 7440-48-4 ND 5.0 6010 Cu (Copper) 7440-50-8 14 5 .0 6010 Hg (Mercury) 7439-97-6 ND 0.050 7471 Mo (Molybdenum) 7439-98-7 ND 5.0 6010 Ni (Nickel) 7440-02-0 6.6 5.0 6010 Pb (Lead) 7439-92-1 12 5.0 6010 Sb (Antimony) 7440-36-0 ND 25 6010 • Se (Selenium) 7783-00-8 ND 0.50 7740 T1 (Thallium) 7440-28-0 ND 25 6010 V (Vanadium) 7440-62-2 15 5.0 6010 Zn (Zinc) 7440-66-6 30 5 .0 6010 +� ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • 3249 Fitzgerald Road•Rancho CafCOva CA 95742•°ox 19161 638-4510•R16 638-7301 • AMERICAN ENVIRONMENTAL LA®ORATORIE9 CORM to DOES ELAP Aecredltation/Reglstratton Number 1233 Analysis Report: CAM Metals, TTLC, EPA Methods 6010/7000 • Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-27A Date Digested: 03/18/92 Batch No. : 53688 Date Analyzed: 03/19/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BHI-5 • Sample: BH1-5 Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) Method Ag (Silver) 7440-22-4 ND 2.5 6010 '• As (Arsenic) 7440-38-2 5.5 0.50 7060 BE (Barium) 7440-39-3 43 5.0 6010 Be (Beryllium) 7440-41-7 ND 0.50 6010 Cd (Cadmium) 7440-43-9 ND 0.50 6010 • Cr (Chromium) 7440-47-3 10 5 .0 6010 Co (Cobalt) 7440-48-4 ND 5.0 6010 Cu (Copper) 7440-50-8 11 5.0 6010 Hg (Mercury) 7439-97-6 ND 0.050 7471 '• Mo (Molybdenum) 7439-98-7 ND 5.0 6010 Ni (Nickel) 7440-02-0 7.0 5.0 6010 Pb (Lead) 7439-92-1 17 5.0 6010 Sb (Antimony) 7440-36-0 ND 25 6010 • Se (Selenium) 7783-00-8 ND 0.50 7740 T1 (Thallium) 7440-28-0 ND 25 6010 V (Vanadium) 7440-62-2 20 5.0 6010 Zn (Zinc) 7440-66-6 34 5.0 6010 ' ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • • 4 erraitu nx« 3249 Ftgerota Rood•Rarcho CO dOa 0.CA 95742•Fox 016)638-4510-(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORM CA DOHS ELAP Accred Ltation/Reglstration N=ber 1233 Analysis Report: CAM Metals, TTLC, EPA Methods 6010/7000 • Client: AEMC Boatman Project No. : 6409 10960 Boatman Wap Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Digested: 03/18/92 COC Log No. : 24918 - 24920 Date Analyzed: 03/19/92 AELC ID No. : L8465 Date Reported: 03/29/92 Batch No. : 53688 Matrix: SOIL METHOD BLANK • Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) Method Ag (Silver) 7440-22-4 ND 2. 5 6010 As (Arsenic) 7440-38-2 ND 0. 50 7060 Ba (Barium) 7440-39-3 ND 5.0 6010 Be (Beryllium) 7440-41-7 ND 0.50 6010 Cd (Cadmium) 7440-43-9 ND 0.50 6010 Cr (Chromium) 7440-47-3 ND 5.0 6010 • Co (Cobalt) 7440-48-4 ND 5.0 6010 Cu (Copper) 7440-50-8 ND 5.0 6010 Hg (Mercury) 7439-97-6 ND 0.050 7471 Mo (Molybdenum) 7439-98-7 ND 5 .0 6010 Ni (Nickel) 7440-02-0 ND 5 .0 6010 Pb (Lead) 7439-92-1 ND 5.0 6010 Sb (Antimony) 7440-36-0 ND 25 6010 Se (Selenium) 7783-00-8 ND 0.50 7740 • T1 (Thallium) 7440-28-0 ND 25 6010 V (Vanadium) 7440-62-2 ND 5.0 6010 Zn (Zinc) 7440-66-6 ND 5.0 6010 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • • • 3249 Fitzgeralo Road•RanCho COIOOVO.CA 95742•Fax(916)638-4510•X9161 638.7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA D085 ELAP Ateredltatlon/Reglstration N=ber 1233 • Analysis Report: CAM Metals, TTLC, EPA Methods 6010/7000 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Reported: 03/29/92 COC Lo No. : 24918 - 24920 AELC ID No. : L8465 Batch No. : 53688 Matrix: SOIL LAB CONTROL STANDARD • LCS LCS Cone. Recovery Analyte CAS No. (mg/L) (percent) Ag (Silver) 7440-22-4 0.50 104 As (Arsenic) 7440-38-2 0.050 100 Ba (Barium) 7440-39-3 0.50 97 Be (Beryllium) 7440-41-7 0.50 101 Cd (Cadmium) 7440-43-9 0.50 102 Cr (Chromium) 7440-47-3 0.50 97 Co (Cobalt) 7440-48-4 0.50 107 Cu (Copper) 7440-50-8 0.50 96 Hg (Mercury) 7439-97-6 0.010 99 Mo (Molybdenum) 7439-98-7 0.50 95 Ni (Nickel) 7440-02-0 0.50 106 Pb (Lead) 7439-92-1 0.50 116 Sb (Antimony) 7440-36-0 0.50 89 Se (Selenium) 7783-00-8 0.050 98 • T1 (Thallium) 7440-28-0 0.50 99 V (Vanadium) 7440-62-2 0.50 90 Zn (Zinc) 7440-66-6 0.50 89 • P • • 3249 Fitzgerald Road•Rancno Cordova.CA 95742•Fax(Q161036-1510-(9161638-7301 • AMERICAN ENVIRONMENTAL V.BORATOii1E5 CO[iP. CA DOHS ELAP Accredltatlon/Reglatratlon Number 1233 • Analysis Report: CAM Metals, TTLC, EPA Methods 6010/7000 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Digested: 03/18/92 COC Log No. : 24918 - 24920 Date Analyzed: 03/19/92 AELC ID No. : L8465 Date Reported: 03/29/92 Batch No. : 53688 Matrix: SOIL MATRIX SPIKE • MS MS Conc. Recovery Analyte CAS No. (mg/kg) (percent) Ag (Silver) 7440-22-4 25 76 As (Arsenic) 7440-38-2 2.5 BE • Ba (Barium) 7440-39-3 25 61 Be (Beryllium) 7440-41-7 25 103 Cd (Cadmium) 7440-43-9 25 100 Cr (Chromium) 7440-47-3 25 88 Co (Cobalt) 7440-48-4 25 98 Cu (Copper) 7440-50-8 25 116 Hg (Mercury) 7439-97-6 0.50 101 Mo (Molybdenum) 7439-98-7 25 93 • Ni (Nickel) 7440-02-0 25 94 Pb (Lead) 7439-92-1 25 79 Sb (Antimony) 7440-36-0 25 93 Se (Selenium) 7783-00-8 2.5 MI • T1 (Thallium) 7440-28-0 25 MI V (Vanadium) 7440-62-2 25 67 Zn (Zinc) 7440-66-6 25 84 BE — Matrix spike recovery data can not be produced because background level exceeds matrix spike concentration. MI ® Matrix spike recovery data can not be generated due to matrix interference. • • wn.,,m a•.•a 3249 FiRgeralo Road•Rancho Cord0VC.CA 95742•%ex(916)638-4510•(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DONS ELAP Accreditation/Registration Number 1233 • Analysis Report: CAM Metals, TTLC, EPA Methods 6010/7000 Client: AEMC Boatman Project No. : 6409 10960 Boatman Wap Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Digested: 03/18/92 COC Log No. : 24918 - 24920 Date Analyzed: 03/19/92 AELC ZD No. : L8465 Date Reported: 03/29/92 Batch No. : 53688 Matrix: SOIL MATRIX SPIKE DUPLICATE • MSD MSD Conc. Recovery Analyte CAS No. (mg/kg) (percent) Ag (Silver) 7440-22-4 25 76 As (Arsenic) 7440-38-2 2.5 BE • Ba (Barium) 7440-39-3 25 64 Be (Beryllium) 7440-41-7 25 102 Cd (Cadmium) 7440-43-9 25 100 Cr (Chromium) 7440-47-3 25 98 • Co (Cobalt) 7440-48-4 25 98 Cu (Copper) 7440-50-8 . 25 97 Hg (Mercury) 7439-97-6 0.50 102 Mo (Molybdenum) 7439-98-7 25 99 3• . Ni (Nickel) 7440-02-0 25 98 Pb (Lead) 7439-92-1 25 84 Sb (Antimony) 7440-36-0 25 104 Se (Selenium) 7783-00-8 2.5 MI • T1 (Thallium) 7440-28-0 25 MI V (Vanadium) 7440-62-2 25 74 Zn (Zinc) 7440-66-6 25 76 BE — Matrix spike recovery data can not be produced because background • level exceeds matrix spike concentration. MI — Matrix spike recovery data can not be generated due to matrix interference. • • ?$xri.ri=orwa 3249Fitzgerald Roaa•Rancho Cordo .CA 95742•Pax(916)638-1510•(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOHS ELAP Accreditation/Registration Number 1233 • Analysis Report: CAM Metals, TTLC, EPA Methods 6010/7000 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Digested: 03/18/92 COC Log No. : 24918 - 24920 Date Analyzed: 03/19/92 AELC ID No. : L8465 Date Reported: 03/29/92 Batch No. : 53688 Matrix: SOIL RELATIVE $ DIFFERENCE • Relative Percent Difference Analyte CAS No. (percent) Ag (Silver) 7440-22-4 0 • As (Arsenic) 7440-38-2 BE Ba (Barium) 7440-39-3 5 Be (Beryllium) 7440-41-7 1 Cd (Cadmium) 7440-43-9 0 • Cr (Chromium) 7440-47-3 11 Co (Cobalt) 7440-48-4 0 Cu (Copper) 7440-50-8 18 Hg (Mercury) 7439-97-6 1 • Mo (Molybdenum) 7439-98-7 6 Ni (Nickel) 7440-02-0 4 Pb (Lead) 7439-92-1 6 Sb (Antimony) 7440-36-0 11 • Se (Selenium) 7783-00-8 MI T1 (Thallium) 7440-28-0 MI V (Vanadium) 7440-62-2 10 Zn (Zinc) 7440-66-6 10 • BE — Matrix spike recovery data can not be produced because background level exceeds matrix spike concentration. MI — Matrix spike recovery data can not be generated due to matrix interference. • • FS n[onm nwx 3249 Fitzgerald Road•Ran ho Cordova.CA 95742•Fax(916)638-4510•(916)638-7301 • AMERICAN ENVIRONMEE LABORATORIES CORP. CA DOES ELAP Accreditation/Regiatrat ion 11=ber 1233 Analysis Report: Polychlorinated Biphenyls, EPA Method 8080 • Shaker, DOHS LOFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-1A Date Extracted: 03/17/92 Batch No. : 8926 Date Analyzed: 03/17/92 Matrix: SOIL Date Reported: 03/20/92 Client ID No. : BH10- • Sample: BH10-5 Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) Aroclor 1016 12674-11-2 ND 1.0 + Aroclor 1221 1104-28-2 ND 1.0 Aroclor 1232 11141-16-5 ND 1.0 Aroclor 1242 53469-21-9 ND 1.0 Aroclor 1248 12672-29-6 ND 1.0 • Aroclor 1254 11097-69-1 ND 1.0 Aroclor 1260 11096-82-5 ND 1.0 ND - Not detected at or above indicated Reporting Limit Rep. Limit - Reporting Limit unless otherwise indicated in parentheses. • • • • 32w Fh_aeraltl Roca•4oncnc�saova.Cq c57.1'.•=a. = .. =6 i J• 4161038 • AMERICAN I . CA DONS ELAP Accreditation/Registration Number 1233 • Analysis Report: Polychlorinated Biphenyls, EPA Method 8080 Shaker, DOHS LUFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 • Project: Solag - San Juan AELC Contact: 640No. 9 JohArndt Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-4A Date Extracted: 03/17,92 Batch No. : 8926 Date Analyzed: 03/17/92 Matrix: SOIL Date Reported: 03/20/92 Client ID No. : BH9-5 • Sample: BH9-5 Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) • Aroclor 1016 12674-11-2 ND 1.0 Aroclor 1221 1104-28-2 ND 1.0 Aroclor 1232 11141-16-5 ND 1.0 Aroclor 1242 53469-21-9 ND 1.0 • Aroclor 1248 12672-29-6 ND 1.0 Aroclor 1254 11097-69-1 ND 1.0 Aroclor 1260 11096-82-5 ND 1.0 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • • • 3249:-7,efo "zc.:•'i! -Cc oC✓ao.c C�:j],t_•_; .. _ __,., 'JI • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOHS ELAP Accredlcacian/Registration Number 1233 Analysis Report: Polychlorinated Biphenyls, EPA Method 8080 • Shaker, DOHS LUFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Waq Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 • Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-7A Date Extracted: 03/17/92 Batch No. : 8926 Date Analyzed: 03/17/92 Matrix: SOIL Date Reported: 03/20/92 Client ID No. : BH8-5 • Sample: BHS-5 Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) Aroclor 1016 12674-11-2 ND 1.0 Aroclor 1221 1104-28-2 ND 1.0 Aroclor 1232 11141-16-5 ND 1.0 Aroclor 1242 53469-21-9 ND 1.0 Aroclor 1248 12672-29-6 ND 1.0 • Aroclor 1254 11097-69-1 NO 1.0 Aroclor 1260 11096-82-5 NO 1.0 ND - Not detected at or above indicated ReportingLimit Rep. Limit - Reporting Limit unless otherwise inicated in parentheses. • • • • • AMEONMENTALRICANCORP CA DORS ELAP Accredltatlon(Re$13tratlon H=her 1233 Analysis Report: Polychlorinated Biphenyls, EPA Method 8080 Shaker, DOHS LUFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 . Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-1OA Date Extracted: 03/17/92 Batch No. : 8926 Date Analyzed: 03/17/92 Matrix: SOIL Date Reported: 03/20/92 Client ID NO. : BH7-5 • Sample: BH7-5 Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) Aroclor 1016 12674-11-2 ND 1.0 Aroclor 1221 1104-28-2 ND 1.0 Aroclor 1232 11141-16-5 ND 1.0 Aroclor 1242 53469-21-9 ND 1.0 • Aroclor 1248 12672-29-6 ND 1.0 Aroclor 1254 11097-69-1 ND 1.0 Aroclor 1260 11096-82-5 ND 1.0 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. r • 14,O1/IEF�ICAN ENVIRONMEE LA60HATpR1E5 COI�P. CA DOHS ELAP Accred Station/Registration Hu bar 1233 Analysis Report: Polychlorinated Biphenyls, EPA Method 8080 • Shaker, DOHS LUFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Aa Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-12A Date Extracted: 03/17/92 Batch No. : 8926 Date Analyzed: 03/17/92 Matrix: SOIL Date Reported: 03/20/92 Client ID No. : BH6-5 • Sample: BH6-5 Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) Aroclor 1016 12674-11-2 ND 1.0 • Aroclor 1221 1104-28-2 ND 1 .0 Aroclor 1232 11141-16-5 ND 1.0 Aroclor 1242 53469-21-9 ND 1.0 Aroclor 1248 12672-29-6 ND 1.0 • Aroclor 1254 11097-69-1 ND 1 .0 Aroclor 1260 11096-82-5 ND 1.0 ND — Not detected at or above indicated Reportin Limit Rep. Limit — Reporting Limit unless otherwise in�icated in parentheses. • f 3249=^cep%. .-cca• ,:r.- ..,... �_ -r _33 '30' • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOHS ELAF Accreditat Lon/Reg Lstration Number 1233 Analysis Report: Polychlorinated Biphenyls, EPA Method 8080 • Shaker, DOHS LUFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-15A Date Extracted: 03/17/92 Batch No. : 8926 Date Analyzed: 03/17/92 Matrix: SOIL Date Reported: 03/20/92 Client ID No. : BH -5 • Sample: BH5-5 Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) Aroclor 1016 12674-11-2 ND 1.0 Aroclor 1221 1104-28-2 ND 1.0 Aroclor 1232 11141-16-5 ND 1.0 Aroclor 1242 53469-21-9 ND 1.0 Aroclor 1248 12672-29-6 ND 1.0 • Aroclor 1254 11097-69-1 ND 1.0 Aroclor 1260 11096-82-5 ND 1.0 ND - Not detected at or above indicated Reporting Limit Rep. Limit - Reporting Limit unless otherwise indicated in parentheses. • • 3 • • i].1�=tz�era,y Raa•c.:^c^c�avn.. .- _%.I�•--c Atal n.9-'c I]•,- r.:b='0, • l�N1ERlCe�N ENVI4iONMEE LABOgATOR1E5 CORP. CA DOHS SLAP Accreditation/Registration Number 1233 • Analysis Report: Polychlorinated Biphenyls, EPA Method 8080 Shaker, DOHS LOFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Aa Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-18A Date Extracted: 03/17/92 Batch No. : 8926 Date Analyzed: 03/17/92 Matrix: SOIL Date Reported., 03/20/92 Client ID No. : BH4-5 • Sample: BH4-5 Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) • Aroclor 1016 12674-11-2 ND 1.0 Aroclor 1221 1104-28-2 ND 1.0 Aroclor 1232 11141-16-5 ND 1.0 Aroclor 1242 53469-21-9 ND 1.0 Aroclor 1248 12672-29-6 ND 1.0 • Aroclor 1254 11097-69-1 ND 1.0 Aroclor 1260 11096-82-5 ND 1.0 ND s Not detected at or above indicated ReportinLimit Rep. Limit — Reporting Limit unless otherwise inheated in parentheses. • • • • • =n;aeCla Bucy•�)ancno C=CeC. _- _ . c_.-L`U• � � - • AMERICAN ENVIRONMENTAL LABORATORIES CORP. C.1 DOHS ELAP AccredLtation/Registrat Lon Number 1233 Analysis Report: Polychlorinated Biphenyls, EPA Method 8080 • Shaker, DOHS LUFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-21A Date Extracted: 03/17/92 Batch No. : 8926 Date Analyzed: 03/17/92 Matrix: SOIL Date Reported: 03/20/92 Client ID No. : BH3-5 • Sample: BH3-5 Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) Aroclor 1016 12674-11-2 ND 1.0 �• Aroclor 1221 1104-28-2 ND 1.0 Aroclor 1232 11141-16-5 ND 1.0 Aroclor 1242 53469-21-9 ND 1.0 Aroclor 1248 12672-29-6 ND 1.0 • Aroclor 1254 11097-69-1 ND 1.0 Aroclor 1260 11096-82-5 ND 1.0 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. a • • i • • }�a9 nzgerala�auC•R�-cna Ccrac.c. >5742-:C* • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DONS ELAP Accreditation/Re&13tratlon Number 1233 • Analysis Report: Polychlorinated Biphenyls, EPA Method 8080 Shaker, DOHS LUFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 COC Lo No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-24A Date Extracted: 03/17/92 Batch No. : 8926 Date Analyzed: 03/17/92 Matrix: SOIL Date Reported: 03/20/92 Client ID No. : BH2-5 • Sample: BH2-5 Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) • Aroclor 1016 12674-11-2 ND 1.0 Aroclor 1221 1104-28-2 ND 1.0 Aroclor 1232 11141-16-5. ND 1.0 Aroclor 1242 53469-21-9 ND 1.0 Aroclor 1248 12672-29-6 ND 1.0 • Aroclor 1254 11097-69-1 ND 1.0 Aroclor 1260 11096-82-5 ND 1.0 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • • • • • 32.14c,Kgeraid C.>cd•Ganc'a C�rao.: :,� _ ._ -. _ "_. _: ., =t�Soa- .'�1 • AMERICAN ENVI(�ONMEE LABORATORIES CORP. CA DOHS ELAP Accreditat Son/Regia trat ion Number 1233 • Analysis Report: Polychlorinated Biphenyls, EPA Method 8080 Shaker, DOHS LUFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-27A Date Extracted: 03/17/92 Batch No. : 8926 Date Analyzed: 03/17/92 Matrix: SOIL Date Reported: 03/20/92 Client ID No. : BHS.-5 • Sample: BHI-5 Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) • Aroclor 1016 12674-11-2 ND 1.0 Aroclor 1221 1104-28-2 ND 1.0 Aroclor 1232 11141-16-5 ND 1.0 Aroclor 1242 53469-21-9 ND 1.0 • Aroclor 1248 12672-29-6 ND 1.0 Aroclor 1254 11097-69-1 ND 1.0 Aroclor 1260 11096-82-5 ND 1.0 ND — Not detected at or above indicated Reporting Limit Rep. Limit a Reporting Limit unless otherwise indicated in parentheses. • • • • • i2a9 F!-�er,.a RGOO•%onc^a Corcova G;<p.iC•-�t ^!_:3-:5 t^• o a p.p3d770+ • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOHS ELAP Accreditation/Reglatration Number 1233 Analysis Report: Polychlorinated Biphenyls, EPA Method 8080 • Shaker, DOHS LUFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 • Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Extracted: 03/17/92 COC Lo NO. : 24918 - 24920 Date Analyzed: 03/17/92 AELC ID No. : L8465 Date Reported: 03/20/92 Batch No. : 8926 Matrix: SOIL METHOD BLANK • Results Rep. Limit Analyte CAS No. (mg/kg) (mg/kg) Aroclor 1221 1104-28-2 ND 1.0 Aroclor 1232 11141-16-5 ND 1.0 Aroclor 1242 53469-21-9 ND 1.0 Aroclor 1248 12672-29-6 ND 1.0 Aroclor 1254 11097-69-1 ND 1.0 Aroclor 1260 11096-82-5 ND 1.0 • ND — Not detected at or above indicated Reportin Limit Rep. Limit — Reporting Limit unless otherwise imitated in parentheses. • • • • 3219 FIt[gerala Roca•RCrc-c CCrac>c L?05751.•-.X 0101 038-1510•,0101 n38-:'01 • AMERICAN ENVIRONMENTAL LABORATORIES COPP. CA DOES ELAP Accreditation/Registration N=ber 1233 • Analysis Report: Polychlorinated Biphenyls, EPA Method 8080 Shaker, DOHS LUFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Extracted: 03/17/92 COC Log No. : 24918 - 24920 Date Analyzed: 03/17/92 AELC ID No. : L8465 Date Reported: 03/20/92 Batch No. : 8926 Matrix: SOIL • MB SPIKE MBS MBS Cone. Recovery Analyte CAS No. (mg/kg) (percent) Aroclor 1260 11096-82-5 5.0 100 • MB SPIKE DUPLICATE MBSD MBSD Cone. Recovery Analyte CAS No. (mg/kg) (percent) • Aroclor 1260 11096-82-5 5.0 106 MB SPIKE RPD MBS Relative Percent Difference Analyte CAS No. (percent) • Aroclor 1260 11096-82-5 6 • 3?a9 Rhgeaitl Roco 4c.�a�o Coraoc.CA 9c732---X X0101 038-4:1". 0101 638-730 1 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOHS ELAF Accreditation/Registration H.ber 1233 • Analysis Report: Polychlorinated Biphenyls, EPA Method 8080 Shaker, DOHS LUFT Method Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 • Project: Solag - San Juan `SLC Contac : John Arndt : 6409 Date Reported: 03/20/92 COC Log No. : 24918 - 24920 AELC ID No. : L8465 Batch No. : 8926 Matrix: SOIL • LAB CONTROL STANDARD LCS LCS Conc. Recovery Analyte CAS No. (mg/L) (percent) Aroclor 1260 11096-82-5 0.5 106 • • • • • • • ,}210 PCgeran�Roca•�ronG^o�Jrauvr. _ %S��•`� -"��°y-J51p. Q101 JJd 7601 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOES ELAP Accreditattonl Registration Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-1A Date Extracted: 03/18/92 Batch No. : 8943 Date Analyzed: 03/18/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH10-5 • SURROGATE Surrogate Surr Conc. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 110 • Toluene-d8 N/A 100 102 p-Bromofluorobenzene 460-00-4 100 101 Sample: BH10-5 Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5 • Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 • 1,2-Dichlorobenzene 95-50-1 ND 5 1,3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 1,1-Dichloroethane 75-34-3 ND 5 12-Dichloroethane 107-06-2 ND 5 1,,1-Dichloroethene 75-35-4 ND 5 1,2-Dichloroethene, total 540-59-0 ND 5 • 1,2-Dichloropropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 I Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 ND 50 Styrene 100-42-5 ND 5 • 2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 ND — Not detected at or above indicated Reporting Limit Rep. Limit s Reporting Limit unless otherwise indicated in parentheses . • 3249 Fi2gero:d Road•Rancho Cordova.CA 95742•Fox(916)638-4510•X9161 6384301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOHS ELAP Adored Ltatlon/Reglstrat Lon N=ber 1233 . Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Waq Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-1A Date Extracted: 03/18/92 Batch No. : 8943 Date Analyzed: 03/16/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BRIO-5 • Sample: BH10-5(cont.) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 1, 1, 1-Trichloroethane 71-55-6 ND 5 +.• 1,1,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5- Trichlorofluoromethane 75-69-4 ND 5 1,1,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes , total 1330-20-7 ND 10 • ND — Not detected at or above indicated ReportingLimit Rep. Limit — Reporting Limit unless otherwise inicated in parentheses. • • • • y°' .,rn w=.wn 3249 flhgerala Road-Roncho Coraovo,CA 95142-:aa(916)638-4510•(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORA CA DOHS ELAP Accreditation/Regi3tratlOn N=ber 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-2A Date Extracted: 03/18/92 Batch No. : 8943 Date Analyzed: 03/18/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BHIO-10 • SURROGATE Surrogate Surr Conc. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 106 • Toluene-d8 N/A 100 102 p-Bromofluorobenzene 460-00-4 100 96 Sample: BH10-10 Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5 • Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 • 1,2-Dichlorobenzene 95-50-1 ND 5 1,3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 1,1-Dichloroethane 75-34-3 ND 5 1,2-Dichloroethane 107-06-2 ND 5 1,1-Dichloroethene 75-35-4 ND 5 1,2-Dichloroethene, total 540-59-0 ND 5 1,2-Dichloropropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 ND 50 Styren! 100-42-5 ND 5 • 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • 1°a .v-n®r— 3249 Fitzgerald Road•Rancho Cordova.CA 95742•Fax(916)638-4510•(916)6384301 • AMERICAN ENVIPONMENTAL LABOgATORIES CORR CA DOHS ELAP Accred Ltation/Reg Latrat Lon Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman We Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Lo No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-2A Date Extracted: 03/18/92 Batch No. : 8943 Date Analyzed: 03/18/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BHIO-10 • Sample: BH10-10(cont.) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 111-Trichloroethane 71-55-6 ND 5 ,• 1,,1,,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5 Trichlorofluoromethane 75-69-4 ND 5 1, 1,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes, total 1330-20-7 ND 10 • ND — Not detected at or above indicated ReportingLimit Rep. Limit — Reporting Limit unless otherwise inicated in parentheses. • • • • �n onueu v.o,a 3249 Fitgeraid Road•Rancho Cordova.CA 95742•Fox(9161 o38-4510•(9161 638-7301 • AMERICAN ENVIRONMENTAL LABGFiATOR1E5 CGRP. CA DONS ELAP Aeeredltat Lon/ReSlatratlen Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-3A Date Extracted: 03/18/92 Batch No. : 8943 Date Analyzed: 03/1S/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BHIO-15 • SURROGATE Surrogate Surr Conc. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 106 • Toluene-d8 N/A 100 101 p-Bromofluorobenzene 460-00-4 100 103 Sample: BHIO-15 Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5 Carbon tetrachloride 56-23-5 ND 5 !• Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 • 1,2-Dichlorobenzene 95-50-1 ND 5 1,3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 1,1-Dichloroethane 75-34-3 ND 5 1, 2-Dichloroethane 107-06-2 ND 5 1, 1-Dichloroethene 75-35-4 ND 5 1, 2-Dichloroethene, total 540-59-0 ND 5 • 1, 2-Dichloropropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 ND 50 Styrene 100-42-5 ND 5 '• 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 ND — Not detected at or above indicated Reportin Limit Rep. Limit — Reporting Limit unless otherwise in�icated in parentheses. • 3c° uv.,ppvma 32A9 Fingerald Road•Rancho Cordova.CA 95742•Fax(916)638-4510•t916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA OOHS ELAP Atered1tat1on/Reg Lattat Lon Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-3A Date Extracted: 03/18/92 Batch No. : 8943 Date Analyzed: 03/18/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH10-15 • Sample: BH10-15(cont.) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 1,1,1-Trichloroethane 71-55-6 ND 5 • 1, 1,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5 Trichlorofluoromethane 75-69-4 ND 5 111,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes, total 1330-20-7 ND 10 • ND — Not detected at or above indicated Reporting Limit Rep. Limit a Reporting Limit unless otherwise indicated in parentheses. • • 0 • 3249 Fitzgerald Rood•Rancho Cordova.CA 95742•Fax 1916)638-4510.1916)638-730 - • AVEFENVIRONMENTAL pCAVRATORIES i . CA DORS ELAP Accreditat ion/Reg i,trat ion Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt No. : 6409 • Date Sampled: 03/12/92 COC Logo No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-4A Date Extracted: 03/18/92 Batch No. : 8943 Date Analyzed: 03/1C/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH9-5 • SURROGATE Surrogate Surr Conc. Recovery Analyte CAS No. (ug/kg) (percent) 1, 2-Dichloroethane-d4 N/A 100 107 • Toluene-d8 N/A 100 102 p-Bromofluorobenzene 460-00-4 100 96 Sample: BH9-5 Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Brom6form 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5' • Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 • 1,2-Dichlorobenzene 95-50-1 ND 5 1,3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 1,1-Dichloroethane 75-34-3 ND 5 1,2-Dichloroethane 107-06-2 ND 5 1, 1-Dichloroethene 75-35-4 ND 5 1,2-Dichloroethene, total 540-59-0 ND 5 '• 1,2-Dichloropropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 NO 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND CO Methylene chloride 75-09-2 NO 5 4-Methyl-2-pentanone 108-10-1 NO 50 Styrene 100-42-5 ND 5 • 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • 7b nmm+.wo 3249 Fitzgerald Road•Rancho Cordova.CA 95742•%ax f916)6383510.1916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOES ELAP Accreditation/Registration Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Slay Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt No. : 6409 • Date Sampled: 03/12/92 COC Logo No. : 24918 - 24920 Date Received: 03/13/92 AELC ZD No. : L8465-4A Date Extracted: 03/18/92 Batch No. : 8943 Date Analyzed: 03/18/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH9-5 • Sample: BH9-5(cont.) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 1,11-Trichloroethane 71-55-6 ND 5 • 1,1,,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5 Trichlorofluoromethane 75-69-4 ND 5 1,1,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes , total 1330-20-7 ND 10 • ND — Not detected at or above indicated Reporting Limit Rep. Limit = Reporting Limit unless otherwise indicated in parentheses. • • a 45e° 3249 F,tgeraid Road•Rcncno Corcova.CA 95742•Fax(916)638-4510•(916)638.7301 • AMERICAN ENV1FlONMEE LABOFlATORIES COFP. CA DOHS ELAP Accreditation/Registration Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-5A Date Extracted: 03/18/92 Batch No. : 8943 Date Analyzed: 03/18/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH9-10 • SURROGATE Surrogate Surr Conc. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 107 ,• Toluene-d8 N/A 100 107 p-Bromofluorobenzene 460-00-4 100 102 Sample: BH9-10 Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5 • Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 • 1,2-Dichlorobenzene 95-50-1 ND 5 13-Dichlorobenzene 541-73-1 ND 5 1,,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 1,1-Dichloroethane 75-34-3 ND 5 1,2-Dichloroethane 107-06-2 ND 5 1,1-Dichloroethene 75-35-4 ND 5 1,2-Dichloroethene, total 540-59-0 ND 5 • 1,2-Dichloropropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 ND 50 Styrene 100-42-5 ND 5 • 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • 72 3249 Firzgeraid Road•Rancho Cordova,CA 95742•Fax(916)638-4510-016)o38-7301 • AMERICAN ENVIRONMENTAL LABOgATOR1E5 CORP. CA DONS ELAP Acered1tat1..1Regietrat1on Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Wap Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-5A Date Extracted: 03/18/92 Batch No. : 8943 Date Analyzed: 03/16/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH9-10 • Sample: BH9-10(cont. ) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 111-Trichloroethane 71-55-6 ND 5 • 1,, 1,,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5 Trichlorofluoromethane 75-69-4 ND 5 1,1,2-Trichlorotrifluoroethane 79-13-1 ND . 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes, total 1330-20-7 ND 10 • NO m Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • • • • �$ .u.ivuowx 3249 Fitzgerald Road•Rancho total CA 95742•Fox 19161 t38-4510-19161638-7301 • A11/I�i�IC/�N ENVIRONMENTAL LABOFlATORIeS COfiR CA 00HS ELAP Accreditatlon(Regiatratlon Number 1233 Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 • Client: AEMC Boatman Project No. : 6409 10960 Boatman We Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-6A Date Extracted: 03/18/92 Batch No. : 8943 Date Analyzed: 03/18/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH9-15 • SURROGATE Surrogate Surr Cone. Recovery Analvte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 103 Toluene-d8 N/A 100 102 p-Bromofluorobenzene 460-00-4 100 97 Sample: BH9-15 Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5 Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 • 1,2-Dichlorobenzene 95-50-1 ND 5 1, 3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 1, 1-Dichloroethane 75-34-3 ND 5 1,2-Dichloroethane 107-06-2 ND 5 1,1-Dichloroethene 75-35-4 ND 5 1, 2-Dichloroethene, total 540-59-0 ND 5 S 1,2-Dichloropropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 ND 50 Styrene 100-42-5 ND 5 • 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • 3u +u,..0=4+•. 3249 Fi2gerala Roca•Rancho CordOvc,CA 95742-Fox!9161 638-4510-(916)838-7301 • AMERICAN ENVIRONMENTAL LAB01ATpR1E5 CORP. CA DOHS ELAP Accreditation/Registration N=ber 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-6A Date Extracted: 03/18/92 Batch No. : 8943 Date Analyzed: 03/l6/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH9-15 • Sample: BH9-15(cont.) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 1,11-Trichloroethane 71-55-6 ND 5 • 1,1,,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5 Trichlorofluoromethane 75-69-4 ND 5 1,1,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes, total 1330-20-7 ND 10 • ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • • • • • 3249 Fthgerald Road•Rancho Cordova.CA 95742•Fax 1910)635a5t3•(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORR CA DOSS SLAP Accred Ltatlan/Reglatration Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Wap Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 0 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-7A Date Extracted: 03/18/92 Batch No. : 8943 Date Analyzed: 03/1S/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH8-5 0 SURROGATE Surrogate Surr Conc. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 106 Toluene-d8 N/A 100 102 p-Bromofluorobenzene 460-00-4 100 97 Sample: BH8-5 Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5 Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 1,2-Dichlorobenzene 95-50-1 ND 5 1,3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 1,1-Dichloroethane 75-34-3 ND 5 1,2-Dichloroethane 107-06-2 ND 5 1,1-Dichloroethene 75-35-4 ND 5 1,2-Dichloroethene, total 540-59-0 ND 5 1,2-Dichloropropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Mechyl-2-pentanone 108-10-1 ND 50 Styrene 100-42-5 ND 5 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 ND — Not detected at or above indicated Reportin Limit Rep. Limit — Reporting Limit unless otherwise in�icated in parentheses. 3249 Fitzgerald Road•Parana Cordova.CA 95742•=ax(916)638.1510•io161 6387301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOES ELAP Accreditation/Registration N=ber 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman We Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-7A Date Extracted: 03/18/92 Batch No. : 8943 Date Analyzed: 03/18/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No, : BH8-5 • Sample: BH8-5(cont. ) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 111-Trichloroethane 71-55-6 ND 5 1,,1,,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5 Trichlorofluoromethane 75-69-4 ND 5 1,1, 2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes, total 1330-20-7 ND 10 • ND - Not detected at or above indicated Reporting Limit Rep, Limit - Reporting Limit unless otherwise in in parentheses. • • 4 • • ,rieo w<A 3249 Fingeraic Road•Rancno Coraovc,CA 95702•-ox(916)638-4510•(916)638-7301 • AMERICAN ENVIFIONMENTALL 1901 ATOFilE9 COARt CA DORS ELAP Aceteditation/Regiattation H=bet 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Wap Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-8A Date Extracted: 03/18/92 Batch No. : 8943 Date Analyzed: 03/18'/92 Matrix: SOIL Date Reported: 03/29/92 Client ID NO. : BHS-10 • SURROGATE Surrogate Surr Conc. Recovery Analyte CAS No. (ug/kg) (percent) • 1,2-Dichloroethane-d4 N/A 100 108 Toluene-d8 N/A 100 101 p-Bromofluorobenzene 460-00-4 100 98 Sample: BH8-10 Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2' ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5 • Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 • 1,2-Dichlorobenzene 95-50-1 ND 5 1,3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 NO 10 11-Dichloroethane 75-34-3 ND 5 1,,2-Dichloroethane 107-06-2 ND 5 1,1-Dichloroethene 75-35-4 ND 5 1,2-Dichloroethene, total 540-59-0 ND 5 • 1,2-Dichloropropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 ND 50 styrene 100-42-5 ND 5 • 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise inicated in parentheses. • 3249 Fitzgerald Road•Rancho Cordow,CA 95742•Fox(916)638-4510•(916)638-7701 AMERICAN ENVIMONMENTAL LABOAATOp1E5 COpP. CA DONS ELAP Aecredlcat Lon/Reglatratlon Number 1233 Analysis Report: Volatile Organic Compounds by CC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt . Job No. : 6409 Date Sampled; 03/12/92 COC Lo No. : 24918 - 24920 Date Received; 03/13/92 AELC ID No. : L8465-8A Date Extracted: 03/18/92 Batch No. : 8943 Date Analyzed: 03/18/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH8-10 Sample: BHB-10(cont.) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 1, 1, 1-Trichloroethane 71-55-6 ND 5 1,1,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5 Trichlorofluoromethane 75-69-4 ND 5 1,1,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes, total 1330-20-7 ND 10 ND - Not detected at or above indicated Reporting Limit Rep. Limit >< Reporting Limit unless otherwise indicated in parentheses. ;f 0.3 n. rn v,nx 3249 Fingeroitl Roatl•Pan Calaova.CA 95742•Fax(916)638-5510•(916)638-7301 • AMERICAN VMUO CA OOHS ELAP Accred Ltation/Registration N=ber 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 COC Lo No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-9A Date Extracted: 03/18/92 Batch No. : 8943 Date Analyzed: 03/18/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BHS-15 • SURROGATE Surrogate Surr Conc, Recovery Analyte CAS No. (ug/kg) (percent) ,• 1,2-Dichloroethane-d4 N/A 100 118 Toluene-d8 N/A 100 103 p-Bromofluorobenzene 460-00-4 100 100 Sample: BH8-15 Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5 Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 • Dibromomethane 74-95-3 ND 5 1,2-Dichlorobenzene 95-50-1 ND 5 1,3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 1,1-Dichloroethane 75-34-3 ND 5 1,2-Dichloroethane 107-06-2 ND 5 1,1-Dichloroethene 75-35-4 ND 5 • 1,2-Dichloroethene, total 540-59-0 ND 5 1,2-Dichloropropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 ND 50 • Styrene 100-42-5 ND 5 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 ND - Not detected at or above indicated Reporting Limit Rep. Limit - Reporting Limit unless otherwise indicated in parentheses. • 3249 Filrgeraid Roca•Rancho cordo .CA 95742•Fax X916)6384510•(9161638-7301 • AMERICAN VFACCR CA DOES ELAP Accred Ltatlon/Registration Number 1233 Analysis Report: Volatile Organic Compounds by CC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ZD No. : L8465-9A Date Extracted: 03/18/92 Batch No. : 8943 Date Analyzed: 03/18/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BHS-15 Sample: BH8-15(cont.) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 w 1,1, 1-Trichloroethane 71-55-6 ND 5 1,1,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5 Trichlorofluoromethane 75-69-4 ND 5 1,1,2-Trichlorotrifluoroethane. 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 . Xylenes, total 1330-20-7 ND 10 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. 3249 F,kge oid Road•Rancno Cotao.o,CA 05742•Fax(916)638-4510•(916)638-7301 AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOHS ELAP Accreditation]Regis trat ion Number 1233 Analysis Report: Volatile Organic Compounds by GC/HS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-IOA Date Extracted: 03/18/92 Batch No. : 8943 Date Analyzed: 03/16/92 Matrix: SOIL Date Reported: 03//29/92 Client ID No. : BH7-5 r SURROGATE Surrogate Surr Conc. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 121 Toluene-d8 N/A 100 104 p-Bromofluorobenzene 460-00-4 100 98 Sample: BH7-5 Results R Analyte CAS No. (ug/kg) (ug mit /kg) Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5 t� Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 1,2-Dichlorobenzene 95-50-1 ND 5 1,3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 1,1-Dichloroethane 75-34-3 ND 5 1,2-Dichloroethane 107-06-2 ND 5 1,1-Dichloroethene 75-35-4 ND 5 1,2-Dichloroethene, total 540-59-0 ND 5 1,2-Dichloropropane 78-87-5 ND 5 cis-1, 3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 ND 50 Styrene 100-42-5 ND 5 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 ND — Not detected at or above indicated Reporting Limit Rep. Limit a Reporting Limit unless otherwise indicated in parentheses. 1 3249 fittge ald Racd•Rancno CordcvO.CA 95742•Fax 1916+638-4510•(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORK CA ➢095 ELAP Aneredltatlon/Reglatration Number 1273 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-IOA Date Extracted: 03/18/92 Batch No. : 8943 Date Analyzed: 03/18/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH7-5 • Sample: BH7-5(cont.) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 1,1,1-Trichloroethane 71-55-6 ND 5 • 1,1,2-Trichloroethane 79-00-5 NO 5 Trichloroethene 79-01-6 ND 5 Trichlorofluoromethane 75-69-4 ND 5 1,1,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes, total 1330-20-7 ND 10 • ND a Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise in in parentheses. • • • • • er' .viii Eo.wv 3249 Fingerotd Road•Rancho Cordova,CA 95742•Fox(916)638-4510•(916)6387301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOSS ELAP Accreditat Lon/Regia trat ion Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Wap Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt . Job No. : 6409 Date Extracted: 03/18/92 COC Lo No. : 24918 - 24920 Date Analyzed: 03/18/92 AELC ID No. : L8465 Date Reported: 03/29/92 Batch No. : 8943 Matrix: SOIL MB SURROGATE • MB Surrogate Surr Conc. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 106 Toluene-d8 N/A 100 101 • p-Bromofluorobenzene 460-00-4 100 95 METHOD BLANK Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5 Carbon tetrachloride 56-23-5 ND 5 ,• Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 1,2-Dichlorobenzene 95-50-1 ND 5 • 1,3-Dichlorobenzene 541-73-1 ND 5 114-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 1,1-Dichloroethane 75-34-3 ND 5 1,2-Dichloroethane 107-06-2 ND 5 11-Dichloroethene 75-35-4 ND 5 1,,2-Dichloroethene, total 540-59-0 ND 5 112-Dichloropropane 78-87-5 ND 5 • cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 ND 50 Styrene 100-42-5 ND 5 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 Toluene 108-88-3 ND 5 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • n..,F„ ..=. 3249 F,tzgeraia Roca•Oancro Coraova,CA 95742-=az!9161638-1510•I9161 6384301 • AMERICAN ENVIRONMENTAL LABOFATOg1Fi5 CORP. CA DONS ELAP Accreditation/Regiatrat Lon N.ber 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Extracted: 03/18/92 COC Log Ni 24918 - 24920 Date Analyzed: 03/18/92 AELC ID No. : L8465 Date Reported: 03/29/92 Batch No. : 8943 Matrix: SOIL METHOD BLANK(cont.) • Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) 1,1,1-Trichloroethane 71-55-6 ND 5 1, 1,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5 Trichlorofluoromethane 75-69-4 ND 5 ,• 1,1,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes, total 1330-20-7 ND 10 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • • • • • • 3249 Fitzgerald Road•Rancho Cordova.CA 95742•Fox(916)638-4510•(916)6387301 • AMERICAN ENVIRONMENTAL WSQRATORlES CORP. CA DOES ELAP Accraditation/Registration Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Vg Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Extracted: 03/18/92 COC Log No. : 24918 - 24920 Date Analyzed: 03/18/92 AELC ID No. : L8465 Date Reported: 03/29/92 Batch No. : 8943 Matrix: SOIL MS SURROGATE • MS MS Surr. Surrogate Conc. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 114 Toluene-d8 N/A 100 103 • p-Bromofluorobenzene 460-00-4 100 96 MATRIX SPIKE - MS MS Conc. Recovery Analyte CAS No, (ug/kg) (percent) • Benzene 71-43-2 50 125 Chlorobenzene 108-90-7 50 102 1,1-Dichloroethene 75-35-4 50 114 Toluene 108-88-3 50 122 Trichloroethene 79-01-6 50 104 MSD SURROGATE • MSD Surr. Surrogate Conc. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 112 • Toluene-d8 N/A 100 102 p-Bromofluorobenzene 460-00-4 100 98 MATRIX SPIKE DUPLICATE MSD MSD Conc. Recovery • Analyte CAS No. (ug/kg) (percent) Benzene 71-43-2 50 116 Chlorobenzene 108-90-7 50 98 1, 1-Dichloroethene 75-35-4 50 108 Toluene 108-88-3 50 113 Trichloroethene 79-01-6 50 98 • • to wi• [n oow 3249 Fingeraia Road•RonC00 Cordova.CA 95742•Fax(916)638-45510-(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DONS ELAP Accreditation/Registration Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Extracted: 03/18/92 COC Log No. : 24918 - 24920 Date Analyzed: 03/18/92 AELC ID No. : L8465 Date Reported: 03/29/92 Batch No. : 8943 Matrix: SOIL RELATIVE % DIFFERENCE • Relative Percent Difference Analyte CAS No. (percent) Benzene 71-43-2 7 Chlorobenzene 108-90-7 4 • 1,1-Dichloroethene 75-35-4 5 Toluene 108-88-3 8 Trichloroethene 79-01-6 6 • • • • • • 3249 Fingeraitl Road•Rancho Coroova.CA 95742•Fax(916)638-4510•(916)638-7301 • AMERICAN fiSN ENVIRLAB CORP. CA DORS ELAP Accredltatlon/Realetratlon Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Wap Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Reported: 03/29/92 COC Log No. : 24918 - 24920 AELC ID No. : L8465 Batch No. : 8943 Matrix: SOIL LAB CONTROL STANDARD • LCS LCS Conc. Recovery Analyte CAS No. (ug/L) (percent) Benzene 71-43-2 50 101 Chlorobenzene 108-90-7 50 90 1,1-Dichloroethene 75-35-4 50 92 • Toluene 108-88-3 50 97 Trichloroethene 79-01-6 50 91 • • • • • • au.0[nowa 3249 Fingerold Road•Rancho Cordova,CA 95742•Fax(916)638-4510•(916)o38-7301 • AMERICAN iM RATORINS CORA CA DOHS ELAP Accredlcation/Regiatraclon Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Wap Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Extracted., 03/19/92 COC Log No. : 24918 - 24920 Date Analyzed: 03/19/92 AELC ID No. : L8465 Date Reported: 03/29/92 Batch No. : 8944 Matrix: SOIL MB SURROGATE • MB Surrogate Surr Cont. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 106 Toluene-d8 N/A 100 97 p-Bromofluorobenzene. 460-00-4 100 98 METHOD BLANK Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64=1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5 Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 NO 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 1,2-Dichlorobenzene 95-50-1 ND 5 • 1, 3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 1,1-Dichloroethane 75-34-3 ND 5 1,2-Dichloroethane 107-06-2 ND 5 1,1-Dichloroethene 75-35-4 ND 5 1,2-Dichloroethene, total 540-59-0 ND 5 1,2-Dichloropropane 78-87-5 ND 5 • cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 ND 50 Stpren; 100-42-5 ND 5 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 • Tetrachloroethene 127-18-4 ND 5 Toluene 108-88-3 ND 5 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • k •n.n eo o,.n 3249 F2gerala Road•Rancho Cordova,CS 95742-;ax(9161638-4510-016)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA D095 ELAP AccreditationlReg iatrat Ion Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Extracted: 03/19/92 COC Lo No. : 24918 - 24920 Date Analyzed: 03/19/92 AELC ID No. : L8465 Date Reported: 03/29/92 Batch No. : 8944 Matrix: SOIL METHOD BLANK(cont.) • Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) 1,1,1-Trichloroethane 71-55-6 ND 5 1,1,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5 • Trichlorofluoromethane 75-69-4 ND 5 1,1,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND " 50 Vinyl chloride 75-01-4 ND 10 Xylenes , total 1330-20-7 ND 10 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • • • • • • .a.,m o.... 3249 Fozgerald Road•Rancho Cordova.CA 95742•Fo:(916)o38-4510•;916)638.7301 • /AMERICAN ENVIRCNMENTAL LA®ORATORIES CORP. CA DOES ELAP Aecredltat1on/R.s1stratlon N.ber 1233 0 Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-11A Date Extracted: 03/19/92 Batch No. : 8944 Date Analyzed: 03/15/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH -10 0 SURROGATE Surrogate Surr Conc. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 107 0 Toluene-d8 N/A 100 100 p-Bromofluorobenzene 460-00-4 100 96 Sample: BH7-10 Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5 i• Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 0 1,2-Dichlorobenzene 95-50-1 ND 5 1,3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 1,1-Dichloroethane 75-34-3 ND 5 1,2-Dichloroethane 107-06-2 ND 5 1,1-Dichloroethene 75-35-4 ND 5 1,2-Dichloroethene, total 540-59-0 ND 5 0 1,2-Dichloropropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 ND 50 Styrene 100-42-5 ND 5 0 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • =n: ienrw+ 3249 Ftzgeraia Road•Rancho Cordova,CA 95742•fax(916)638.4510•(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOHS ELAP Accreditatton/Reaiatratlan N=ber 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 CCC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-11A Date Extracted: 03/19/92 Batch No. : 8944 Date Analyzed: 03/19/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH7-10 • Sample: BH7-10(cont. ) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 1,1,1-Trichloroethane 71-55-6 ND 5 • 1,1,2 -Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5 Trichlorofluoromethane 75-69-4 ND 5 1, 1,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes , total 1330-20-7 ND 10 • ND m Not detected at or above indicated Reporting Limit Rep. Limit - Reporting Limit unless otherwise indicated in parentheses. i• • • A • • �e .n,•.�n o,no 3249 fingeraid Road•Rancho Cardovc.CA 95742•=cx(916)638-4510•X916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA OOHS ELAP Accredltatlen/Reglatratlon Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Wap Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-12A Date Extracted: 03/19/92 Batch No. : 8944 Date Analyzed: 03/15/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH6-5 • SURROGATE Surrogate Surr Conc. Recovery Analyte CAS No. (ug/kg) (percent) • 1,2-Dichloroethane-d4 N/A 100 107 Toluene-d8 N/A 100 102 p-Bromofluorobenzene 460-00-4 100 95 Sample: BH6-5 Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 'ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 NO 100 Carbon disulfide 75-15-0 ND 5 • Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 • 1,2-Dichlorobenzene 95-50-1 ND 5 1,3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 1,1-Dichloroethane 75-34-3 ND 5 1,2-Dichloroethane 107-06-2 ND 5 1,1-Dichloroethene 75-35-4 ND 5 1,2-Dichloroethene, total 540-59-0 ND 5 • 1,2-Dichloropropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 NO 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 NO 50 Styrene 100-42-5 ND 5 • 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 ND - Not detected at or above indicated Reporting Limit Rep. Limit - Reporting Limit unless otherwise inicated in parentheses. • r$ +n mruo•,.: 3249 F'ihgeroid Rocd-Roncno Cordova.CA 95742•Fox(916)638.3510-(916)638-7301 • AMERICAN ENVIRONMENTAL LA90PATOPIES COPA. CA DOHS ELAP Aee red Ltac Lon(Reg iacrac Lon Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-12A Date Extracted: 03/19/92 Batch No. : 8944 Date Analyzed: 03/19/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH6-5 • Sample: BH6-5(cont.) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 • 1,1,1-Trichloroethane 71-55-6 NO 5 1,1,2-Trichloroethane 79-00-5 NO 5 Trichloroethene 79-01-6 NO 5 Trichlorofluoromethane 75-69-4 ND 5 11,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes, total 1330-20-7 ND 10 • ND — Not detected at or above indicated ReportingLimit Rep. Limit — Reporting Limit unless otherwise inicated in parentheses. • • • • • ?$a,r•r.,torvna 3249 Fitgerold Rood•Rancho CardOvO.CA 95742•Fox(9161638-4510•(016)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORA CA D095 SLAP Accreditation/Registration Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Wap Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-13A Date Extracted: 03/19/92 Batch No. : 8944 Date Analyzed: 03/19/92 Matrix: SOIL Date Reported: 03/29%92 Client ID No. : BH6-10 • SURROGATE Surrogate Surr Conc. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 109 • Toluene-d8 N/A 100 103 p-Bromofluorobenzene 460-00-4 100 94 Sample: BH6-10 Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5 Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 • 1,2-Dichlorobenzene 95-50-1 ND 5 1,3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 1,1-Dichloroethane 75-34-3 ND 5 1,2-Dichloroethane 107-06-2 ND 5 1,1-Dichloroethene 75-35-4 ND 5 1,2-Dichloroethene, total 540-59-0 ND 5 • 1,2-Dichloropropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 ND 50 Styrene 100-42-5 NO 5 a 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 ND o Not detected at or above indicated ReportingLimit Rep. Limit — Reporting Limit unless otherwise inicated in parentheses. • 7n unruor,nw 3249 Fllzgerold Road•Poncho Cordova.CA 95742•Fax(9161638-4510•(916(638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DONS SLAP Aeered Ltatlan/Reaietratian N, ber 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Wap Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-13A Date Extracted., 03/19/92 Batch No. : 8944 Date Analyzed: 03/1:/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH6-10 • Sample: BH6-10(cont. ) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 • 1,1,1-Trichloroethane 71-55-6 ND 5 1, 1,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5 Trichlorofluoromethane 75-69-4 ND 5 1,1,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes, total 1330-20-7 ND 10 • ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • • • • • • •n,n wn= 3249 Fitzgerald Road•Rancho Cordova,CA 95742•Pax 1016)o38-1510•(9MJ 638-1301 • AMERICAN ENVIRONMENTAL LABOFlATOQIES COiiR CA DOES ELAP Accred Ltatlon/Reaiatration Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Wap Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 COC Lo No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-14A Date Extracted: 03/19/92 Batch No. : 8944 Date Analyzed: 03/15/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH6-15 • SURROGATE Surrogate Surr Conc. Recovery Analyte CAS No. (ug/kg) (percent) • 1,2-Dichloroethane-d4 N/A 100 103 Toluene-d8 N/A 100 103 p-Bromofluorobenzene 460-00-4 100 97 Sample: BH6-15 Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 • Carbon disulfide 75-15-0 ND 5 Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 • 1,2-Dichlorobenzene 95-50-1 ND 5 1,3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 1,1-Dichloroethane 75-34-3 ND 5 1,2-Dichloroethane 107-06-2 ND 5 1, 1-Dichloroethene 75-35-4 ND 5 1,2-Dichloroethene, total 540-59-0 ND 5 • 1,2-Dichloropropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 ND 50 Styrene 100-42-5 ND 5 • 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 ND a Not detected at or above indicated Reporting Limit Rep. Limit - Reporting Limit unless otherwise indicated in parentheses. • 3249 Fitzgerald Road•Ronaba Cordova.CA 95742-°ax(916)639-4510-!916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA OOHS ELAP ACcred1titJ.n)Reg1]tr.t1.n Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-14A Date Extracted: 03/19/92 Batch No. : 8944 Date Analyzed: 03/19/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH6-15 • Sample: BH6-15(cont.) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 1,1,1-Trichloroethane 71-55-6 ND 5 • 1, 1,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5 Trichlorofluoromethane 75-69-4 ND 5 1, 1,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes , total 1330-20-7 ND 10 • ND — Not detected at or above indicated Reporting Limit Rep. Limit m Reporting Limit unless otherwise indicated in parentheses. • • • • • 3249 Fitzgerald Road•Rancho Cordova.CA 95742•Fox(916)638-4510-(916)6387301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. LA DONS ELAP Accredit.[Lon/R.SLetration Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-15A Date Extracted: 03/19/92 Batch No. : 8944 Date Analyzed: 03/19/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH5-5 • SURROGATE Surrogate Surr Conc. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 103 '• Toluene-d8 N/A 100 103 p-Bromofluorobenzene 460-00-4' 100 99 Sample: BH5-5 Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 �• Carbon disulfide 75-15-0 ND 5 Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 • 1,2-Dichlorobenzene 95-50-1 ND 5 1,3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 1, 1-Dichloroethane 75-34-3 ND 5 1,2-Dichloroethane 107-06-2 ND 5 1,1-Dichloroethene 75-35-4 ND 5 1,2-Dichloroethene, total 540-59-0 ND 5 • 1,2-Dichloropropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 ND 50 Styrene 100-42-5 ND 5 • 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 ND — Not detected at or above indicated Reporting Limit Rep. Limit a Reporting Limit unless otherwise indicated in parentheses. • k4 aun.i[o o.no 3219 Fingemfd Road.Rancho Cordova.CA 95742•FOX(916)638,4510-f916)638-7301 • AMERICAN ENVIAONMEE LABICAIES CORP. CA D0SS ELAP Accreditation/Regietration N=ber 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-15A Date Extracted: 03/19/92 Batch No. : 8944 Date Analyzed: 03/15/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH5-5 • Sample: BH5-5(cont. ) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 1,1, 1-Trichloroethane 71-55-6 ND 5 • 1,1,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5 Trichlorofluoromethane 75-69-4 ND 5 1,1,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes, total 1330-20-7 ND 10 • ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses . • • • • a .c to=wc 3249 Fitgeroid Rood•Poncno Cordova.CA 95742•Fax(916)638-4510•(916)638-7301 • AMERICAN ENVIRONMENTAL LA®ORATORIEE CDg0. CA DOHS ELAP AnCred Ltit Lon/Registration Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-16A Date Extracted: 03/19/92 Batch No. : 8944 Date Analyzed: 03/19/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH5-10 • SURROGATE Surrogate Surr Conc. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 102 Toluene-d8 N/A 100 102 p-Bromofluorobenzene 460-00-4 100 99 Sample: BH5-10 Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5 Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 • 1,2-Dichlorobenzene 95-50-1 ND 5 1,3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 1,1-Dichloroethane 75-34-3 ND 5 1,2-Dichloroethane 107-06-2 ND 5 1,1-Dichloroethene 75-35-4 ND 5 1,2-Dichloroethene, total 540-59-0 ND 5 1,2-Dichloropropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 NO 5 4-Methyl-2-pentanone 108-10-1 ND 50 Stvrene 100-42-5 ND 5 • 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise inicated in parentheses. • au n,oPwo 3249 Fingerold Road•Rancho CoTd0VC.CA 95742•Fax(9161638-4510•x;9161 638-7301 • AMERICAN � ir . CA DOHS ELAP ACrred1tetL.n/Re6letret1cn Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Wap Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-16A Date Extracted: 03/19/92 Batch No. : 8944 Date Analyzed: 03/19/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH5-10 • Sample: BH5-10(cont. ) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 1,1,1-Trichloroethane 71-55-6 ND 5 • 1,1,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5 75-69-4 ND 5 Trichlorofluoromethane 1,1,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes, total 1330-20-7 ND 10 • ND - Not detected at or above indicated R6porting Limit Rep. Limit - Reporting Limit unless otherwise indicated in parentheses. • • • • • a„aroowc 3249 Pingerolc Roca•Poncho Coroovo.CA 05742•fox(916)638-4510•(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DONS ELAP Accred1tation/Reg1strat1.. Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Wap Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-17A Date Extracted: 03/19/92 Batch No. : 8944 Date Analyzed: 03/19/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH5-15 • SURROGATE Surrogate Surr Cone. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 105 • Toluene-d8 N/A 100 103 p-Bromofluorobenzene 460-00-4 100 96 Sample: BH5-15 Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5 • Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 • 1,2-Dichlorobenzene 95-50-1 ND 5 1,3- Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 1,1-Dichloroethane 75-34-3 ND 5 1,2-Dichloroethane 107-06-2 ND 5 1,1-Dichloroethene 75-35-4 ND 5 1,2-Dichloroethene, total 540-59-0 ND 5 • 1,2-Dichloropropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 NO 50 Stpren; 100-42-5 ND 5 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • 3249 Fitzgerald Road•Rancho Cordova.CA 95742•Fax(916)638-4510•(916(638-7301 • AMERICAN ENVIAONM6E LA00RATOg1E9 CORP. CA Doss ELAP Accreditation/Registration Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-17A Date Extracted: 03/19/92 Batch No. : 8944 Date Analyzed: 03/19/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH5-15 • Sample: BH5-15(cont.) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 1,1,1-Trichloroethane 71-55-6 ND 5 • ,1,1,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5 Trichlorofluoromethane 75-69-4 ND 5 1,1,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes, total 1330-20-7 ND 10 • ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • • • • • a$ =em mann 3249 Fitzgerald Road•Rancho Cordova,CA 95742•Fax(916(638-4510•(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATOR1e5 COFlP. CA DONS ELAP Accred1tat1onlReg1.trat1on N.bet 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Waq Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Lo No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-18A Date Extracted: 03/19/92 Batch No. : 8944 Date Analyzed: 03/19/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH4-5 • SURROGATE Surrogate Surr Conc. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 107 • Toluene-d8 N/A 100 109 p-Bromofluorobenzene 460-00-4 100 101 Sample: BH4-5 Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5 • Carbon tetrachloride 56-23-5 ND 5 1 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 • 1,2-Dichlorobenzene 95-50-1 ND 5 1,3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 15-11-8 ND 10 1,1-Dichloroethane 75-34-3 ND 5 1,2-Dichloroethane 107-06-2 ND 5 1,1-Dichloroethene 75-35-4 ND 5 1,2-Dichloroethene, total 540-59-0 ND 5 • 1,2-Dichloropropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 ND 50 Styrene 100-42-5 ND 5 • 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • +1.111 to awe 3249 Fitzgerald Road•Rancho Cordova,CA 95742•Fox(916)638-4510•(916)638-7301 • AMERICAN A . CA DOHS ELAP Aeeredltat Lonl Reg1.tratlon Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman We Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-18A Date Extracted: 03/19/92 Batch No. : 8944 Date Analyzed: 03/19/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH4-5 • Sample: BH4-5(cont.) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 1,1,1-Trichloroethane 71-55-6 ND 5 • 1,1,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5 Trichlorofluoromethane 75-69-4 ND 5 1 1,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes , total 1330-20-7 ND 10 • ND — Not detected at or above indicated ReVorting Limit Rep. Limit m Reporting Limit unless otherwise indicated in parentheses. • • • • • otrn eo.nx 3249 Fitzgerald Road•Rancho Cordova CA 95742•Fox(916)638-4510•(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOHS EUP Acereditacion/Reglettation Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-19A Date Extracted: 03/19/92 Batch No. : 8944 Date Analyzed: 03/15/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH4-10 • SURROGATE Surrogate Surr Conc, Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 107 • Toluene-d8 N/A 100 103 p-Bromofluorobenzene 460-00-4 100 100 Sample: BH4-10 Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 B'romoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5 • Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 • 1,2-Dichlorobenzene 95-50-1 ND 5 1,3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 1,1-Dichloroethane 75-34-3 ND 5 1,2-Dichloroethane 107-06-2 ND 5 1,1-Dichloroethene 75-35-4 ND 5 1,2-Dichloroethene, total 540-59-0 ND 5 • 1,2-Dichloroppropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 ND 50 Stvrene 100-42-5 ND 5 • 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • �a +rvuen v»o 3249 Fitzgerald Road•Rancho Cordova.CA 95742•Fox(916)638-4510•(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DORS ELAP Atereditat Ion/Reg iatrat ion Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-19A Date Extracted: 03/19/92 Batch No. : 8944 Date Analyzed: 03/19/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH4-10 • Sample: BH4-10(cont.) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 1,1,1-Trichloroethane 71-55-6 ND 5 • 1,1,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5 Trichlorofluoromethane 75-69-4 ND 5 1, 1,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes, total 1330-20-7 ND 10 • ND .- Not detected at or above indicated Reporting Limit Rep. Limit - Reporting Limit unless otherwise indicated in parentheses. • • Y • • 9s +n.0[uvwo 3249 Fitzgerald Road•poncho Cordova.CA 95742•Fox(916)638-4510•(916(638-7301 • AMERICAN ENVIRONMENTAL LAEORATORIE$COP0. CA DOHS ELAP Accreditation/Registration Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Wap Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Lo No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-20A Date Extracted: 03/19/92 Batch No. : 8944 Date Analyzed: 03/19/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH4-15 • SURROGATE Surrogate Surr Conc. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 108 • Toluene-d8 N/A 100 102 p-Bromofluorobenzene 460-00-4 100 98 Sample: BH4-15 Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5 • Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 • 1,2-Dichlorobenzene 95-50-1 ND 5 13-Dichlorobenzene 541-73-1 ND 5 1,,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 1, 1-Dichloroethane 75-34-3 ND 5 1,2-Dichloroethane 107-06-2 ND 5 1,1-Dichloroethene 75-35-4 ND 5 1,2-Dichloroethene, total 540-59-0 ND 5 1,2-Dichloropropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1,3•Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-73-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 ND 50 Styrene 100-42-5 ND 5 • 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachlozoethene 127-18-4 ND 5 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses, • & 3249 Fit[gercd Roaa•Rancho Cordova.CA 95742•Fax(916)638-4510•(916)6387301 • AMERICAN ENVIRONMENTAL LABORATORIES COR0. CA DOHS ELAP Accreditation/Regia trat ion Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-20A Date Extracted: 03/19/92 Batch No. : 8944 Date Analyzed: 03/19/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH4-15 • Sample: BH4-15(cont.) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 1,1,1-Trichloroethane 71-55-6 ND 5 ,• 1,1,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5 Trichlorofluoromethane 75-69-4 ND 5 1,1,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes, total 1330-20-7 ND 10 • ND - Not detected at or above indicated Reporting Limit Rep. Limit - Reporting Limit unless otherwise indicated in parentheses. y • s • +namvw+ 3249 fingerad Road•Ronoho Cordova,CA 95742•Fox(916(638-4510•(9161 o.384301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOES ELAP AncredLtatlon/Reg Latration Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Wap Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Extracted: 03/19/92 COC Log No. : 24918 - 24920 Date Analyzed: 03/19/92 AELC ID No. : L8465 Date Reported: 03/29/92 Batch No. : 8944 Matrix: SOIL MS SURROGATE • MS MS Surr. Surrogate Conc. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 109 Toluene-d8 N/A 100 102 • p-Bromofluorobenzene 460-00-4 100 98 MATRIX SPIKE MS MS Conc. Recovery Analyte CAS No. (ug/kg) (percent) • Benzene 71-43-2 50 122 Chlorobenzene 108-90-7 50 100 I,1-Dichloroethene 75-35-4 50 113 Toluene 108-88-3 50 119 Trichloroethene 79-01-6 50 104 MSD SURROGATE • MSD Surr. Surrogate Conc. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 110 • Toluene-d8 N/A 100 101 p-Bromofluorobenzene 460-00-4 100 97 MATRIX SPIKE DUPLICATE MSD MSD Conc. Recovery Analyte CAS No. (ug/kg) (percent) • Benzene 71-43-2 50 106 I Chlorobenzene 108-90-7 50 91 I, I-Dichloroethene 75-35-4 50 98 Toluene 108-88-3 50 103 Trichloroethene 79-01-6 50 90 1 • 6$....am'. 3249 Fikgerold Road•Roncno Cordova.CA 95742•Fax(916)638-4510•(916)638-7301 • AMERICAN ENVIRONMENTAL LA®ORATORIES CORP. to D098 ELAP Accreditation/Registration Number 1233 Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 • Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Extracted: 03/19/92 COC Log No. : 24918 - 24920 Date Analyzed: 03/19/92 AELC ID No. : L8465 Date Reported: 03/29/92 Batch No. : 8944 Matrix: SOIL RELATIVE $ DIFFERENCE • Relative Percent Difference Analyte CAS No. (percent) Benzene 71-43-2 14 Chlorobenzene 108-90-7 9 • 1,1-Dichloroethene 75-35-4 14 Toluene 108-88-3 14 Trichloroethene 79-01-6 14 • • • • • 4 vinnluomn 3249 Fitzgerald Road•Rancho Cordova.CA 95742•Fox 1916)638-4510•(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DONS SLAP AetreditationlRegiatration N=ber 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Reported: 03/31/92 AELCLLog C ID No. : 28465 24920 Batch No. : 8944 Matrix: SOIL LAB CONTROL STANDARD • LCS LCS Conc. Recovery Analyte CAS No. (ug/L) (percent) Benzene 71-43-2 50 101 Chlorobenzene 108-90-7 50 90 1,1-Dichloroethene 75-35-4 50 92 Toluene 108-88-3 50 97 Trichloroethene 79-01-6 50 91 • • • • Je +,;.uxo•wo 3249 Fitzgerald Road•Rancnc Cordova.CA 95742•Fox(916)638-4510•(916)638-7301 • AMERICAN eNVIgONMHE LABI ClQ1E5 COriP. CA DOHS FLAP Accreditation/Reglatration Number 1233 Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 • Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Extracted: 03/20/92 COC Log No. : 24918 - 24920 Date Analyzed: 03/20/92 AELC ID No. : L8465 Date Reported: 03/29/92 Batch No. : 8945 Matrix: SOIL MB SURROGATE • MB Surrogate Surr Conc. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 104 Toluene-d8 N/A 100 101 • p-Bromofluorobenzene 460-00-4 100 95 METHOD BLANK Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5 Carbon tetrachloride 56-23-5 ND 5 • Chlorobenzene 108-90-7 ND 5 Chloroethane 75-0.0-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND LO Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 1,2-Dichlorobenzene 95-50-1 ND 5 • 1,3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 11-Dichloroethane 75-34-3 ND 5 1,,2-Dichloroethane 107-06-2 ND 5 1, 1-Dichloroethene 75-35-4 ND 5 1,2-Dichloroethene, total 540-59-0 ND 5 1,2-Dichloropropane 78-87-5 ND 5 cis-1, 3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 ND 50 Styrene 100-42-5 ND 5 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 • Tetrachloroethene 127-18-4 ND 5 Toluene 108-88-3 ND 5 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • 14 3249 Fitzgerald Roatl•Rcncho Cordova.CA 95742-Fox(916)638-4510-(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA OOHS ELAP ACCrldLtati.af RlgiltratL.. Nw ber 1233 Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 • Client: &EMC Boatman Project No. : 6409 10960 Boatman Wap Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Extracted: 03/20/92 COC Log No. : 24918 - 24920 Date Analyzed: 03/20/92 AELC ID No. : L8465 Date Reported: 03/29/92 Batch No. : 8945 Matrix: SOIL METHOD BLANK(cont.) • Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) 1,1,1-Trichloroethane 71-55-6 ND 5 1,1,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5 Trichlorofluoromethane 75-69-4 ND 5 • 1,1,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Viriyl chloride 75-01-4 ND 10 Xylenes, total 1330-20-7 ND . 10 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • • • • • • cron lu o•w+ 3249 Filzgercid Road•Rancho Cordava,CA 95742•Fax(916)638.4510•(916)638-7301 • AMEENVIAONMENTALRICAAIES N U DOHS FLAP AccredLtat Lon/Reg Lscrat Lan Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Wap Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-21A Date Extracted: 03/20/92 Batch No. : 8945 Date Analyzed: 03/20/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BHS-5 • SURROGATE Surrogate Surr Conc. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 105 • Toluene-d8 N/A 100 100 p-Bromofluorobenzene 460-00-4 100 97 Sample: BH3-5 Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5 • Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 • 1,2-Dichlorobenzene 95-50-1 ND 5 1,3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 1,1-Dichloroethane 75-34-3 ND 5 1,2-Dichloroethane 107-06-2 ND 5 1,1-Dichloroethene 75-35-4 ND 5 1,2-Dichloroethene, total 540-59-0 ND 5 • 12-Dichloropropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 ND 50 Styrene 100-42-5 ND 5 • 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • �' xnaeo v.nc 3249 Fitzgerald Road-Rancho Cordova.CA 95742•Fat(916)638-4510•(916)638-7301 • AMERICAN ENVIRONMlE LABOAATOFIES CORP. CA OOHS ELAP ACLredltationlRegiftrat Lon Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-21A Date Extracted: 03/20/92 Batch No. : 8945 Date Analyzed: 03/20;92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH3-5 • Sample: BH3-5(cont.) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 1,1,1-Trichloroethane 71-55-6 ND 5 • 1,1,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 NO 5 Trichlorofluoromethane 75-69-4 ND 5 1,1,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes, total 1330-20-7 ND 10 • ND - Not detected at or above indicated ReportingLimit step. Limit - Reporting Limit unless otherwise inicated in parentheses . • • • • • am^i to arca 3249 Fltpgerald Rood•Poncho Cordovo.CA 95742•Fax(916)6384510•(916)638-7301 • AMERICAN ENVIRONMENTAL LAEORATORIEE CORD. CA DOHS ELAP Accredttatlon/Raglscraclen Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Wap Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-22A Date Extracted: 03/20/92 Batch No. : 8945 Date Analyzed: 03/20/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH3-10 • SURROGATE Surrogate Surr Conc. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 109 • Toluene-d8 N/A 100 101 p=Bromofluorobenzene 460-00-4 100 96 Sample: BH3-10 Results Rep, Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5 • Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 • 1,2-Dichlorobenzene 95-50-1 ND 5 1,3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 1, 1-Dichloroethane 75-34-3 ND 5 1,2-Dichloroethane 107-06-2 ND 5 1,1-Dichloroethene 75-35-4 ND 5 1,2-Dichloroethene, total 540-59-0 ND 5 1,2-Dichloroppropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 ND 50 Stvrene 100-42-5 ND 5 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • 3$ o,oma,wc 3249 Fitzgerati Road•Rancno Cordova,CA 95742•For(916)638-4510-(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOHS SLAP Accredltat ion/Regietret Lon Number 1233 • Analysis Report: Volatile organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-22A Date Extracted: 03/20/92 Batch No. : 8945 Date Analyzed: 03/20/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH3-10 • Sample: BH3-10(cont.) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 1,1,1-Trichloroethane 71-55-6 ND 5 • 1,1,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5 Trichlorofluoromethane 75-69-4 ND 5 1i1,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vnyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes, total 1330-20-7 ND 10 • ND a Not detected at or above indicated Reporting Limit Rep. Limit - Reporting Limit unless otherwise indicated in parentheses. • • • • 0$ urn to c,nc 3249 Fitzgerotd Road•Rancho Cordova,CA 95742•Fox(916)638-4510•(916)638-7301 • AMERICAN ENVIRONMENTAL t.ABOAATORIES COfiR CA DOHS ELAP Accreditation/Aegiatration N.ber 1233 Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Wap Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-23A Date Extracted: 03/20/92 Batch No. : 8945 Date Analyzed: 03/20/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH3-15 SURROGATE Surrogate Surr Conc. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 105 Toluene-d8 N/A 100 102 p-Bromofluorobenzene 460-00-4 100 101 Sample: BH3-15 Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5 Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 1,2-Dichlorobenzene 95-50-1 ND 5 1,3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 1,1-Dichloroethane 75-34-3 ND 5 1,2-Dichloroethane 107-06-2 ND 5 1,1-Dichloroethene 75-35-4 ND 5 1,2-Dichloroethene, total 540-59-0 ND 5 1,2-Dichloroppropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1, 3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 ND 50 Styrene 100-42-5 ND 5 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 ND a Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise inicated in parentheses. . min naw 3249 Fitzgerald Rood•Ramno Cordova,CA 95742•Fax(916)638-4510'(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOES SLAP Accreditation/Registration Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Waq Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Proj.ect: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-23A Date Extracted: 03/20/92 Batch No. : 8945 Date Analyzed: 03/20/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH3-15 • Sample: BH3-15(cont.) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 1,1,1-Trichloroethane 71-55-6 ND 5 1,1,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5 Trichlorofluoromethane 75-69-4 ND 5 1,1,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes, total 1330-20-7 ND 10 • ND — Not detected at or above indicated Reporting Limit Rep. Limit a Reporting Limit unless otherwise indicated in parentheses. • • • ui.raim r.nx 3249 Fitzgerald Rodd•Rancho Cordova,CA 95742•Fax(916)638-4510•(916)o38-1301 • AMERICAN ENVIRONMENTAL LABORATORIES CORK CA DORS ELAP AoeredLtatioalRegistration Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-24A Date Extracted: 03/20/92 Batch No. : 8945 Date Analyzed: 03/20/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH2-5 • SURROGATE Surrogate Surr Conc. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 109 • Toluene-d8 N/A 100 101 p-Bromofluorobenzene' 460-00-4 100 97 Sample: BH2-5 Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5 • Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 • 1,2-Dichlorobenzene 95-50-1 ND 5 1,3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 11-Dichloroethane 75-34-3 ND 5 1,,2-Dichloroethane 107-06-2 ND 5 1,1-Dichloroethene 75-35-4 ND 5 1,2-Dichloroethene, total 540-59-0 ND 5 • 1,2-Dichloropropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 ND 50 Styrene 100-42-5 ND 5 • 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 ND - Not detected at or above indicated Reporting Limit Rep. Limit - Reporting Limit unless otherwise indicated in parentheses. • c,nnmowo 3249 Fih9ercid Road•Rancho Cordova.CA 95742•Fox(916)638-4510•(916)638-7301 AMERICAN ENVIRONMENTALLABORATORIES CORP. CA DOHS ELAP At9red1tat Lon/Resietrat ion Number 1233 Analysis Report: Volatile Organic Compounds by CC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-24A Date Extracted: 03/20/92 Batch No. : 8945 Date Analyzed: 03/20/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH2-5 Sample: BH2-5(cont. ) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 1,1,1-Trichloroethane 71-55-6 ND 5 1,1,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5 Trichlorofluoromethane 75-69-4 ND 5 1,1,2-Trichlorotrifluoroethane 79-13-1 NO 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes, total 1330-20-7 ND 10 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. 0$ m•.m rwe 3249 Fingercid Rootl•Rancho Cordov .CA 95742•cax(916(638-L510•(916)638-7301 • AMERICAN ENVIRONMENTAL LA®ORATORIES CORP. CA D095 ELAF Accr.dltatian/Registratian N=ber 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 CCC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-25A Date Extracted: 03/20/92 Batch No. : 8945 Date Analyzed: 03/20'/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH2-10 • SURROGATE Surrogate Surr Conc. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 109 • Toluene-d8 N/A 100 102 p-Bromofluorobenzene 460-00-4 100 97 Sample: BH2-10 Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5 Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 1,2-Dichlorobenzene 95-50-1 ND 5 1,3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 1, 1-Dichloroethane 75-34-3 ND 5 1,2-Dichloroethane 107-06-2 ND 5 1,1-Dichloroethene 75-35-4 ND 5 1,2-Dichloroethene, total 540-59-0 ND 5 • 1,2-Dichloroppropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 ND 50 Styren; 100-42-5 ND 5 • 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 ND - Not detected at or above indicated Reporting Limit Rep. Limit - Reporting Limit unless otherwise in in parentheses. 9$ WIMIIwn 3249 Fitzgerolo Rood•Roncno Cordova.CA 95742-Fox(916)638-4510•(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DORS FLAP Accreditation/Registration Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Wap Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 COC Lo No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-25A Date Extracted: 03/20/92 Batch No. : 8945 Date Analyzed: 03/20/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH2-10 • Sample: BH2-10(cont.) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 1,1, 1-Trichloroethane 71-55-6 ND 5 • 1, 1,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5 Trichlorofluoromethane 75-69-4 ND 5 1,1,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes, total 1330-20-7 ND 10 • ND s Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. • • • • • "� +rrito.+.•a 3249 Fitzgerald Road•Rancho Cordova.CA 95742•Fax(916(638-4510•(916(638-7301 • AMERICAN eCORP. CA DOHS EI.AY Accred Ltation/Reglatrat Lon Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC BoatmanProject No. : 6409 Stanton, CAa90680 qq Contact: Kevin Sheridan Phone: (714) 826-6320 Project: Solag - San Juan - AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-26A Date Extracted: 03/20/92 Batch No. : 8945 Date Analyzed: 03/2C/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH2-15 • SURROGATE Surrogate Surr Conc. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 108 ,• Toluene-d8 N/A 100 103 p-Bromofluorobenzene 460-00-4 100 99 Sample: BH2-15 Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5 Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 • 1,2-Dichlorobenzene 95-50-1 ND 5 1,3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 1,1-Dichloroethane 75-34-3 ND 5 1 2-Dichloroethane 107-06-2 ND 5 1,1-Dichloroethene 75-35-4 ND 5 1,2-Dichloroethene, total 540-59-0 ND 5 • 1,2-Dichloropropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 ND 50 Styrene 100-42-5 ND 5 • 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 ND - Not detected at or above indicated Reporting Limit Rep. Limit - Reporting Limit unless otherwise indicated in parentheses. • fie° .r.r„o ren. 3249 Fittgerold Road-Ron r o Cordova.CA 95742•Fox 1916)638-4510•(916)o38-7301 AMERICAN ENVIRONMENTAL LAEORATORIES CORA CA DOHS ELAP Accreditation/Registration Number 1233 Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Wap Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-26A Date Extracted: 03/20/92 Batch No. : 8945 Date Analyzed: 03/2C/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BH2-15 Sample: BH2-15(cont.) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 1,1,1-Trichloroethane 71-55-6 ND 5 1, 1,2-Trichloroethane 79-00-5 NO 5 Trichloroethene 79-01-6 ND 5 Trichlorofluoromethane 75-69-4 ND 5 111,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes , total 1330-20-7 ND 10 NO - Not detected at or above indicated Reporting Limit Rep. Limit - Reporting Limit unless otherwise indicated in parentheses . 3249 Mzgero)d Rood•Roncno Cordon,CA 95742•Fox(916)6384510•(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DORS ELAP AeereditatIon/Regiatration Umber 1233 Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Wap Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 COC Lo No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-27A Date Extracted: 03/20/92 Batch No. : 8945 Date Analyzed: 03/20/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BHI-5 SURROGATE Surrogate Surr Conc. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 104 Toluene-d8 N/A 100 102 p-Bromofluorobenzene 460-00-4 100 100 Sample: BHI-5 Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 . Carbon disulfide 75-15-0 ND 5 Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethvl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 1,2-Dichlorobenzene 95-50-1 ND 5 1,3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 NO 5 Dichlorodifluoromethane 75-71-8 ND 10 1,1-Dichloroethane 75-34-3 ND 5 12-Dichloroethane 107-06-2 ND 5 1,,1-Dichloroethene 75-35-4 ND 5 • 1,2-Dichloroethene, total 540-59-0 ND 5 1,2-Dichloropropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 ND 50 • Styrene 100-42-5 NO 5 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 NO — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses, 29 3249 Fitoerald Road•Rancho Cordo%,a,CA 95742•Fox(916)638-4510•(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORK CA DOHS ELAP Accreditation/Registration N=ber 1233 Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ZD No. : L8465-27A Date Extracted: 03/20/92 Batch No. : 8945 Date Analyzed: 03/20/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BHI-5 • Sample: BHI-5(cont. ) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 ' 1,1,1-Trichloroethane 71-55-6 ND 5 1,1,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5 Trichlorofluoromethane 75-69-4 ND 5 1,1,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes, total 1330-20-7 ND 10 • ND m Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses . • • • • • sy +a,nno,n. 3249 Fitzgerald Road•Poncho Cordova.CA 95742•Fox(916)638-4510•(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA D095 ELAP AccrediteticnlRegiatr.t ion Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-28A Date Extracted: 03/20/92 Batch No. : 8945 Date Analyzed: 03/20'/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BHI-10 • SURROGATE Surrogate Surr Conc. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 105 • Toluene-d8 N/A 100 102 p-Bromofluorobenzene 460-00-4 100 99 Sample: BHI-10 Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5 • Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene 108-90-7 ND 5 Chloroethane 75-00-3 ND 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 NO 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 '• 1,2-Dichlorobenzene 95-50-1 NO 5 1,3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 NO 10 1,1-Dichloroethane 75-34-3 NO 5 1,2-Dichloroethane 107-06-2 ND 5 1,1-Dichloroethene 75-35-4 ND 5 1,2-Dichloroethene, total 540-59-0 NO 5 • 1,2-Dichloropropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 NO 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 t 2-Hexanone 591-78-6 NO 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 ND 50 Styrene 100-42-5 ND 5 • 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 NO 5 ND - Not detected at or above indicated Reporting Limit Rep. Limit - Reporting Limit unless otherwise indicated in parentheses. • & 3249 fingercol Road•Rancno Cordova,CA 95742•faa(916)638-4510•(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA D095 FLAP Accreditation/Registration Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-28A Date Extracted: 03/20/92 Batch No. : 8945 Date Analyzed: 03/2G/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BHI-10 • Sample: BHI-10(cont.) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 1,1,1-Trichloroethane 71-55-6 ND 5 • 1,1,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5 Trichlorofluoromethane 75-69-4 NO 5 1,1,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes, total 1330-20-7 ND 10 • ND — Not detected at or above indicated Reporting Limit Rep. Limit Reporting Limit unless otherwise indicated in parentheses. • • • • • 4 ulr,iiEo rn+ 3249 Fitzgerald Rood•ROnCho COfdOVO.CA 95742-Fax(916)638-4510•(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOHS ELAP Accreditation/Resistration Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Wap Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465-29A Date Extracted: 03/20/92 Batch No. : 8945 Date Analyzed: 03/20%92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BHI-15 • SURROGATE Surrogate Surr Conc. Recovery Analyte CAS No. (ug/kg) (percent) • 1,2-Dichloroethane-d4 N/A 100 102 Toluene-d8 N/A 100 103 p-Bromofluorobenzene 460-00-4 100 97 Sample: BH1-15 Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) • Acetone 67-64-1 ND 100 Benzene 71-43-2 ND 5 Bromodichloromethane 75-27-4 ND 5 Bromoform 75-25-2 ND 5 Bromomethane 74-83-9 ND 10 2-Butanone 78-93-3 ND 100 Carbon disulfide 75-15-0 ND 5 • Carbon tetrachloride 56-23-5 ND 5 Chlorobenzene - 108-90-7 ND 5 Chloroethane 75-00-3 NO 10 2-Chloroethyl vinyl ether 110-75-8 ND 50 Chloroform 67-66-3 ND 5 Chloromethane 74-87-3 ND 10 Dibromochloromethane 124-48-1 ND 5 Dibromomethane 74-95-3 ND 5 • 1,2-Dichlorobenzene 95-50-1 ND 5 1,3-Dichlorobenzene 541-73-1 ND 5 1,4-Dichlorobenzene 106-46-7 ND 5 Dichlorodifluoromethane 75-71-8 ND 10 1,1-Dichloroethane 75-34-3 ND 5 1,2-Dichloroethane 107-06-2 ND 5 1,1-Dichloroethene 75-35-4 ND 5 1,2-Dichloroethene, total 540-59-0 ND 5 • 12-Dichloropropane 78-87-5 ND 5 cis-1,3-Dichloropropene 10061-01-5 ND 5 trans-1,3-Dichloropropene 10061-02-6 ND 5 Ethylbenzene 100-41-4 ND 5 2-Hexanone 591-78-6 ND 50 Methylene chloride 75-09-2 ND 5 4-Methyl-2-pentanone 108-10-1 ND 50 Styrene 100-42-5 ND 5 • 1,1,2,2-Tetrachloroethane 79-34-5 ND 5 Tetrachloroethene 127-18-4 ND 5 ND — Not detected at or above indicated Reporting Limit Rep. Limit — Reporting Limit unless otherwise indicated in parentheses. &v,rm m e,wn 3249 FlhgerG4 Pond•Rancho Cordova.CA 95742•For(9161638-4510-(916(638-7301 • �������� ENVIRONMENTAL LABOFATOrilES CO�P. CA DOES ELAP Accreditation/Registration Member 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Lo No. : 24918 - 24920 Date Received: 03/13/92 AELC 19 No. : L8465-29A Date Extracted: 03/20/92 Batch No. : 8945 Date Analyzed: 03/20/92 Matrix: SOIL Date Reported: 03/29/92 Client ID No. : BHI-15 • Sample: BH1-15(cont. ) Results Rep. Limit Analyte CAS No. (ug/kg) (ug/kg) Toluene 108-88-3 ND 5 1,1,1-Trichloroethane 71-55-6 ND 5 • 1,1,2-Trichloroethane 79-00-5 ND 5 Trichloroethene 79-01-6 ND 5 Trichlorofluoromethane 75-69-4 ND 5 1,1,2-Trichlorotrifluoroethane 79-13-1 ND 5 Vinyl acetate 108-05-4 ND 50 Vinyl chloride 75-01-4 ND 10 Xylenes, total 1330-20-7 ND 10 • ND — Not detected at or above indicated Reporting Limit Rep. Limit a Reporting Limit unless otherwise indicated in parentheses . • • • t • wrrmtw.na 3249 FI&geraid Road•Rancho Cordon.CA 95742•Fax(916)638-4510•(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATORIES CORP. CA DOES ELAP ACCreditation)Registration Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Extracted: 03/20/92 COC Log No. : 24918 - 24920 Date Analyzed: 03/20/92 AELC ID No. : L8465 Date Reported: 03/29/92 Batch No. : 8945 Matrix: SOIL MS SURROGATE • MS MS Surr. Surrogate Cone. Recovery Analyte CAS No. (ug/kg) (percent) 1,2-Dichloroethane-d4 N/A 100 106 Toluene-d8 N/A 100 102 p-Bromofluorobenzene 460-00-4 100 99 MATRIX SPIKE MS MS Cone. Recovery Analyte CAS No. (ug/kg) (percent) • Benzene 71-43-2 50 122 Chlorobenzene 108-90-7 50 105 1,1-Dichloroethene 75-35-4 50 114 Toluene 108-88-3 50 117 Trichloroethene 79-01-6 50 102 • MSD SURROGATE MSD Surr. Surrogate Cone. Recovery Analyte CAS No. (ug/kg) (percent) • 1,2-Dichloroethane-d4 N/A 100 106 Toluene-d8 N/A 100 102 p-Bromofluorobenzene 460-00-4 100 98 MATRIX SPIKE DUPLICATE MSD MSD Cone. Recovery Analyte CAS No. (ug/kg) (percent) Benzene 71-43-2 50 124 Chlorobenzene 108-90-7 50 108 1,1-Dichloroethene 75-35-4 50 116 Toluene 108-88-3 50 121 Trichloroethene 79-01-6 50 104 tl$ wr.auov.wc 3249 Fitlgefaid Rand•RanChO Cordova,CA 95742•Fox(916)638-4510•19161 638-7301 • AMERICAN ENVIRONMENTAL LABOriATORIES COriR CA DONS ELAP Accreditation/Reg ietrat ion Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Extracted: 03/20/92 CCC Lo No. : 24918 - 24920 Date Analyzed: 03/20/92 AELC ID No. : L8465 Date Reported: 03/29/92 Batch No. : 8945 Matrix: SOIL RELATIVE % DIFFERENCE • Relative Percent Difference Analyte CAS No. (percent) Benzene 71-43-2 2 Chlorobenzene 108-90-7 3 • 1,1-Dichloroethene 75-35-4 2 Toluene 108-88-3 3 Trichloroethene 79-01-6 2 • • ;• i ,• '• • i$,¢rtuown, 3249 Fitzgerald Road•Rancho CORIO ,C4 95742•far(916)638-4510•(916)638-7301 • AMERICAN ENVIRONMENTAL LABORATO gIES CORP. CA DOHS ELAP Accreditation/Registration Number 1233 • Analysis Report: Volatile Organic Compounds by GC/MS, EPA Method 8240 Client: AEMC Boatman Project No. : 6409 10960 Boatman Wap Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt • Job No. : 6409 Date Reported: 03/31/92 COC Log No. : 24918 - 24920 AELC ID No. : L8465 Batch No. : 8945 Matrix: SOIL IAB CONTROL STANDARD • LCS LCS Conc. Recovery Analyte CAS No. (ug/L) (percent) Benzene 71-43-2 50 101 Chlorobenzene 108-90-7 50 90 • 1, 1-Dichloroethene 75-35-4 50 92 Toluene 108-88-3 50 97 Trichloroethene 79-01-6 50 91 • • • • ae.a m.w a 3249 Fitzgerald Rood•Rancno Cordova,CA 95742•fox(916)638-4510•(916)638-7301 ' PRELIMINARY SITE ASSESSMENT REPORT t For SOI-AG DISPOSAL MAINTENANCE YARD tLocated At 31931 Paseo Adelanto ' San ,Tuan Capistrano, California 1 1 1 1 t • AMERICAN EP nAONMENTAL LABORATORIES CORM G DOE, AP Accreditation/Registration Number 1233 • Analysis Report: pH, EPA Meti.od 9045 Client: AEMC Boatman Project No. : 6409 10960 Boatman Way Contact: Kevin Sheridan Stanton, CA 90680 Phone: (714) 826-6320 Project: Solag - San Juan AELC Contact: John Arndt Job No. : 6409 • Date Sampled: 03/12/92 COC Log No. : 24918 - 24920 Date Received: 03/13/92 AELC ID No. : L8465 Date Prepared: 03/17/92 Batch No. : 53683 Date Analyzed: 03/17,/92 Matrix: SOIL Date Reported: 03/29/92 • MEASUREMENT Sample I.D. pH Client AELC (Standard Units) BH10-5 IA 7.8 BH9-5 4A 7.5 • BH8-5 7A 7.9 BH7-5 10A 7.6 BH6-5 12A 8. 7 BH5-5 15A 8.6 • BH4-5 18A 8.7 BH3-5 21A 8.5 BH2-5 24A 8.7 BH1-5 27A 7.9 • • • • • a WICUoaax 3249 FiRgero)d Rood•Rancho Cordova-CA 95742•Fax(916)638-4510•(916)638-7301 1 1 PRELIMINARY SITE ASSESSMENT REPORT 1 For 1 SOLAG DISPOSAL MAINTENANCE YARD 1 Located At j 1 31731 Paseo Adelanto San Juan Capistrano, California 1 1 June 19, 1991 1 Prepared for 1 SOLAG DISPOSAL P.O. Box 1100 San Juan Capistrano, CA 92693 1 Prepared By 1 HEKIMIAN & ASSOCIATES, INC. 1 16692 Gothard Street Huntington Beach, California 92647 1 (714) 84 1 FbQ, Leslie R. Anderson 1 M.A., Urb. & Reg. Planning Project Manager 1 Kenneth K. Hekimian, Ph.D., P.E. President, Quality Control Review ' FILE NO. 1744SP ' PRELIMINARY SITE ASSESSMENT REPORT FOR SOLAG DISPOSAL MAINTENANCE YARD Located At 31731 Paseo Adelanto ' San Juan Capistrano, California Reference: (1) Proposal for Property Transfer or Loan Preliminary Site Assessment for property located at 31731 Paseo Adelanto, San Juan Capistrano, California. INTRODUCTION This letter report presents a summary of the activities and the results of the Preliminary Environmental Assessment performed by Hekimian & Associates, Inc. for the subject property illustrated in Figure 1. This assessment was requested by Solag Disposal, Inc., and generally follows the financial institution guidelines for a Phase I Environmental Risk ' Report. PURPOSE AND SCOPE ' The purpose of this investigation was to determine if there exists any significant surface or subsurface property contamination by hazardous and toxic substances that could constitute a potential liability for the property owner or lessee. The Preliminary Site Assessment includes the following activities and research: 1 1. Historical survey of former land uses and development with emphasis on possible use and/or storage of hazardous materials and/or waste (business licenses, constructions permits and drawings, aerial photography, etc.) ' 2. Search of official records for possible hazardous materials spills, use/storage violations (fire department, Health Department). 3. Review of official records regarding adjacent properties hazardous materials spills or leaks that could have affected subject property (industrial plants, ' service stations, etc.). ' 4. Preparation of site sketch showing existing property boundaries and improvements, and locations for storage and/or use of hazardous materials ' and/or waste, if any. 1 ' TABLE OF CONTENTS Paee ' INTRODUCTION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 ' PURPOSE AND SCOPE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 ACTIVITIES CARRIED OUT . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 ' SITE DESCRIPTION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 ' SURROUNDING PROPERTIES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 HISTORY OF SPILLS AND VIOLATIONS IN THE VICINITY . . . . . . . . . . 6 ' HYDROLOGY . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9 RESULTS AND CONCLUSIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9 ' DISCLAIMER . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11 ' SOURCE LIST . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12 LIST OF FIGURES Figure 1. Site Location Map . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2 Figure 2. Site Plan . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 Figure 3. Vicinity Development 7 APPENDICES ' Appendix I - O.C.F.D. Chemical Inventory Disclosure Statement Appendix II City of San Juan Capistrano Building Permits. Appendix III - Orange County Health Care Agency Subject Property UST Records. 1 ceryl I ^ cA Iu a Area of significant facility invesdgation: 1 square mile SAN W v ' PA ASL \SWv AGATE ESP 0� ' Ep SANtA C 9 ANp ? z0 0��� 5 N GA > Z N �P Cl�E\SP vnA G „ Z ' J Q p C9 Area of investigation: 1000 feet radius r� )A N AZ ST Q P Ti TP c4((FpNQ /SS (p AS N AN J pa �G O STS ,, CAPI T NO6 r �P ROgE 4P� 0 5 y I SPRIN \ Z ' F(,, c/ RTO Q 9j\ AM RAK �T_ 7� CS `OBOE A v4 J� STA SITE LOCATION puGO T 0� O' ESeP P 5 PPA ORA/ 9 n 4 E ORB��tt 7 PA 1� � ODC4 ( F R 801 n L v2 > J DEL D 3;ac0<<F n LIBRARY ti q, O O:;Ci a .F,y�•,cl' p �f>� tiONq 5 � p ISPO OFC 4s 4 J`P Oe C; Z r0 f d1 5 F►IyIRpEgSTA. V '°fPO P M�sCo jPLy�gH 2Qt 8 O9r P.O. '�ZQi �LONDRINA Q �vpq.34F, CL AVE DATA 2Of 5t n Q Q ,\ I J O fAL aN l FQOV IL 2 lV €E. CA PADRE j JQ �Li y,�C ' ,.$CANOEPA& ESTACZ 9 �. HEKIMIAN & ASSOCIATES, I 16571 Gemini Lane ' Huntington Beach,CA 92647 (714)841-6298 CONSULTING ENGINEERS AND ENVIRONMENTAL PLANNERS FAX(714)948.2603 SCALE: 1"=10001 APPROVED BY: DRAWN BY MP ' nN DATE: 6-13-91 REVISED SOLAG DISPOSAL MAINTENANCE YARD 31731 Paseo Adelanto, San Juan Capistrano, California DRAWING NUMBER SITE LOCATION MAP Figure 1 1 5. If former or present hazardous materials were or are present, determine approximate depth of groundwater in area and approximate groundwater flow direction, to extent available. ' 6. Preparation of a summary report indicating the investigation done, sources of information, data obtained and interpretation of data regarding identified or possible site contamination. 1 ACTIVITIES CARRIED OUT Historical background on the property was traced by review of occupancy, building and talteration permits, and historical aerial photography that show improvements on the lot. Surrounding property conditions and history were obtained from the same sources and ' particularly the City of San Juan Capistrano Zoning and Planning Department concerning historic and future development in the general vicinity. The Orange County Health Care Agency and the San Diego Regional Water Quality Control Board were checked for records of violations or spills of hazardous materials that would affect the subject site. The following regulatory agency lists were reviewed: EPA: CERCLIS; DHS: BEP, Cortese, ' ASPIS; SDRWQCB: LUSTIS; California Waste Management Board Active Landfills. An inspection of the subject property was performed concerning facilities, activities, storage ' and use of hazardous materials and substances. Adjacent properties and land uses were surveyed regarding possible use or storage of hazardous materials that might impact the subject site. 1 ' SITE DESCRIPTION The property illustrated in Figure 2 and located at the northernmost end of Paseo ' Adelanto is a solid waste (refuse) removal company's storage and maintenance yard. The site consists of two adjacent, fenced and unpaved parcels. The western parcel is occupied by the employee parking and by the vehicle maintenance area, while the eastern parcel is ' mainly occupied by various trash dumpsters. The property is bounded by a vacant field and a single family residence at the north, by single family residences at the east, by vehicle storage yards at the south, and by the Trabuco Creek at the west. ' The site is an irregularly-shaped lot which occupies parcels six and nine of block 143 in the City of San Juan Capistrano, County of Orange, State of California, as per map recorded ' in book 121, page 14, in the office of the County Assessor of said County. 3 I 6 O TIRE INSTALL AREA MISCELLANEOUS SINGLE IS), GTDRAGE VEHICLE RUBBISH FAMILY ' CONTAINERS MAINTENANCE RESIDENTIAL 9 TRAILERS AREA X X X ,y DUMPSTER RAMP X '�X Qa X X ❑ 13 ❑ C3 C3 A 4L cl ' k x STACKED BINS X D UMPSTERS MP�Y� 1 /l X ' f DIRT LOT Q �0 0 0❑ ❑ ❑ ro a "1 ' FORM DDD x f�x —x EE NCE A X 1� PUBLIC X—�X X' ` ROLLING GATE PARKtN6 y �R 11,0000 GALLON OFFICES PARTS 00 COLLECTION TRUCK STORAGE DUMPSTERS ` FENCE VCHANLINK A.S.T. 7, \ 10.000 GALLON FRESH LUBRICANT ' DIESEL U.ST. FRESH MOTOR OIL O 5m DIESEL A.S.T. O 1,500 GALLON DIESEL HEKIMIAN & ASSOCIATIPS , 1as71cem(oiLaw A.S T. ( NOT USED ) "UrAi ton amxb,CA 9*0 � (714)$41.62/6 p G CONSULTING&KINCOSMD F.(1ry ./. N7'XL PL WNERS 1,1 FAX(714) 2W . ,SCALE: NTS- APPaoVto Br. _ DRAWN er VW.5.' GLOSSARY : DATE: 5/ 14/91 REVISED J.5.7. UNDERGROUND STORAGE 1 The yard, first occupied in the early 1970's and formerly accessed from Los Rios Street at the east, is now accessed from Paseo Adelanto at the west. The western parcel is used for employee parking and for equipment maintenance operations. Along the northern edge of the parcel is a series of converted truck trailers and roll-off containers which are ' used to store equipment replacement parts, various fresh lubricants and solvents, and welding supplies (see Appendix I). The fresh lubricants and solvents are properly stored, ' capped in their original containers. At the time Hekimian & Associates, (HAI) staff visited the site, a few five-gallon pails of waste oil were stored on a small concrete pad outside one of the trailers. The pails were not capped and there was evidence of substantial ' spillage onto the concrete pad which was covered with granulated sorbent. Located nearby is a roll-off dumpster ramp which is used for on-site trash. The ramp was ' constructed in 1983 without a construction permit. The area, formerly used as a waste oil disposal pit, was roughly remediated before the ramp was constructed. ' The area immediately west of the ramp is used to steam clean equipment and vehicles. The ground, topped with crushed rock, shows substantial staining and discoloration. ' Located in the middle of the property is the vehicle maintenance area. The site is paved with concrete and is roofed over by an overhead 25 foot tall steel canopy (see Appendix 1I). Below the canopy are a few more spare parts storage boxes. A Safety Meen-brand ' parts washer is regularly serviced by the manufacturer. Just south of the maintenance area are several roll-off boxes which are used for ' miscellaneous parts storage and office space. ' West of the offices and parts storage area is the fuel and lubricants storage area. On site is one 10,000 gallon underground diesel fuel storage tank. The tank is of single-wall steel construction and it is kept in compliance with regulations by means of testing and inventory ' reconciliation (see appendix III). Within the same area are several above ground storage tanks and drums of diesel, fresh lubricant and waste oils. Except for an unused 1,500 gallon aboveground tank, the other vessels stand within secondary containment pans. The ' ground around this area shows evidence of moderate surface spillage - mainly due to poor product handling practices. ' The eastern parcel is unpaved and is used for equipment and materials storage. The northeastern corner of the property is occupied by overgrown trees and shrubs and ' by miscellaneous rubbish. The southeast corner is occupied by old collection trucks and dumpsters. The rest of the parcel is occupied by stacks of bins and dumpsters. No ' hazardous materials, or trace of it, was identified on this parcel. 1 5 1 A review of the Fairchild aerial photography collection housed at Whittier College showed that the subject property was unimproved land in 1929. The single family residences to the east along Los Rios Street, and Trabuco Creek are clearly visible. The properties adjacent to the north and to the south were also unimproved. None of the frames reviewed revealed any further development. ' The subject property lies in an area of the City of San Juan Capistrano which is part of the Los Rios Historical District and is presently a legally accepted non-conforming use. ' The subject property, along with some adjacent lands is planned to be redeveloped into a community park. ' SURROUNDING PROPERTIES - Illustrated in Figure 3 Immediately south of the subject property is the City of San Juan Capistrano's recreational vehicle storage yard, and a vehicle parking lot which is occupied by Modern Tree Service, a landscape contractor. Further south is Kelly Ware, a concrete paving and masonry construction contractor's yard. Further south is Town Tours's stables, a tourist attraction that offers group hay rides and barbeques. Further south is Ito Nursery, a wholesale and retail plant nursery. Immediately west of the subject property is the Trabuco Creek, a flood control channel. Further west, the area is developed residentially. ' Immediately north of the subject property is a vacant field which, together with the subject property, is planned to be redeveloped into a community park. Further north, past Ramos ' Street, the area is developed residentially. ' Immediately east of the subject property, as shown in Figure 2, are two single family residences and a small parking lot which was formerly used as the subject property's entrance from Los Rios Street. The area along Los Rios Street is developed residentially and constitutes the Los Rios Historical District. The District is listed in the National Historical Places Registry and includes old adobe and wood-framed housing which is particularly representative of early California development. Further east, past the railroad tracks, is the Capistrano train depot. Further east yet is the City's main shopping and tourist district which is composed of several restaurants, souvenir and gift shops. Located at the northeastern corner of Camino Capistrano and Ortega Highway is the San Juan Capistrano Mission and the grounds upon which the City's original pueblo was established. HISTORY OF SPILLS AND CONTAMINATION (illustrated in Figure 1): As described previously, there is one underground and a few aboveground storage tanks ' at the subject site. The underground storage tank is monitored in accord with Orange County Health Care Agency's alternative number five, which mandates inventory reconciliation and tank testing. The records (see Appendix III) indicate that the underground tank has always shown test and gauge results that are well within regulatory 6 i LEGEND: GAJ UUAW I KELLY WARE MASONRY CONSTRUCTION \ CAPISTpi"o 2 MODERN "TREE SERVICE PARKING LOT Nt15510N ISFR. SINGLE ARANO BY RESIN IDENTIAL J Lp 5�� o R-4 uhN P O 2 w 1 / -rpuWST' I DIST SCALE: 0 100 2W 300 400 500 4 P ITO i A NURSERY HEKIMIAN & ASSOCIATES, INC. 16571 tai Lase i - - Huntington Beadi:CA 92647 (711)9/1-00 CONSULTING ENGINEERS AND ENVIR6,W&NTAL PLANNERS FAX(714),i02W L+- I SCALE:AS.S14OWN APPROVtO BY: DRAWN By S. 1 , I Z DATE: f GSI B�gIfl I�',Pl1SAI REVISED ` 1 agency standards. County Health Care Agency records also show that in 1988 and 1989 the site operator was issued a violation for not maintaining adequate tank gauging records ' on site. This sort of violation is of a purely administrative nature and, therefore, does not have a negative environmental impact on the subject property. ' As noted earlier, the subject property displays considerable evidence of fuel and lubricant spills originating from poor maintenance and operation practices. No evidence has been found that any of the tanks and vessels leak. 1 ' Given the type of operations that take place at the subject site, it is presumed that the surface contamination does not extend further than a couple of feet in depth. The exact extent of contamination is to be determined during the second phase of the site assessment. There are a few leaking underground storage tanks cases within a one square mile area ' of the subject property which are handled by the San Diego Regional Water Quality Control Board. These sites are listed below and are indexed on Figure 1. ' 1. Chevron Station #8719: 26988 Ortega Highway, approximately 1800 feet east of the subject property, documented gasoline and waste oil contamination in soil only from leaking underground storage tanks. The tanks have been replaced and the site ' remediated. 2. City of San Juan Capistrano - City Hall: 32400 Paseo Adelanto, approximately 2900 ' feet south of the subject property documented gasoline contamination in soil only from a leaking underground storage tank. The site has been remediated and the case ' closed. 3. Mission Pipe and Supply Co.: 32107 Alipaz Street, approximately 2700 feet southwest ' of the subject property documented gasoline contamination in soil only from a leaking underground storage tank. The site has been remediated. ' 4. Chevron Station: 32009 Camino Capistrano, approximately 1700 feet south of the subject property, documented gasoline contamination of groundwater from a leaking underground storage tank. The tanks have been replaced, and the full extent of ' contamination is being determined. 5. Super - 7/11 Station #2115-18901 (Southland Corporation): 32022 Camino Capistrano, ' approximately 1800 feet south of the subject property, documented gasoline contamination of the groundwater from a leaking underground storage tank. The site ' has been demolished and is currently undergoing remedial action. 8 ' 6. Shell Station: 27101 Ortega Highway, approximately 2600 feet east of the subject property, documented gasoline contamination of groundwater from a leaking ' underground storage tank. The tanks have been replaced and a groundwater treatment system has been put into operation. ' 7. ARCO: 26851 Ortega Highway, approximately 1400 feet east of the subject property has documented gasoline contamination of groundwater from a leaking underground ' storage tank. The case was opened recently, and a preliminary site assessment is underway. HYDROLOGY ' The nearest well of record, according to the Capistrano Valley Water District, is state well number 85/8W-1K2, located on Avenida De La Vista, about 1200 feet north of the subject property. The last reading of groundwater depth was taken on February, 1991 at 17 feet ' below ground elevation. the groundwater flow direction is generally accepted to be to the southwest. RESULTS AND CONCLUSIONS ' Regulatory agencies' official records, land use review and site survey of the subject property and immediately adjacent properties revealed limited use of moderate quantities ' of hazardous materials. ' Most fresh and waste lubricants, and fuels are properly stored in accordance with all applicable regulations, the only exception being a few pails of waste oil which are improperly stored uncapped and outside a secondary containment area. ' Much of the groundsurface in the aboveground fuel and lubricant storage area shows evidence of moderate surface spillage - mainly due to poor product handling practices. The area presently occupied by the roll-off dumpster ramp was formerly used as a hazardous waste dumping pit. The area was reportedly roughly remediated in 1983 before ' the ramp was constructed. The groundsurface in the adjacent steam cleaning area shows substantial staining and discoloration. ' San Diego Regional Water Quality Control Board LUSTIS cases 1, 2 and 3 involve petroleum product contamination in soil only stemming from leaking underground storage tanks. The sources of contamination have been removed and the sites have been remediated. Cases 4, 5, 6 and 7, instead impacted local groundwater also. These cases are closely supervised by the Board and are at various stages of remediation. None of 1 9 1 these cases appears to be of substantial enough gravity or proximity to the subject property to be of environmental concern to it. No "Superfund" case was identified within one square mile of the subject site. ' The information available suggests that closer exploration and sampling be conducted at the points of concern on the subject property. These concerns are to be addressed during the second phase of the subject property's site assessment. 1 1 1 1 10 i DISCLAIMER 1 Hekimian & Associates, Inc. has performed the activities cited herein, solicited and received information and documentation from public agencies and private parties and ' conducted appropriate visitations and observations in accord with generally accepted requirements for a preliminary site assessment of this nature. Interviews were held with representatives of tenants. Information, data, documentation and observations from all ' sources were compared and analyzed in order to reach the results and conclusions delineated above. ' This work has been conducted in an objective and unbiased manner and in accord with generally accepted professional practice for this type of work. Hekimian & Associates, Inc. believes the results and conclusions to be accurate and relevant but cannot accept responsibility for the accuracy or completeness of public documentation or possible withholding of information by interviewees or other private parties. 1 ' /bdv 1 1 1 11 1 SOURCE LIST Public Sector - City of San Juan Capistrano, Community Redevelopment Agency, Subject Site ' Redevelopment Plan. - City of San Juan Capistrano Building Department, Building and Occupancy Permits. ' - City of San Juan Capistrano Planning and Zoning Department, Zoning and Land Use information. - City of San Juan Capistrano Department of Public Works, Area Development. - City of San Juan Capistrano Finance Department, Business License Information. - San Diego Regional Water Quality Control Board, Groundwater Contamination Case Review. - City of San Juan Capistrano, Water District, Groundwater Information. Published References ' - California Office of Planning and Research, (Cortese) - List of Identified Hazardous Waste and Substance Sites. ' - California Waste Management Board: Active Landfills, September 1989. Department of Health Services, (ASPIS) - Abandoned Sites Program Information System. ' - Department of Health Services, (BEP) - Expenditure Plan for the Hazardous Substance Clean Up Bond Act of 1984, Revised January 1989. ' - San Diego Regional Water Quality Control board: (LUSTIS) Leaking Underground Storage Tank List. - Fairchild Aerial Photography Collection, 1929, 1937, 1939, 1941, 1947, 1950, 1957, 1959, housed at Whittier College, Geology Department. (Pending) - U.S. Environmental Protection Agency: CERCLIS List, Riverside County, California, December 1988. 12 � Ilr• r r Q� r r r Itr tr r r ti r r r ,,, - `l Orange County Fire Department CHEMICAL INVENTORY DISCLOSURE PACKET for: EName:, 4, IrJC . ddressi 31 73/ Asto 41r1w V10 _5�E,d .T.�,v iii Tc�,va 9 2 7 -j o f Pages,: _ Total # of Trade Secret Chemicals;Reported: 0-- i Total # of non Trade Secret Chemicals Reported. 8 Total # of Chemicals Reported: g r ' aI`. , , <i. s ADMINISTERII Inspector's Initials. Daae, atm Entrys �Ful non r '1 i I 1. � r I �1` Agenry Use Only Hazardous Materials Disclosure Information Packet 1 on us�es.��ar� ss rina ou 5eIr+d DrSOOSRly C Business Name /✓ 3/73/ 1.9seo .5' -�izdfo Ste.✓ ��*�.� L`�ois%ef.✓v ��1 y�7675" Bush=Sitc Address(Not a PO Bar.)- lneiude Bu$ding or Suite # City - State Zip 1 Mailing Address Business Name (d different from above) ' .PIai3 iron Wifing Address (d ddferent from above) / Of City State tip 'a CTo,L/ G17 Mad to the Attention o hos>IA-S '�,2u�i 5 : sine (Xis' '-- Business Phone a.? .F.tJ:'16Fiit'"�.5 .., �i. � ';�9:xonlcci�7`. �f 4q:;emerLnroFg�?,i$if4G;�11�3F�s�4�.1 -- - r s&#4ugob 6,,rrct,e6 ois e2�IZ 077el AA�dE7T11 (extension) n 14FTE2 Pim S/4�r`5 45 moi- 7/ _- ?42 SHIFT HOU - / �— PHONE(with extension) ' SKWI AbQ� AAM77711� PHONE(mw extension ' - - ITTLE 2 _ PHONE(with extension) - - 21 P M4 Aw a y(with mension •,.- Sl-:"Ii,uY ,ill - General and Building Inforfnation Doing Business as (DBA) - if different than Business Name 19 2E C 9 C,4,0 94?/ SGS 7Z 9/ Business License Number Dunn & Bradstreet (D&B) Number EPA ID# Rte. 6b,�1, ,QrH,o✓s�� Seoyle, r, Give description of the main operation of your business r),4� 60-A) AD Shift Hours 7� Number of Employees Shift Hours Number of Employees Shift Hours Number of Employees Yes Standard Industrial Code (SIC) uniform Building/O=paney Code(UBC) Are you anon-pato orppni�tiort? 3 Acer Lot Size - Identify in sq.h or acreage Number of Boors - Repotting Siatus(Section M ' Circle"..One ' A No Chemicals are used in any way in our business operations. B Chemicals are used in our company, but we do NOT meet the requirements for disclosure. We have no chemicals that require disclosure in any amount. OChemicals are used in our business and we are submitting our Chemical Inventory Disclosure Forms. - _.- I - 1i- .. . . ..+'+i- -....; .S3l�.Y e.., .,.y✓. "F.3.'.tp�:�'. r.'.la2JISs� 't4 r<f'f :."-z. r s - 1 _ ****SPECIAL NOTICL. If any of the following cot :.: c❑ n nus.;,, L rey.. D% , State and Federal law tc . da,. updated Disclosure Form; 1. Change of Businer, woress 2. Change of Business ownership 3. Change of Busincsa Name 4. Cessation of Business Operation(s) 5. Change of Business occupancy Class (UBC) 6. - - Reclassifiation of TRADE SECRET INFORMATION 7. Change of handling or use of previously undisclosed hazardous material,waste or combination thereof. 1 9. Storage or use of any new hazardous materials that would require you to comply with the disclosure laws. 9. A significant change in the use, handling or quantity of any hazardous material for which Disclosure Information has already been filed. 1 .SRCLIn1l� ,=sem I certify, under the penalty of perjury, that the above information is true and correct to the best of my knowledge. ZZ/ 2 / Zz1 Signature — Date +�. G Cro zTt i eta bis mrii ' Name and Title (please type or print) Retort&Form Tw- 1 1 1 - 4V ft—. +� L PM sy"f ? ti'° ( JA. OFFICIAL ADMINISTERING AGENCY USE '- ': : Date Ret m ed / Date Revi,ed j Total Hours Spent 1 Reviewed/Inspectcd by IIf business is a target harard, describe why ' Boundary/Jurisdiction Cade NFIRS Code - ..Chemical Range District Code Inspection # Bus Plan Range Fire Mgt Zone _ File Status- -- Billing Category RMPP Code RWP Date Required RMPP Date Complied Notes: !XT J A'. 416ran"ge do"un yMireDep'artffle"ntThMCA*rINIPNIllhyTISGTOSItE"FOF�M" Rt Please, Carefully Read Attached Instructions Date qL2 ?1br —Z I B.I.D. 13cf(o Page of now AME 1219621 Z Darr# jqq3__ _ INFORMATIONt 'Physick Health: 7- General; Material Fnrm: Material Type: WAkW RMATION: EPA Code: State Colic: C I sms: Mill W MSX W RadkWive Aniollm: MIXTURES (IL(the three nwid hazardom ingredients) rf". 311-6 3firX/ V41f ye) sittraplal CODES LOC Matrix Units of Max Used Max On Site Avg Daily # Dn" Sj-,f I 1r, ll C P T D Page Grid Measure Tim Year On Any Day Quantity On Silc ( ".0'i", WCATION: R Uwe ads. eal 69 aT) F2 EC Zk iV/072/—/ NAME VZ If&V—' 6t II". INFORMATIONi Physical: Health: I,?- General: 7- Material Form: I'l W ;INFORMATION: EPA Code; State Code: Class: Min W Max W RadioadiveAn"mt: MIXTURES (List the three immadl haurdow ingredients) # MIMA; 2) Stoffw;& CODES LOC Matrix Units or Max: Used Max On Site Avg Daily # Days circ 'r C P T D Page Grid Measure Thou Year On Any Day Quantity On Site ( mil.ii,wr G :7-)0 141 10!5 I&JAbi 09W 60AW �Aw M M M M M M M M M M M 4 0 1 Unty Fire Department CHEMICAL INVENTORY DISCLOSURE 1-01 6,tti Please, Carefully Read Attached Instri 1(,lion,,; Date —112—L BID, lic/L Page of C k 41Q1' AM13 i��Pkjdcal: Health: General: 2— Matetint Film: L Mill"J"I hl't,: IN1.4 EPA Code: State Code: Claes: Min %: Max %: Aiw,�, WiltIii Wilms ftsiml hazardow hW*dknis) ly 14= f CODES LOC Matrix Units of Max Used Max On Site Avg Daily # OmSi I C P T D Page Grid Measure 11im'Year On Any Day Quantity On Site vim -Z— Oe c ceta/ li General: Z— mma Health: Code: State Code: Class: Min %: Max ille bactiniticlous ingredients) y�CHBMICAL NAME We. I'Oc Matrix Units Of MAX.Psed Max On Site Avg Daily # Days Size of 1�11g('t Page Grid measure "Ibria Year On Any Day Quantity On Site Container 12, 3 r Yvan, yr ?k .ounty�Ire%epadment gEMl CAI. INVEN-COIAY C)(SCLOSI (IAL t II Please, Carefully Read Attached Instructions Date ti B.1.01! /30/47 / Page „ 0 12 1 �h6yalaL• �L Ilealth: _ _ Oencmi: 7, _ _ MalrJnt Farm: NvP ••I 1 Code, State Code: Clam: Min %: h1ex %: lWkrorm Anv,,n, T~�Ingredknk) CH CAb NAME MI LOC Matrix Unita of Max toed Max On Site Avg Daily h' Dm- .•I 1 r D Pit Edd measure 7hrul 'ur On Any Day Quantity On SH(- """j,'' l. . //."D//J G?, / /� %mac%t's� iir• — -- - Ixn :r/1�>-'. .p,IlpIG4 „1_ Heallh: Z Oeneralt �_ Material Form: 111nl"I'd -1.11., !WA Cdda State Code: CID.": Min %: Max %: ._ Radkxxihe Anxxnn: r , pl W ingredients) „•,,?•`' �PCNBMWAL NAME It I • ` I � H J'... LOC Matrix Units of Maxl aed Max On Site. Avg Daily M D., -- — •' 1 �•`I b Page Odd Measure 7h 'year On Any Day Vuantily On srl^ WIZ; Awl Offty Fire Department CHEMICAL INVENTORY DISCLOSURE= I--OHM r ; . Please, Carefully ead Attached Instructions II- l� Date z BID, /30/4 / Page LHealth: OenenL• -- -. . .- Mal.rr.rr�rrn: .calk Slate Code: Char. Min W alae 4E: Rndk. '%n:,br.-• . CliWt)ede 1 lama ar•r CHBMIGW NAME 1 ,j it LOC Matrix Unita of Max Ueed Mn On Silr -r, Dail\ h .r�".D Page Grid Measure 'IhruilYdr On/Any Daly 'tua/ntily / r tit '��� } ' 21 _� li`l�A./r / l 1-3w') ' sr ` b{alplti �_ Health: General: —_ Maferlal Form: -� alnirr P,I Irr" A Cada Slate Code: Cls."! Min W Max W _ IWk%K1Kr Any, i hezordom Ingredients) CHEMICAL NAME ,r I if LOC Matrix tinils or Mu,Used Max On She Avg Daily d Daya qi7, ,d I ,.r O Page Odd Measure 7h IYes On Any Day Qua tit y On Site r ma6 r ' =: exp4net -, the'sour ,rr;r Of r -` ,veeer:7inrtr Oslo rsp�vl a,n....•"o�tt�,_.�i�u"' "` r -,^(Essamlelly similar to U.S.DepMnrnt of La1swFarmWDSHA-20 .:3 and yanxNly acaplsd M CMi1da for ? 'T Do Not Dupacan This Form.llaquait an Orlpwul. -� .c r'. ' ---PRODUCT Oxygen CHEMICAL Oxygen SYNONYMS Not applicable NAME FORMULA Oz CHEMICAL Not applicable f. FAMILY MOLECULAR 32OD WEIGHT ' TRADE NAME Oxygen 7:_--------.2„ Y. 11111111r ' For mixtures of this product request the respective component Material Safety Data Sheets. See Section IX. ' MATERIAL (CAS NO-) Wt (%) 1984.1985 ACGIH TLV-TWA (OSHA-PEL) Oxygen (7782-44-7) `` 100 None currently established (None currently estaolished) : ;' CA.aT 1 BOILING POINT, 760 mm. Hg -183°C (-297.4°F) FREEZING POINT -218.4°C (-361.17) SPECIFIC GRAVITY (H2O = 1) Gas VAPOR PRESSURE AT 20C. Gas VAPOR DENSITY (air = 1) 1.105 ® 25'C SOLUBILITY IN Negligible ' WATER, % by wt. PERCENT VOLATILES EVAPORATION RATE BY VOLUME 100 Not applicable (Butyl Acetate = t) APPEARANCE AND ODOR Colorless, odorless gas at normal temperature and pressure. - ' IN CASE OF EMERGENCIES involving this material, further information s available at all limes. R In the USA 304 — 744-3481 In Carica 514 — 645-5311 m For routine information contact your local supp'lei Union Carbide requests the users of this oroduci 'c stuev this V-tenal Safety Data She-- C t ar ec ware z hazards and safety information. Td promote safe lise C!- .h.s orocucf a user ,nould (1) > am.n - ees. aCerris nc r, .. cr. of the ntormation on this MSDS and anv oroouc: ns _aioiv ,formation. customers ier'ne;;rncudt,ane(2_' :eques - - - - - -- -. - - h,zaros and saety ntormauon an ,THRESHOLD LIMITYAWE: None currently established 1FFECTS OF SINGLE(ACUTE)OVEREXPOSURE: SWALLOWING—No evidence of adverse effects from available information, SKIN ABSORPTION —No evidence of adverse effects from available information. - INHALATION— Breathing 80%or more oxygen at atmospheric pressure for more than a few flours may cause nasal stuffiness, cough, sore throat, chest pain and breathing difficulty. Breathing oxygen at higher pressure increases the likelihood of adverse effects within a shorter time period. Breathing pure oxygen under pressure may cause lung damage and also central nervous system effects resulting in dizziness, poor coordination, tingling sensation, visual and hearing disturbances, muscular twitching, unconsciousness and convulsions. Breathing oxygen under pressure may cause prolongation of adaptation to darkness and reduced peripheral vision. SKIN CONTACT — No evidence of adverse effects from available information. , EYE CONTACT — No evidence of adverse effects from avaiiaDle information. FFECTS OF REPEATED (CHRONIC) OVEREXPOSURE: No evidence of adverse effects from available information. MTHER EFFECTS OF OVEREXPOSURE: See "Notes to Phvsician:' EDICAL CONDITIONS AGGRAVATED BY OVEREXPOSURE: See 'Notes to Physician" IWGNIFICANT LABORATORY DATA WITH POSSIBLE RELEVANCE TO HUMAN HEALTH HAZARD EVALUATION:None currently own. EMERGENCY AND FIRST AID PROCEDURES: - LALLOWING—This product is a gas at normal temperature and pressure. W / KIN — No emergency care anticipated. J INHALATION — Remove to fresh air. Give artificial respiration if not breathing. Keep victim warm and at rest. Call a physician. YES — No emergency care anlicipated. ITES TO PHYSICIAN:Supportive treatment should incl ace immediate sedation,anticonvulsive therapy if needed,and rest.Animal dles suggest:nar rhe administraron of certain drugs. inc:acing phenothiazine drugs and chloroquine,increases the susceptibility c !ozicily from oxwgen at high concentrations or pressures. Animal studies also indicate that vitamin E deficiency may increase Che pribiliry to ,x}gen .0xicny y obstruction during high oxygen tension may cause aiveolar collapse following absorption of the oxygen. Similarly, occlusion eustachian tubes may cause retraction of the eardrum and obstruction of the paranasal sinuses may produce "vacuum-type" eadache. born premarure!rrAnts expcsee!c high oxygen conc&(aaricns may suffer getayed retinal damage which can progress to retinal chment ane bucdress(retrolental fibrep•'asia). Retinai damage can also occur in adults exposed to 100%oxygen under greater an atmospheric pressure, particularly in individuals whose retinal circulation has been previously compromised. dividuals exposed for long periods to oxygen at high pressure and all who exhibit overt oxygen toxicity should have ophthalmologic nations. ,ICN CS.7 -.`! -v-._GING AND CUTTING: Read and - - -,st3r^ :.^.^ '^a r_::.re :; -^._;ructions and :me precautionary label on �ice uc ­ zan Standard Z49. Sawyry n ar tint ' �Qviisnec ov :he American Welding Society, PO. Box a0, Miam,, - -_r dz 73135 and OSHA Pueticalion 2c-_L., 29CFRI9101. U.S S avernmem Printing Office. Washington, D.C. 20402 .o•e det3 - _'ner SAF-=—Y AND HEAL.H informs. - .efo...^_rides..ee^u C!ir- -_ .52-529. TP ecau!ions and Safe Practices .. - - ve,! .� __..,.c _ �.i: : ' :�tic=e _as welding, �.;tung, and Healing,' You �. .-:;c _ mu _:v;sirn -or^ nications Ceganment. _ Deal UCT` rXygen '776 ar X85 AUTOIGNITION —FLASHPOINT ,_ Notapplicable r '�-^ ^ •: Not app tca le .(test method) _ TEMPERATURE FLAMMABLE LIMITS -COWER Not applicable UPPER Not applicable ' IN AIR, % by volume EXTINGUISHING MEDIA:Vigorously accelerates combustion,Use media appropriate for surrounding fire.Water(f.e.safety shower) is the preferred extinguishing media for clothing fires. SPECIAL FIRE FIGHTING PROCEDURES.Evacuate all personnel from danger area. Immediately cool containers with water spray from maximum distance until cool, then move containers away from fire area if without risk. UNUSUAL FIRE AND EXPLOSION HAZARDS:Oxidizing agent,vigorously accelerates combustion.Contact with flammable materials ' may cause `ire or explosion. Container may rupture due to heat of tire. No part of a container should be subjected to a temperature higher than 52°C(approximately 1250F). Most containers are provided with a pressure relief device designed to vent contents when they are exoosed to elevated temperature.Smoking,flames and electric sparks in the presence of enriched oxygen atmospheres are potential explosion hazwos. STABILITYCONDITIONS TO AVOID: See Section IX. UNSTABLE STABLE X ' INCOMPATIBILITY (materials to avoid): Combustible materials, asphalt, flammable materials, especially oils and greases. ' HAZARDOUS DECOMPOSITION PRODUCTS: None" ' HAZARDOUS POLYMERIZATION 1 CONDITIONS TO AVCIC: lone currently known. May Occur Will not Occur X ' ,•- � v_ VU.'SP1LL"ORsI.E.A PROCEDURES STEPS TO BE TAKEN IF MATERIAL IS RELEASED OR SPILLED:Shut off leak if without risk.Ventilate area of leak or move leaking container to well-ventilated area.Remove all flammable materials from vicinity.Oxygen must never be perm!tted to strike an oily surface. greasy clothes, or other combustible material. WASTE DISPOSAL.NETHOD: SIowiv-eiease into atmcsonere. n :- _an. "u;::r.:rs sr==.. =emc•:� " ------" -_ _._ .;.._ ' >.� '7 == n�sr1985 _:VI,I, PEC fid G. N RESPIRATORY PROTECTION (specify,type): Not required. LOCAL EXHAUST— Not applicable. MECHANICAL(general) —Acceptable. VENTILATION SPECIAL — Not applicable. I OTHER — Not applicable. PRCTECTIVE GLOVES: Pre+erred for cylinder handling. EYE PROTECTION: Select :n accordance with OSHA 29 CFR 1910.133. OTHER PROTECTIVE EQUIPMENT:Metatarsal shoes for cylinder handling. Select in accordance with OSHA 29 CFR 1410.132 and 1910. WARNING:High pressure gas.Vigorously accelerates combustion.Avoid contact with oils,greases and other flammable materials. Never use manifolds for oxygen cylinders unless specifically designed for such use. Use only with equipment conditioned for oxygen service.Use piping and epuipmeni adequately designed to withstand pressures to be encountered.Protect container against physical amage.Isolate from combustible gas installations and combustible materials by adequate distance or by gas-tight.fire-resistive barriers. rotect against overheating.Never use an oxygen jet for cleaning purposes of any sort,especially clothing,as it increases the likelihood -../ of an engulfing fire. Note:Reverse flow into cylinder may cause rupture. Use a check valve or other protective apparatus in any line Uiping from the cylinder to prevent reverse flow. TURES: When two or more gases. or liquefied gases are mixed, their hazardous properties may combine to create additional, unexpected hazards. OGlain and evaluate the safety information for each component before you produce the mixture. Consult an ndu,trrei =yc.e^:st. .r ctner trained person when you make your safety evaluation of the end product.Remember,gases and liquids ave creper^as .vmcn can cause serious injury or death. Be sure to read and understand all labels and other instructions supplied with all of this product. - -_ -•:,N!-, ,v,:h 0;3s;lcs snouic be confirmed prior fo use. For safety information on general handling of compressed gas yllncars,.:c:=!.n a copy of pamphler P-1, "Safe Handling of Compressed Gases in Containers"from the Compressed Gas Association, Inc.. 7235 Jefferson Davis Highway, Arlington, VA 22202. E? '- =_.:NG AND STCRAGE CONDITIONS: Never work on a pressurized system. If there is a leak, close the cyfinder valve. :system dy venting to a safe place,then repair the leak.Never lubricate oxygen valves,regulators,etc.,with any combustible substance. e oeimc-, =xpressed herein are those of qualified experts within Union Carbide. We believe that the information contained herein •he date if l.h,9 Mmol t.nl -!v Dlata ?;nce the use of this information and these opinions and ".he conditions -.-: ,rF� qc: -.,r.e ,Ire .c..uci of Union :;aro,oe, ',t is the user's obligation to determine the conditions o! safe use q? 3'cNE E ;J,;~ _ ;&. IN CANADA: - . c,o= -crocrauon Union ^zreica Caraca 1 - WIN . .? /,Y,-, _srr tersf.a n rur4NMn/pct.tllslWb w�4 q ,gr `- `Materia! Safety Data= ieet 4. .n.i:Y ?iq..'�T�i"F!i.c . .- [-_ - -�y3b]Y/R'1V;4k'14;z .- Prepared' Accords to the OSHA Maisrd Communication standard 129 CFR 1910:12001: (Formerly Called MATERIAL INFORMATION BULLETIN) ' CPS 27 105 DANGERS HARMFUL OR FATAL IF SWALLOWED PROLONGED OR REPEATED CONTACT WITH SKIN CAN BE BARMFUL MAY CAUSE SKIN IRRITATION C@BUSTIBLE KEEP OUT OF REACH OF CHILDREN TYPICAL COMPOSITION Petroleum m_d-distillate (CAS 68476-34-6) >99% hd=_t vas m:av -'.-elude anti-rust agent, metal deactivator, ar.ti-oxidant <1t EXPOSURE STANDARD No Federal OSrA acxsure standard or ACGIH TLV has been established for this ' mate"-al. PHYSIOLOGICAL L HEALTH EFFECTS EMPRGENCY G FIRST AID ?ROCEDURES Eyes Expected to cause no more than minor eye . Flush eyes immediately with fresh water irritation. for at least -15 minutes while holding the ' eyelids open. If irritation persists, see a doctor. Skin - May cause skin irritation. Application of Remove contaminated clothing. Wash skin a similar material onto the skin of thoroughly with soap and water. See A rabbits produced moderate to severe skin doctor if irritation occurs. Launder irritation. Prolonged or repeated skin contaminated clothing. contact may be harmful. See Additional Health Data. Inhal ation Prolonged breathing of high vapor _f there are =:-t or s•✓n7-toms due to concentratite. ons can cause zeal ner7ous oreathing t5-, s material as described in system; effects. See Addct_enal Health this MSDS, move the person to fresh air. Data. If any of these effects continue, see a ' doctor. Inyesticn Not expected to have acute systemic If swallowed, give water or milk to drink toxicity by ingestion.. Note to Physics-an: and telephone for medical advice. DO HOT ' Ingestion of this product or subsequent make person vomit unless directed to do so vomiting can result in -sc_ration of light by medical persc:nel. If medical advice hydrocarbon __ ._id v"c c_ c—. t>—L..a c-Lnet be obta..rJ , then 'axe the t-r .... med_ `--- mer- -, treatment certa ,or - r M ` Y expected to *act: zany environmental Envirorwesstal This matereraaI is not -- .—. .- - P P ental _ SPECIAL PROTECTIVE IN1PORMATIOR problems other than those associated with oil spills. Eye.Protection:- Do not'get. in eyes. ZTEye _ Precautions if Material is Released or ' contact mn be bvo`ided by nearing chemical SpiIledrjEliminate all :open flame in safety-rodvicinity of spill or released vapor. Stop Skin Protection: Avoid contact with skin the source of the leak or release. Clean or clothing. Skin contact can be up releases as soon as possible, observing ' minimized by wearing impervious protective precautions in Special Protective clothing including gloves. Information. Contain liquid to prevent Respiratory Protection: This material may further contamination of soil, surface ` be an inhalation hazard, and unless water or groundwater. Clean up small ventilation is adequate, the use of an spills using appropriate techniques such approved respirator is recommended. as sorbent materials or pumping. Where Ventilation: Use this naterial only in feasible and appropriate, remove ' well ventilated areas. contaminated soil. Follow prescribed procedures for reporting and responding to FIRE 720T _IOX larger releases. ' Waste Disposal Methods: Place contaminated Liquid evaporates and forms vapor (fumes] materials in disposable containers and which can catch fire and burn with dispose of in a manner consistent with explosive violence. invisible vapor applicable regulations. Contact loc=_1 ' spreads easily and can be set on fire by environmental or health authorities for many sources such as pilot lights, welding approved disposal of this material. equipment, and electrical motors and switches. Fire hazard is greater as liquid REACTIVITY DATA temperature rises above 85°F. Flash Point: (P-M)140°F(600C) Stability (Thermal, Light, etc.): Stable Autoignitioa Temp.: NDA Incompatibility (Materials to Avoid) : Nay ' Flammability Limits: n/a react with strong oxidizing materials. Extinguishing Media: CO2, Dry Chemical, Hazardous Decomposition Products: Normal Foam, Water Fog combustion forms carbon dioxide and water Special Fire Fighting Procedures: For vapor; incomplete combustion can produce fires involving this material, do not carbon monoxide. enter any enclosed or confined fire space Ra=ardous Polymerization: Will not occur. without proper protective equipment. This ' may include self-contained breathing PHYSICAL PROPERTIES apparatus to protect against the hazardous effects of normal products of combustion Solubility: Miscible with hydrocarbons; or oxygen, deficiency. Read the entire insoluble in water. t1S 5. Appearance (Color, Odor, etc.): Pale yellow liquid SPECIAL PRECAUTIONS Boiling Point: 176-ZB2°C (Min.) ' - Melting Point: n/a ?age 3. Specific Gravity: 0.82 @ 15.6/15.6°C Vapor Pressure: 0.04 psia @ 40°C Vapor Density (Air-1): NDA ' Percent Volatile (Volume 4): NDA Evaporation: NDA viscosity: 1.9 cst @ 40-C im_Lr- , Sulfur Content: 500 ppm (Nast.; n/a = Not Avpy_cable MA No .ata 3va2ate'e - .. - .-_cur ;aloe :. vain :. � _. .. re r.ar- Tr x•rvea :e .. __t n -i T- �¢ 'J_o� . -. - —: -.- ,.- - A 11 Matena Safety-D - aShe-ef ' OIEVRON Special Diesel CPS 272105 ADDITIONAL HEALTH DATA Signs and symptoms of central nervous system effects may include one or more of the following: headache, dizziness, loss of appetite, weakness and loss of coordination. Affected persons usually experience complete recovery when removed from the exposure area. ' Tb:<_ product contains a petroleum mid-distillate. Toxicology data from studies on similar `ycrocaracr. a-3istillates indicate that lifetime application to the skin of mice r=_sclter a _ow-level skin carcinogenicity response c.',aracter_ze by low tumor incidence ' a,c lcnc la envy. Ot.)er similar materials caused gene mutations in the Mouse Lymphoma assay and in t.`.a Rat Bone Marrow Cytogenetic Assay. .r of or .r.tarcatent sxin contac. with this product is not expected to produce any ' se=cots e"ec':z .f _t is washed from the skin'. White ncrmai handling of this product is _: net like: cause cancer in humans, skin contact and breathing of mists, fumes or vapors s,`.oulc be r=__c d to a minimum. We strongly recommend that the precautions outlined in ' this MSDS be followed when handling this material. ^ SPECIAL PRECAUTIONS ' READ AND OBSERVE ALL PRECAUTIONS ON PRODUCT LABEL. DO NOT USE OR STORE near flame, sparks or hot surfaces. USE ONLY IN WELL VENTILATED AREA. rKeep container closed. DO NOT wel ', heat or drill container. Reclaca cap or bung, Emptied container stil'- contains .`.azardous or explosive vapor or lice nzz use . less::- - -- _ , ty dr'_:. ._ a_xp'csi_.. may result. as --r-a:_e hew air =.: zzce lilt . = •yes may ac:-elate and _usa c 1 1 r 1 i r - - - MATERIALSAF SHEET Mwentlally sImllar'lo Form OSHA-20) �Compllss wlth 29CFR 1910.1200) SECTION I TRADE NAME ROSEMEAD OIL PRODUCTS 12912 LAKELAND RD. SANTA FE SPRINGS, CA 90670 CHEMICAL FAMILY: PETROLEUM (213)441-3261 SECTION II - HAZARDOUS INGREDIENTS COMPONENTS CAS. TLVIPEL PERCENT BY NOS_ PPM + 1 WEIGHTNOLUME 1 3=- HIST (.D,c _?0 i.3-!9 ;0. !000) SECCTION III - VIRE AND EXPLOSION HAZARD DATA -U.Z.APDCUS THERMAL DECCMPCSiTION FLA.MABLE V:. . - LIMITS: . .=Cti _til =OS:=i, in�^J ' FLASH POINT: 1 I EXTINGUISHING i MEDIA: CARBON DIOXIDE, DRY CFEMICAL, FOAM, HALON, WATER FOG I C.O.C. 38007 Min. f DOT INFORMATION: N/A ' UNUSUAL FIRE AND EXPLOSION HAZARDS: VAPORS MAY IGNITE, MINIMIZE BREATHING VAPORS, GASES, FUMES AND DECOMPISITION PRODUCTS. I SP_C:AL .=IRE FiG I"tNG ?RCCEDL-PES: ,c_ _rhnE' D?C"_:C"-.'- _ ",a- . ,D >=T v ;n,l•••AT vn ' SECTION i'/ AL GA BOILING RANGE Approx. 5000 F SOLUBILITY: 1i_ -aa_e_; _nsO1 . PH: N/A. - ' VAPCR PRESSURE: `r , VAPOP DENSITY EVAYP.ATICN RATEAPI WEIGHT " 'JOLAT7LE aRAVIT1' -ER GALLON BY'JOLUME 'NCCMPAT?IL:TY EASE FIRST AID "^.___x._.._ •� ' — _-_ +✓TS :_. - PROCEDURES. LOW ORDER OF TOXICITY. MAY CAUSE DO NOT INDUCE VOMITING. GET MEDICAL IRRITATION IN VERY SENSLTIVE INDIVIDUALS. ATTENTION. - ,_ JE NO ADVERSE AFFECTS ON SHORT TERM REMOVE TO FRESH AIR. IF BREATHING EXPOSURE. STOPS, APPLY RESUSCITATION, GET MEDICAL ATTENTION. ' E X EXPECTED TO CAUSE NO MORE THEN MILD FLUSH WITH FRESH WATER FOR AT LEAST O IRRITATION, EXCEPT IN VERY SENSITIVE 15 MINUTES. GET MEDICAL ATTENTION ' INDIVIDUALS. IF IRRITATION PRESIST_S. % H El XT Z., rr. __lH SC u_FECTS . ={CEnm WASH THOROUGHLY AFTER HANDLING. s` FOR PRCLONGZD :r'GSi :.= -2v SENSITIVE LAUNDER CONTAMINATED CLOTHING. j 4 INDIVIDUALS. i GET MEDICAL ATTENTION IF IRRITATION OR INFLAt"ATION DEVELOPS. SECTION VII - SPILL OR LEAK PROCEDURES STEPS TC BE TAKEN IN CASE PREVENT ENTRY INTO S'cWGR OR WATERWAY. AVOID CONTACT WI MATERIAL IS RELEASED OR SPILLED: OPEN FLAME. PICK UP FREE LIQUID FOR DISPOSAL. ABSORB ' REMAINING WITH INERT MATERIAL. WASTE DISPOSAL METHOD: DISPOSE OF ALL CONTAMINATED MATERIAL IN ACCORDANCE WITH. LOCM., STATE AND FEDERAL REGULATIONS. TRANSPORTATION INFORMATION: CONSULT EPA, DOT, LOCAL AND STATE REGULATIONS. SECTION VIII - SPECIAL PROTECTION INFORMATION RESPIRATORY ?RC7EC7ION: 9CT. 7S7-ALi: ZQU13w. SEE SEC.II 6 5:C.711 RCTECTIVE GLOVE5: 7 EMIC4_-R=5_S_: Wt USEGOGGLES OR FACE SHIELD GLJVES G PF :=: _ =ROLJNGZD .,..TaCT. WHEN CONTACT COULD POSSIBLY OCCUR. --H ERPROTEC7IYEEOLLlPSIIENE 'SZD _ ..rr 7N USE. 'WEAR CHEMICALRES=STAN- ARC , i .....TS WiiZREr :i:GH=' 7CCUR. YENTILATICN: SEE S7- ._I. USE MECHANICAL VENTILATION IF NECESSARY. 1 I CAUTIONS =�'t�:.L- ;•S'-C 3E __� WH N '.ANDL �C R -C?.NG: xi =I=3 OR ?FFSS!:R7-LE CONTAINER. DO NOT SAFky. t7i4I _ _ aro F«rR osHArt-46) -;•ca,+Pli.k Y_ OE-NAME- - 6LEANrI21G SOLPENT. OR THINNERair -7t �- CHEMICAL FAMILY: PETiOSEMEA001L.PRODUCES NAPTHA LEUM RO12912LTJfKE[UIND RD w y. SANTkE'E,5j1-N CA 90670 ' SECTION 11 - HAZARDOUS INGREDIENTS . CAJL nYTeL FEACENTrr COMPONENTS Nos_ PVM mow WEUNTIVOLIRIK ' I COrBUSTI3LE 64742-88- 1, E_43AFFINS 5 NAPTHENS t SHA 5OJ PER, t CG IH 85-94 100 TLQ ??Ct4?T=CS 6-15 ' ECTION III - FIRE AND EXPLOSION HAZARD DATA HAZARDOUSTHERMAL DECOMPOSITION FLAMABLE Z F30N 'MONOXIDE, CARBON DIOXIDE AND UN=DENTIFIED ORGANIC LIMITS: S i0 air ' CG*vUNDS IN 3L'.CY SMOKE i Upper - 6 . FLASH POINT: E)MNGUISHING MEDIA: CARBON DIOXIDE , DRY CHEMICAL, FOAM, HELON, WATER FOG. TCC 116 Deg F ' DO NOT USE WATER STREAM DOT INFORMATION: -- COMBUSTIBLE 'UNUSUAL FIRE AND AVOID ACCUM—G .ATION OF '_ER 3ECAUSE THIS PRODUCT WILL FLOAT ON ' i.9,.PLOSION HAZARDS WATER AND 14_4Y REIGNITE ON THE SURFACE. SPECIAL FIRE SHOULD WEAR SELF-CONTAINED BREATHING APPARATUS. USE WATER SPRAY 1 FIGHTING PROCEDURES TO COOL NEARBY =:=3OSE'J CONTAINERS AND STRUCTURES. i I � SECTION IV - PHYSICAL DATA A ' 301UNG RANGE 325-384 F SOLUBILiTY:Ia War=_r Nil VAPOR PRESSURE APPEARANCE AND ODOR: LIGHT COLOR:D Ie? HG/20 7C at 100 F HYDRO CARBON ODOR a ' VAPOR DENSITY I EVAPORATION RATEAPI MEQ_:^ % vOL.. ..� j GRAVITY TCP. ��N 1 ' (BULYL ACE7ATE=1) W r-1) 4.8 0. 1 47 .6 De¢ I 657' Ib= 100' SECTION V - REACTIVITY DATA - ' ' INCOMPATIBILITY 1 +MATERIALSTCAVOIC►: ''DYTDAI-NG ?G-NTS -^- OVOID: -TP3LE ' PDOUS ?ECCMPOS,"!ON R?CDUCS: ------ -- -- - _- It - ../ w MAY CAIISE VOMIT-Ng-:--.BREATHING VOMIT MAY DO NOT .IFDIICE VOMITING GE2 IMF TATE _ CAUSE CHEMICAL PNEUMONITIS AND PULMONARY MEDICAL ATTENTION. F V02SITING OCCURS, i EDEMA(HEEAB]RRHAGE KEEP HEA>yELOiT:HIPSr�TQ EBLVENT IR ,°, r • BREATHI '- EDNGSt' p. U � T ;• MAY IRRITATE MUCOUS MEMBRANES, CAUSE REMOVE TO .PRESS AIR. RESUSCITATE IF NOT t E L HEADACHES, NAUSEA, VOMITING AND COMA. BREATHING;"BUT NOT IF.UNCONSCIOUS OR F 1 VERY HIGH CONCENTRATIONS MAY CAUSE CONVULSING. GET MEDICAL ATTENTION. r UNCONSCIOUSNESS OR DEATH. EMAY IRRITATE IMMEDIATELY FLUSH WITH LOTS OF SOAP AND X E WATER FOR 15 MIN. , LIFTING UPPER AND O LOWER EYELIDS. GET MEDICAL ATTENTION. S ul R 1 E MAY DR S{IN. ?ROLONGED ONT3CT uAY 12,.*=DLATELY WASH WITH LOTS OF SOAP AND s CAUSE DEZuAT=TrS. WATER. REMOVE AND LAUNDER CONTAMINATED CLOTHING. GET MEDICAL ATTENTION IF IRRITATION PERSISTS. SECTION VII - SPILL OR LEAK PROCEDURES ' STEPS TO 3E TAKEN IN CASE MATERIAL IS RELEASED OR SPILLED: ELIMINATE IGNITION SOURCE. WEAR PROPER PROTECTIVE EQUIPMENT_ PREVENT ENTRY INTO SEWER OR WATER WAY. PICK UP FREE LIQUID FOR DISPOSAL. ABSORB ' REMAINING MATERIAL WITH INERT MATERIAL, WASTE DISPOSAL METHOR . DISPOSE OF ALL CONTAMINATED MATERIAL IN ACCORDANCE WITH LOCAL, STATE AND FEDERAL REGULATIONS. ' TRANSPORTATION INFORMATION: CONSULT EPA, DOT, LOCAL AND STATE REGULATIONS. SECTION Vill - SPECIAL PROTECTION INFORMATION RESPIRATORY USE IOSH AFPROVED CANNISTER RESPIRATOR IF USING PRODUCT IN ENVIROMENT PRG T ECTION: EXCEED- ING PERMISSBLE EXPOSURE LEVELS — SEF, SEC II SRC'? TiV'c 3LOVES: RI 3BER GLOVES EYE PROTECTION: CHEMICAL GOGGLES i OTHER PROTE•:TIVE EQUIPMENT: LONG SLEEVED SHIRT, PANTS, SAFETY SHOES AND RUBBER APRON. API ;ROWER SHOULD 3E ACCESSIBLE. �ENTL ON: SEE SI . II USE MECr9NICAL VENTILATION IF NECESSARY. 1 SECTION iX - SPECIAL PRECAUTIONS —�-:v 4),EN rANDUNG OR STORING: DO NOT ALTER OR PRESSURIZE CONTAINER. DO NOT SOURCE. AVOID SW:TC_ LOADING — GROLTiD ALL EQUIPMENT AND "DOLS. -.- HIGH CONC=`;:',7I0NS `4AY CAUSE IT-,:--.RAT- DYSr TICTION. DA73 ,Cf SLLV �"..0 '_= MOST 2EL IP3L_ :i✓ __�'Sc: _C _ _ .- _ __1.... 3E �i:IH_-. ` (Essenttalty elmiYarto Form OSkA-20) Compiles with 28CFR 7910.tT00ii`-'� -_- - y ���� '�"� _ SECTION I >, RAW ^ AIIMMATICTRANSMISSION ',: ,� , .. ^ rs +u_?c i 'k ' ' FLUID EMEAD _R ,:,.•• OIC PROpUC1S.. IZI112 SPRINGS, RD SANTA FE NGS CA 90670 CHEMICAL FAMILY: PETROLEUM -< 1941-3261 1 ' 9 .nom, .. .. . .:._ " SECTION If - HAZARDOUS INGREDIENTS _ COMPONENTS Com+ nvfi'E' PERCENT BY NMI PPM ,rap,. WEIGHTIVOLUME I OIL MIST (OSP..,-29 CFR-1910. 1000) 5 SECTION !!I • FIRE AND EXPLOSION HAZARD DATA � HAZARDOUS?HERMAL DECOMPOSITION FLAMABLE LIMITS: N/A CARBON DSOX:DE A-ND TOXIC GASES `EXTINGUISHING FL45H POINT: ' I�MEDIA.' CARBON DIO%IDE, DRY CHEMICAL, FOAM, HALON, WATER FOG C.O.C. 380OF Min. DOT INFORMATION: N/A ' I UNUSUAL FIRE AND EXPLOSION HAZARDS: VAPORS MAY IGNITE, MINIMIZE BREATHING VAPORS, GASES, FUMES AND DECOMPISITION PRODUCTS. ' SPECIAL FIRE FIGHTING PROCEDURES: USE PROPER PROTECTIVE EQUI?'+ENT AND SELF CONTAINED BREAT3=NG A?PA?ATOS IN CONFINED, ENCLOSED AREAS, SECTION IV - r! YSICAL DATA BCIUNG RANGE Approx. 5000 F SOLUBILITY: In water; Insol. PH: N/A /Re't ' IVAPOR PRESSURE N/A AP-�LcRANC'e AND ODOR: tee, -y--` y _ m ub:ica.l._r tVAPOP DENSITY EVAPORATION RATE GRAVITY PER GALLON BY VOLL�'MLE t iFE , ATI YP. 1 � . HIER THAN THAN AIR LESTHANEEiE TR 3C2 Dec I i.3. 1bs . I SEECTiCNI V — _.y"Ciit!{ 1 i uQ:} � INCDMPATIBILI i +MATERIALS TC AVOID.: s7?CNG ^X---7-:1'- 00 Z J_ 1 EALTKW'MD� 77 Flr4rr AID PROCEDURES_l.l;.EFFECT& T AFFECTS ON SHORT TERM E Pi E A j2p ]MUMR � VT MR f �WTj�— 0 E S MWT VIT)ttArS. U EXPECTED TO CAUSE NO E-FEC--s' EXCEPT WASH. THMUGHLY AFMii FOR PROLONGED EXPOSURE IN SENSITIVEQQRE Ad .40FZAWNAMEM INDIVIDUALS: CAL --I TION VE SECTION VII - SPILL OR LEAK PROCEDURES STEPS 70 BE TAKEN iN CASE PREVENT :NTRY INTO SEWER OR WATIERWA=. AVOID CONTACT WITH MATERIAL IS RELEASED OR SPILLED: OPEN FLAME. PICK UP FREE LIQUID FOR DISPOSAL. ABSORB REMAINING WITH INERT MATERIAL. WASTE DISPOSAL METHOD: DISPOSE OF ALL CONTAMIN_T-D MATERIAL TN ACCORDANCE WITH LOCAL, STATE AND F-Dc REGULATIONS. TRANSPORTATION INFORMATION: CONSULT EPA, DOT, LOCAL AND STATE REGULATIONS. SECTION VIII - SPECIAL PROTECTION INFORMATION RESPIRATORY PROT.EC71011: ';C: 'ZS"ALT-Y UQUIREPD. SEE SEC.11 & SBC.Iji R OTEC 71V 1'3 L'_'!5 S I _-UT" -?ZS IS 7__N T EYE PROTECTION:.USE GOGGLES OR FACE SHIELD ,LOVZE TO ?ROLONGED CONTACT, WHEN CONTACT COULD POSSIBLY OCCUR. OTHER PROTECTIVF� FOUIPMENT, WF EN NOT IN USE. WEAR CiiEMIC.�LL RESISTANT_-,7 ---------- I m- CU CO �T OCCUR. VENTILATION: SEE SEC.11, USE MECH.ANIC.-'! VENTILATION IF NECESSARY. SE 7"'Q N S;:=_'.- PRECAUTIONS CAI 5'S - "-a-N 4wp -.AIDUSIG _R c-,CRtNG: imp RIZH CONTAINER. DO NOT A OR ?RE_SSJ' sc ER _ND p_, x - ENAME ! L ,:,• i HAZARDOUS 1 >.' r . .XeC. COMPONENTS PERCENT 6Y _ ;^, siR•i�:y,,.. . NOS: WOONTNOLUME 2 rnt OIL MST J(OSHA 29 CFR 1910 1000) "{ ` 5 i SECTION III FIRE AND EXPLOSION HAZARD-DATA HAZARDOUS THERM- - DECOMPOSITION "FLAMABLE - LIMITS: Nfr'. , ' �GAR_'JN DIO%IDF AND TO%IC GASES A EXT INGUtSHFLASH POINT: ING MEDIA: CARBON DIO%IDE, DRY CHEMICAL, FOAM, HALON, WATER FOG _ C.O.C. 380°F Mia. -.Wq - - DOT INFORMATION: N/A UNUSUAL FiRE AND - - EXPLOSION HAZARDS: VAPORS MAY IGNITE, MINIMIZE BREATHING VAPORS, GASES, FUMES AND DECOMPISITION PRODUCTS. ' r SPECIAL FIRE FIGHTING PROCEDURES: USE PROPER PROTECTIVE EQUIPMENT AND SELF CONTAINED BREATHING APPARATUS IN CONFINED, ENCLOSED AREAS. SECTION IV - PHYSICAL DATA ' BOILING RANGE Approx. 5000 F SOLUBILITY: In water, IOs Ol. PH: N/A VAPOR PRESSURE _N/A APPEARANCE AND ODOR: Petroleum Lubricant II V-POR DENSITY EVAPORAnON RATE APIWEIGHT %VOLATILE GRAVITY PER GALLON BY VOLUME HEAVIER THAN AIR LESS THAN ETHER TYP. Typ' 302: Dee 7.3= lbs ! N/A SECTION V - REACTIVITY DATA INCCMPATIBILITY — �MATERW_STOAVOID►- STRONG O}:=D1Z-_NG AGFNTS STABILITY: C0401TICNs a AVOID: SI?3LE -- DO NOT 9EA= ABOVE FLASHPC:NT I HAZARDG:. ::FCCMPC5i'lCN P?CDu,._ . .'n.' - ' ? 5 i 1� p . — 1 u { E SECTION VII - SPILL OR LEAK PROCEDURES STEPS TO BE TAKEN IN CASE. - , � MATERIAL Is RELEASED OR SPILLED' PICK UP FREE LIQUID FOR DISPOSAL. =ABSORB �*�itEMAINING SiITH INERTTE _ g:�'Y�a •"- WASTE DISPOSAL METHOD: DISPOSE OF ALL CONTAMINATED MATERIAL IN ACCORDANCE WITH LOCM., STATE AND FEDERAL -. i"REGULATIONS. w - 7AANSPORTATIOM INf-ORMATION:'L;��: _ ' ONSULT EPA, DOT, LOCAL AND STATE REGULATIONS. SECTION VIII - SPECIAL PROTECTION INFORMATION RESPIRATORY - - PROTECTION: NOT USUALLY REQUIRED. SEE SEC.II & SEC.III ' PROTT_ECILV€GLOVE&US: CHEMICAL-RESISTANT lEYEPROTECTidioE GOGGLES GLOR FACE SHT-ELD GLOVES TO PREVENT PROLONGED CONTACT. WHEN CONTACT COULD POSSIBLY OCCUR. OTHER PROTECTIVEEQUIPMENT. KEE? CONTAINERS CLOSED WHEN NOT IN USE. WEAR CHEMICAL RESISTA:v'T CLOTHES, APRON & BOOTS WHERE CONTAMINATION MIGHT OCCUR. 1 VENALA710N SEE S£C.II. USE MECHANICAL VENTILATION IF NECESSARY. SECTION IX - SPECIAL PRECAUTIONS PRECAUTICNS TO BE TAV-N ,WHEN CANDLING OR STORING: Dp YCT :;L'DER OR PRESSURIZE CONTAINER. DO :v%. I i 3E--..:.__ .;LND 1 -i.. 'i 2 '1 .c _'i6-..._ -_ .f KFn.� fire �•yr •'.) • t�;l'j F M I. •tlN /•')YS.1 1�' Y• 1 4 -. .�'.'.�'•.�-...r—++'.«' .wJ.... C. �) - .":4 C;YY YI L 1 "i: :1• / i 14 1 1 /. • : ,Y" C! +Nf1 WA: -4 I I....I. / ! M I-,ca• .I;, _ i. :•:1• 1 I r :!`afy.•..y.��.1 :� -..;:p. i;i .: J'• i L4 el .. I "� -rie=i�`d i'7'fs-"i-^�-�f,_.: a�li•M 'I Ii a7' vi. -�;. 5'� �'iz�=rr f'..:kpf r. 1. 77 t b i-ANi NT YA"�..• Hyl r#moo;_ �:c*;i+r^+rrP.t ` �_9 ao -.-iii s I�\s w•r r� Y a�i:r s�:�)r��•., +•1` T^^� .gss��'Ieo® r• r r • • I t E� a �"O$ P�r IF SWALLOWED.. ,CAN CAIISCAT M SICrAN . h _ E a , NAIISEA, VOMITING VOMITING PROMPTLY i BY PAIITffT UNCOHSCIDU _•R, a ..��ry� r m_ctxx- . x�?egr pp - O p t .f - t - r^F. _ i C _d•. 'ter a �'afC U T x ANESTHETIC. RESPIRATORY TRACT. AFTER HIGH. VAPOR EXPOSURE RMVE TO FUSE �« E L MAY CAIISE SERIDII3 NEBVOIIS SYSTEM DEPRES— AIB. .IF BREATHING IS DIFFICULT GIVE x .` r Q � SION. MAY CAUSE DAMAGE TO KIDNEYS, BLOOD OXYGEN, IF BREATHING HAS STOPPED GI4Lt x F M NERVES, LIVER AND LUNGS. ARTIFICIAL RESPIRATION. r* XPRIMARY IRRITATION, REDNESS, TEARING, FLUSH WITH PLENTY OF CLEAN WATER FOR pp 'y BLURRED VISION 15 MINUTES. GET MEDICAL ATTENTION. o rs U R c PRIMARY IRRITATION, DEFFATTING, FLUSH WITH PLENTY OF CLEAN WATER. REMOVE r K DERMATITIS. AND LAUNDER CONTAMINATED CLOTHING. x rSECTION VII - SPILL OR LEAK PROCEDURES STEPS TO BE TAKEN IN CASE ISOLATE FROM OXIDIZERS, HEAT AND OPEN FLAME. STOP SPILL AT SOURCE. MATERIAL IS RELEASED OR SPILLED-WEAR PROPER PROTECTIVE EQUIPMENT. PREVENT ENTRY INTO SEWER OR WATERWAY. PICK IIP FREE LIQUID FOR DISPOSAL. ABSORB REMAINING MATERIALWIT_H_INERT____ _ r WWAASTEDIXOSALMETNOD DISPOSE OF ALL CONTAMINATED MATERIAL IN ACCORDANCE WITH LOCAL, ' STATE AND FEDERAL REGULATIONS, TRANSPORTATIONINPORMATION: CONSULT EPA, DOT, LOCAL AND STATE REGULATIONS. SECTION Vlll - SPECIAL PROTECTION INFORMATION RESPIRATORY r PROTECTION: IF VAPORS EXCEED TLV (See Sec II) USE NIOSH/OSHA APPROVED SELF—CONTAINED AIR PACK. r . PROTECTIVE GLOVES WEAR GLOVES IMPERVIOUS TO EYE PRC7?CT,ION: OS i9 APPROVED ---?LASH GOGGLES. SOLVENTS. OTHER PROTECTIVE EOUIPMENT: FOOTWEAR IMPERVIOUS TO SOLVENTS. r VENTILATION: USE MECHANICAL VENTILATION IF VAPORS EXCEED TLV. SEE SEC II r rSECTION IX - SPECIAL Pc--CAUTION-43 PRECAUTIONS TO BETAKEN WHEN HANDLING OR STORING: DO NOT STCFH ABOVE 120 Deg F. AVOID FREE FALL OF LIQUID. DO NOT ALTER OR PRESSURIZE CONTAINER. ;'CUND CONTA=`IER WHEN SOURING. Lin'BiLIT rTHE INFORMATION IN THIS DATA SHE=- HAS BEE' '•P ?E RE''- =i, -E SOURCES .AVAILABLE AT THE `14E i3' THE SELLER � Jk S1VvUt "R rJI\DIY='�dEJ ' ill fLTY OF SAN JUAN CAPISTRAN04 4Z APPLICATION FOR BUILDING PERMIT AND RECEIPT OF PLANS Building Address �� (�S �l OS Date 2/2 Tract Lot Type of Construction \/ N Occupancy Group 43 ,Z vD ' Owner t�OC./aG Ar0M 'rM )L.Ll S Business Phone 24o - 044-& ' Address Cw)G ( I 6c7 Home Phone 4ci 3 2 2l0 Architect Business Phone (;-4- Address C�Ld.lO Gh�Pf �1YL l�N?a ' Description of Work: p ►�/��l/J1 / uC / - ' Approximate Size of Building do ' Estimated Plan Check Fee $ By O� Plan Check Deposit $ 6 Date Paid ' Item Received By Date ' Plans y }� Energy Calculations 6 ' Structural Calculations - Soils Report OA ' Other: pL'A_ ' The undersigned hereby applies for a permit for the aforementic ` check deposit is a partial payment of estimated plan check fee: if permit is not issued. The exact fees will be computed and 1 prior to permit issuance. This application shall become null i not issued within 180 days of this date. One 180-day extension requested in writing 30 days prior to expiration of this applic renew action for an application after expiration, the plans shf a new plan check fee shall be paid. T4 i�n� c Si anat�;ral MW ' Thcr..as merreil , Director Ccmrnunity Planning and Development ' FRC:d: N . S . Cochran , Building Official SUBJECT: Notice to remove illegal structure - Solag On December 18 , 1984 , a "Stop Work" notice was issued to Solag Disposal Co . , 31731 Los Rios St . , citing them for erection of a ' structure without first obtaining a building permit , and requiring removal of the structure within 48 hours . -cllowinc discussion with Tom Tomlinson , Solag received permission : o '_et the structure stand during the permit application process . ' On January 9 , 1985 , it was noted that the incomplete structure was being occupied , and a second notice to "Stop Work" was issued . ' r structural analysis of the structure as it exists was made on January 10 , 1985 , which revealed that the structure under con- struction does not meet minimum code structural requirements ' and is , therefore , unsafe and will have to be redesigned and rebuilt if a permit is ever issued to build it. For this reason, a third notice was issued to Solag today, January 11 , 1985 , re- requiring the immediate removal of the structure as a matter of safety . This "Notice" was given to Solag at a meeting , a report of which is attached hereto for information. Solag will be monitored for compliance with the demolition order. N . S . Cochran ' NSC :ms APPLICATIO Fi+ ET y, ERMIT 4w0 ,VIC C£NVER DRIVE WEST SANT NA :.AI BUIE DING ` °• `.• nr • CITr AREA 3.�E. NJ�'Aal I AC�}JS [-�CA.�_ � r.< '.. -1�✓l�-_�_+-�.iJ..'LY`L--�.�___ .J NEAREST CRCSS STREET ADGFT LR OWNER m I VP9ROSCD / VRE$EFl rr, 'f RESYl? 4 v !•n [ Df 'CST CIES 5•r .A.,, SO,I�f FEET r 4AAALCS xrc R(9][n r . :Y 5 I ; 'A; 2 FT EECTR:• A::.IAN:—(5 NIRfS •L. Of :BUMF NCA. IAwROG', 1.1x v..'e•.[,-. V '• •J^: POND"-, S.vN rn: o0L_, 3.SG 616 TIME CCOC] 1 25 1 •I. < �� _ 5•LYS 6 L� 4,5 r'.:8[ C'4N11N4 ^' TC.� err - ' WORN w -w-^EYf CI ` c e ]LIOC-TED $TO,^'IROS ' n'9'NG 5,0:' SENFAdOw°-xO, LI RA •ICN MOORS AND TITIN STORM C R3 .'_ 1151 UMiiR M•:LL u±!L Sino MISCCClAREOtS AND IFf Or MCTORS � - .^ ♦ T / � Zr rbc SCI,'- -. y _ n.5 r G•• c t - CORSTR,KTIDY ORrEF, VOTE 2.50 TEMAJRA9v uNLEMG.LL,D RES. 5[RV:CE MElfx rRCS 4FNl A-Jx SIRc.RO_N- SER. CC 0 _ 4650 ! ! O25 SCR'• .E w(R° R50 r..! 12e FOR [A.. vC-E°_ I T eV h.c I GERI/iT 1551hY<E EAr °CS F, I,-r '10': 1 AAI 209 171,331 13.50'+ 3 2 a 1 ' APPENDIX III Orange County Health Care Agency Subject Site UST Records t TOM URAM DIRECTOR CAROL 0.KISER 4 NTY OF DIRECTOR OF ADMINISTRATION ' z 1 s 6FtANCme HEALTH CARE AGENCY CUSTODIAN OF RECORDS ' 515 N.SYCAMORE AVENUE,SUITE 120 SANTA ANA,CALIFORNIA 92701 FAX(714)835-9312 ' (714)834-3446 RE: 31731 Paseo Adelante San Juan Capistrano, CA. ' The undersigned declares: 1. 1 am the duly authorized Custodian of Records delivered herewith and have the authority to certify these records as to their authenticity. 2. The copies of records accompanying this Declaration are true ' copies of all of the records described in your request in this action to the extent I have them. 3. The records were prepared in the ordinary course of the business ' concerned at or near the time of the act, condition, or event which they depict. 4. The Health Care Agency may not be the only source of record. Please check with the Fire Department, the Water Quality Control Board and/or the State Department of Health Services. I declare under penalty of perjury that the foregoing is true and correct. Executed at Santa Ana, California this 20th day of May, 1991. A A diA 0S Jean-Mari eqa ' Custodian of Re rds Health Care Agency County of orange JML/gb 0020h ' Monitoring Procedure for Implementation of Alternative Number Five: Inventory Reconciliation, Tank Testing and Pipeline Leak Detectors. This monitoring alternative is limited to those tanks which contain motor vehicle fuel . You must submit a copy of a detailed monitoring plan outlining the moni- toring alternative chosen for each tank at your facility. You may use this checklist to submit the appropriate information, or you may submit your own detailed monitoring plan to the Orange County Health Care Agency. Keep a copy of this monitoring procedure on-site at all times. Return a copy of this monitoring procedure to: ENVIRONMENTAL HEALTH ORANGE COUNTY HEALTH CARE AGENCY ' PUBLIC HEALTH P. 0. BOX 355 Santa Ana, California 92702 ' ATTENTION: WASTE MANAGEMENT SECTION FACILITY NAME: So+w Zve ' FACILITY ADDRESS: f0C ' S.J.0 sem,.,, C1��. 4e, -'.24;73 FACILITY TELEPHONE NUMBER: '7i c/ �? g/o - o5416 ' KEEP RECORDS OF ALL INVENTORY RECONCILIATION INFORMATION ON-SITE. A. A calibrated dipstick shall be used to measure liquid in the tank ' daily. This liquid measurement shall be recorded on an inventory sheet. Daily meter readings for underground storage tank inputs and withdrawals shall also be recorded on the inventory sheet. Comparison of these measurements shall be calculated on the inventory sheet. A sample of the inventory reconciliation sheet you are using to log this information should be attached to this monitoring plan. Please send a sample log sheet with at least one week of inventory information ' completed. (See Sample Inventory Reconciliation Sheet - Attachment 1. ) Meters shall be inspected by the County Department of Weights and ' Measures or a device repairman as defined in the California Business and Professions Code, Division 5, Chapter 5.5 (Section 2644(b)) every two years. // ' Indicate date of last meter inspection // llf 7 Indicate the person responsible for measuring liquid in tank, logging information and calculating measurement error: Name: ?>c ?yJ� Title: OP7e7#-114 -, jbj' :ljs 03/16/87 1 Ti-Ec`.v 11 (6 / 8 1 � Allowable measurement error based on tank size: Tank Size Allowable Measurement Error 4,000 25 gallons ' 4,000 to 81000 50 gallons 8,000 to 12,000 75 gallons 12,000 100 gallons ' Indicate size of all fuel tanks located on-site and allowable measure- ment error: ' (For example: (1) 1000 gasoline - allowable error = 25 Gallons (2) 4000 diesel - allowable error = 50 Gallons. ) ' �/O OD'V - -7 l Y/4 / w ' If inventory reconciliation indicates a loss of the hazardous sub- stance greater than that specified, the following procedure shall be implemented: (See Attachment 2 - Section 2644(f)) tThe owner or operator shall , on a quarterly basis, submit a state- ment to the County of Orange, Health Care gency, that either: t (a) The data is within allowable variations, or (b) A listing of the dates and variation that exceed the allow- able variations. B. A full system (tank and piping) precision test is required annually for all tanks. Indicate date of last precision test for each tank on-site that is being monitored according to alternative number five. /01'7 /Z) 1 1 ' NOTE: A complete copy of the precision test results must be sub- mitted to Orange County Health Care Agency annually. 1 :ljs 03/16/87 2 1 r'b Vsl11F.1'r:JW4SAND(N1YAl,r LNTA(.PLANNf/15 17 Goldm Well BoFirpes PukEZY-CHFK WORKSHEET ' 15142 GoWm Wcu Circle - DATE: %YcFImin:wr.CA 91633 (714)9933333 Tank( : / tl3luc ) Tait Level: /G Product: �T a Cap: ) ,,r, � Chert Cali . ��5 /• ? 1 . _OUZ��()Q 's measured Gravity; Product Tempt 7 OF- Coe;ficient: x �/- Sr$ (p) •trcre•..•.rIrv}r�rfefrrrr�rrerr�rr•rr.eirrutrrA�rHurrrrPtfrur►rrrrr.r.rr.rrrrru�rrtrt.rrurras�..Yutrtr,rrettt��fA/rf�fP�. �. Level Level Ga�,4 t % A • Level Temp Temp Gain + %(H) Tamp TkMl v; Start End Lots - x(A) Result Start End Lose - x(e) Result Result Tisa i, x .c,Y32L/ V/ ! (J -UG ( x </, cifa Cj 1; ? l3,"UU: , x •vU?� - :OL/Ul - x� �,f'? --cJ / . ;07ST Ci, . , % .firr�'c:� . - !_,36 4/U� /C/!: ' c>uc, x l _ �y.� �J ( -r, ( ' '2 '52 - .': f l x u2'.! 04 G 4-1. c gG 7o - ^ / C? x•otJ :(.-12 SIU 5 IJUI - ' UUII % e-I• 0: 70 S - T %. '�7?,. '.—o 2GL ./ �� 7 w nraf/ X 7• rr 17.? - '. C)l Cl cl ft--,Or !S ♦'U; / SS � . f) ' x. ,tl'i! )�� 97 BSc/ , - C)Ci� x4/- 4ra . -pf�C S x .UUZ�I --ver 3Sc/ 35l 7r ,c3 xZ-/:5 ;= - !ii 7c,067. 'f!s 1 c 7s7, oS, System Certified in Coes liaace \ CA O e 4' Statton Location: f� j c ` y p Ye "�., with Local Regulatlonal F; 1r t .1 . A6008e1 3/ 73/ Ara . a„in tc. ��,Irt0e,1) Took Only Pagopol �\r r ort No. l .C'ty stoef tip II ' Prp urt Volume Delay T#met hrtt Chso9e par NoY +0?/r? h Cray; -7 I I Teat Start Tits{ c `/ Toot YSn1eQ TLpI �rJ: (/g, C. Specify the system or method used to monitor for leaks in the pipe- lines connected to the tanks. Check one : ' The suction system will be monitored audibly/visually for ' signs of leakage when the tank is used. Warning signs of leakage are: Mechanical Signs t -- Hesitation in delivery of motor fuel by the suction pump at the dispenser may be a sign of a piping leak. ' -- Rattling sound and irregular fuel flow in a suction pump- ing system is a sign that air is entering the dispensing system and mixing with the fuel . Air could be entering ' through a loose fitting or a hole in the piping. -- Dispenser meter spin without fuel delivery from a remote ' (submerged) pumping system may indicate a leak in the piping. -- Large discrepancy appearing only between the fuel amount on invoice and the measured amount in the tank after de- livery may indicate a leak in the fillpipe, or delivery measurement error. ' -- Display wheels skipping or jumping. -- The pump is running but not pumping liquid. ' -- The pump seems to overspeed when first turned on and then slow down as it begins to pump liquid. Environmental Signs ' -- Gasoline/fuel odor in soil near tank may be a sign of a leaking tank or piping. It may also indicate overspilling of fuel during deliveries. -- Motor fuel or its odor in underground sturctures such as basements or sewers may indicate a leaking tank. ' -- Clumps of dying or sickly plants on property near under- ground tanks may also point to a leaking problem. -- Motor fuel in drinking water wells or on the surface of ' streams, rivers and lakes ineicates a problem. Indicate who will be responsible for monitoring the suction ' lines daily. Name Title T— 1 ' 3/1 03/16/87 3 1 For pressurized system, provide a purchase invoice for in- stallation of leak detectors. (Please attach and submit to Orange County Health Care Agency. ) I have read and understand the foregoing information regarding implementa- tion of moniroing Alternative Number Five for the underground storage tank located at this facility, and will be monitoring the underground tanks accordingly. ' Nam Print ature D to 1 1 1 1 1 ' :1,75 03/16/$7 4 ' TOM CRAM DIRECTOR 4OUNTYOF FLANGE L. RCXEHLING, M.D. HEALTH DIrICLw l- 5 ``3 HEALTH CARE AGENCY "" TA ANA, ►'"LLT CPHO AMA, CA 91406 TCL : 714/931-7401 MAILING ADOME9 . r.0. ►Olt ))B BANTA ANA: CA 92701 ' PUBLIC HEALTH AND MEDICAL SERVICES ENVIRONMENTAL HEALTH UNDERGROUND STORAGE TANK MONITORING PROPOSAL 1 . FACILITY LOCATION Ill . TANK OWNER Facility Name fa o(gg 0 Nawe (Corp., individual, Street Address 3/7-3 ✓�+`'�'ven�Qe(d(.�- � public agency) %%f�"mys /2IVe�S� City I". J(L 9n/ [rJOiS flifii' ' Street Address 7?j' /�/Ik'6 k/,* Q Zip eW 12 &Z5r L City -4 '-� ... e/ -W States 9--.;?6 Zip i Phone Try R. FACILITY OPERATOR - Property Dlrner (if different from tank owner) Mame '10s , Business Phone -7/6,. Z —oqr(ed IV. INFORMATION Total Muuber of Tanks Located at this Facility Tank Selected Monitors Alternatir . Indicate y number Tank / Material and method the type of monitor�n9 system being proposed Stared Capacity' for faplementation. See attached excerpts from the (gallons) State Underground Storage Tank Regulations. 1 / Dt 'e >e I 10, 000 s 2 3 4 If aternative 2, 3, 4, or 6 is proposed for isVIementation, indicate the depth to first groundwater i ' OFFICE USE ONLY Proposal Approved By Date PAC. 1 P.O. 80X 1100 • SAN JUAN CAPISTRANO, CALIFORNIA 92693 • PHONE: (714) 240-0446 1 October 19 , 1987 i Public Health and Medical Service 1 Enviromental Health P.O. Box 355 Santa Ana, Ca 92702 1 ATT: Underground Storage Tanks 1 SUBJ : Underground Tank Monitoring and Testing 31731 Paseo Adelanto San Juan Capistrano , Ca 92675 ' Dear Sir: The following quarterly report is submitted: 1 "Inventory reconcilation has been done on a daily basis and the data attained is within allowable variations . " 1 In addition, testing of the diesel tank was accomplished on October 7 , 1987 . A copy of the test results are enclosed. 1 If you have any additional information, I can be reached at Solag Disposal, Inc. (714) 240-0448 Sincerely, 1b4olieb i 1 1 i HEKIMIAN & ASSOCIATES, INC. al -76 -70 - J. I YI.\:5C1.11A•G FSGINEERS AND ENVIRONMENTAL PLANNERS I � L Golden West Busircss Puk EZY-CHEK WORKSHEET 151,12 Golden Wen Circle Westminster,CA 92681 DATE: /o / 7 (7 141 895-5535 Tankl : 10 /t)C ) Test Levels H/A Products SP Cap: , Chart Cal , t•iS '/ J - -002�1�1A) Measured Gravity: ("l j Product Temp: 7-7 OF Coefficient: . v ,roc SS?' T s �,� /. S:r:, (8) r / / Temp. Cals .r,•.., /r;vax nrl c � •••••.•••••••••••••••••••u•••u.•u•uu•••uuu•uruur»urrrrru••rr•rrrr•rrrrrrrrrrurrrr•rrurrrur�u•ur•u•rr•••• Level Level Gain t x(A) Level Temp Temp Gain 4 x(8) Tamp Final Start End Loss - x(A) Result Start End Loss - x(8) Result Result Tina -7Ci I/ -; x _c702L1x 9 () 3 - - ? 7 x .pU2 - .�J� s � /�/lJ �/U�l - rJU � [ � r�. l : X /- l.r_ -G l 'CJ7�S �i X .rxt? l - (:.l' 6 /o�. yU<. - uU? % </ , r ? .. U 3 32 - / / x . u2(-r ' 026 //Lo //o5 - -.00 I x �/ C1q � - 7C'05 . 7C-)?/I/ SZ 70 - / c� x•OU-,/ =ot2W - VCJI - 7CUC," x �/. �, 'r:=' -7r1 / S S - vv� 7D SS —/ / x.ra' a A01 ' Or 7 - - CD(?,/ x �/ �ti : C) 0907 rte•+ / . t ,.��•� j 3W v rIC'l� % y• cY '�, v- CJ �,� ��P'`C)d�:T�p_3SL/ 35l -�x3 I System Certified in Compliance / ye �C� x \ Ck Station Locations SO )C q / y1-AW Sq with Local Regulations: �u JI ✓\\ t a y •• Address: �/ 7�/ �C cc ,s, „ C oL_ Tank Only Passeds Op 'rateors /1 r/e / -� Cc. r. ,Yt rsftrc•no No. .City State Sip (Yes/No) �, �.(Stgriature) Product Volume ``=�--- Delay Time: hrs. Reason: Change per Hour: '� U GCrews /.Z re- Test Start Tissas �-r r/S"a 15 /e t=/ _ Test Finish Time: /U: el-.—r,p, MIT- PART V BUSINESS SITE PLAN B. FACILITY LAYOUT MAP y L Location of Material Safety Data Sheets (MSDS): 6a� O� C --P fTISi S f O 'PArStCp �'7G L M.l�i-p - P#r5S-o PeVIS -M 9 Uo + Y (u�vnt'EV RL. ALt`6J 1 114tlK k-D TOO �Y-sf�- Fi�! fire itse� eT—_ S.LV�+T +s� Di¢ulbs �r1oT I u ❑ �--- w n s rt �: I h+6sv�cG�D C Z,Co n (� s OIL V12�31�N9 'j'►�K SSUo'.� l4�ea y STC�rc� ' Ya"Mtk6 T f Y�ae,p .S �D �J Pa�Mf ►"L �otV�- ' F (flammable) C (corrosive) E (explosive) P (poison) 0 (oxidizer) R (radioactive) W (water reactive) r ' HAZA 9 TOM URAM _ \ DIRECTOR OIJ NTY OF' RANGE L. REX EHLING, M.D. HEALTH OFFICER \\2 `1 HEALTHCARE AGENCY 1>3s WEST ANA. 92706 SANTA ANA, GA 93)06 ' TEL[PHON[: 7141234.7 MAILING ADORES P.O. BOX 355 SANTATAA ANA; CA 93703 PUBLIC HEALTH AND MEDICAL SERVICES ' ENVIRONMENTAL HEALTH PERMIT TO OPERA�INSTALLATION APPLICATION FOR: COMPLETE P I A 2 i (Check One) FAFILITY MODIFICATION DATE COMPLETE PAGE I 0 FACILITY INFORMATION I TYPE OF CONSTRUCTION 'N-AME_�_�1 a,�i—��u .-a-<—.._{' �c_ ! INDICATE NO. OF TAW( S ) STREET ADDRESu S 317 >j( (7 �0 / .,,,}-o INSTALLATION( S ) (COf,PLETE PAGE Z ) 'CITY �r..p(( REPAIR(S ) /RELINE(S ) II NSTTALLLT IKON/REMOVAL ATFTHIIS LOCATION 1_ CLOSURE(S ) /REMOVAL(S ) 'TYPE OF BVSINESS GASOLINE STATION SYSTEM MODIFICATION ( E .G. REP PI FARM OTHER (SPECIFY) GOVERNMENT _ OTHER tEPTH TO FIRST GROUNDWATER FT. TANK OWNER I ZA HOUR EMERGENCY CONTACT PERSON E ( CORP. , INDIVIDUAL, PUBLIC AGENCY ) DAYS p N 1 n --n_•� -�-"C NIGHTS TREET ADDRESS u M L Pn N 1 L I NG ADDRESS L; . �� 1 1 0-0 �1 APPLICANT �l TATE (� ZIP ! Z NA/.tE �E NO. -7/l{ ' 340 '� �Y' 46 PLEASE PRIM SIGNATURE COMPANY NAME CILITY OPERATOR CONTACT PERS CIE +rC� b PHONE NO. 13,-(-- Go I N E SS Pf-IONIZE NO. pyDL Y o - C 4�k /�� Aqp E NEW I NLS TOOAD T 1 1 •TU��T RE IAL N N T I ATIAN ANY CONSTRUCTION SOR MODS F«I CATD I UVS���LAJNS MUSSTORAGT BE APPRVE� PR OFFICE USE ONLY 'FACILITY PERMIT NO. / '7-J "r PLAN APPROVAL DATE BY NO. PLAN CHECK NO. FEES FIELD INSPECTION DATE 'NUMBER OF TANKS TO BE BILLED SURCHARGE BILLING REV. 07/ Z0/07 ' T A N K I N F O R M A T I O N TANK I. 0. #1 #2 #3 #4 IF MOTOR VEHICLE ' T T FUEL, PLEASE PROPOSED R R SPECIFY THE 1 E GRADE CURRENTLY L D CAS NO. ( IF TRADE SECRET, PLEASE STATE TYPE TANK, SUMP, OTHERS ' C DOUBLE WALL SINGLE WALL I GGZ/ YEAR MANUFACTURED INSTALLED / ( OI Z VAULTED NOT VAULTED N I MANUFACTURER y / ' T P CAPACITY GALLON 'IV WU7 M CONSTRUCTION MATERIAL �L Al A Y THICKNESS UNITS / ' 1 LINING/COATING !� EXTERIOR INTERIOR 7 NJ MANUFACTURER 67-7 E CAPACITY GALLON 7 I N CONSTRUCTION MATERIAL 5 R R THICKNESS UNITS Y LINING/COATING EXTERIOR INTERIOR ' TYPE OF LEAK DETECTION / AND MANUFACTURER P LOCATION (UNDER/ABOVE ' GROUND I SUCTION/PRESSURE GRAY I TY UNKNOWN P I CONSTRUCTION PRIMARY MATERIAL 1 MANUFACTURER ' CONSTRUCTION N MATERIAL 7 SECONDARY G I MANUFACTURER 7 TYPE OF LEAK DETECTION AND MANUFACTURER OVERFILL/SPILL CONTAINMENT, J ^ PROTECTION TYPE A)o ' FOR TANKS INSTALLED PRIOR TO I / 1 /84 SPECIFY THE MONITORING S SYSTEM ATTACH A DIAGRAM ( 8 1/2" X 11' ' ) INCLUDE THE LOCATIONS OF THE UNDERGROUND STORAGE TANK(S) , PIPING, AUXILIARY EQUIPMENT, BUILDINGS AND OTHER LANDMARKS. _2_ 1 COUNTY OF ORANGE/HEALTH CARE AGENCY Fm� /f r�t"'A' � ENVIRONEMTNAL HEALTH ( 714 ) 874-8175 1 � I ' - 1725 WEST 175H STREET, P.O. BOX 755 SANTA ANA, CA 92702 UNDERGROUND TANK INSPECTION FORM �so /-- PERMIT NO. : FACILITY NAME: S[J d A 21592!'5,20 INSPECTION DATE: STRE@T: � ®Q.SQn �(� e lQ r MAP CCORD I NATES: ' CITY" ZIP: y DISTRICT: {p ' NEAREST CROSS STREET: J/Pil D�J 1!SOT� PHONE: qlq ),:�qG EX CODE: ) STATUS : L PUBLIC AGENCY: ' CCM•PL 1 ANCE : PERMIT DATE: _/_/_ UNDERGROUND: 1 . GAS STATION 2 . NOT GAS STATION STATE VARIANCE: ] NUMBER OF TANKS THIS LOCATION: DEPTH TO WATER TABLE: (FT. ) ' DEALER SUPV. : IONS{ PHONE: TANK OWNER (MAILING ADDRESS) ,J NAME: 7 /LD M 1 i :5 ( 1 (4-1 t6 _ PHONE: (-/l7 STREET: ?�-i•' II ��/j CITY: Y -3 ,g 6npi 4fA LU ST: �� ZIP: / ' 75- EMERGENCY CONTACT �PERSONS `` NAME: AJV /�Yl'!-YGll, l.(S _ _ PHONE: NIGHTS: PHONE: ( ) E1I.G�VLP 1 ' INSPECTOR #: 173 SIGNATURE: ��N//T //} (Yf21�IJ!-� DATE: t- ' RECEIVED BY: �1/ice /�/ /�.6.CJ DATE: ELAPSED TIME: -5-0 (MIN. ) PAGE 1 C5- rY OF ORANGE/HEALTH CARE AGENC( EN-RON4ENTAL HEALTH (714 ) 834 - 8175 1725 WEST 17TH STREET, P.O. BOX 355 SANTA ANA, CA 92702 1 LINDERGROL^0 TANK INSPECTION FORM 1 FACILITY ACCOUNT NO. : { ,�I.) 7 PERMIT NO. : HCA TANK ID: co I FAC. TANK ID: DATE INSTALLED: 1 STORED: CAS #: DCD r 19`!3 O NAME: A e—p-p T/S: TANK CAPACITY: IO Dov PREttSSLIRE/ Y 1/GRAVITY: , TANK CONSTRUCTION MATERIAL: ( 1 PIPING CONSTRUCTION MATERIAL: TANK MONITOR: [ _2J PIPING MONITOR: �� /�i H/9 MONITORING OPTION: S 1 VIOLATIONS: OTHER: IHCA TANK ID: FAC. TANK fD: DATE INSTALLED: STORED: CAS L: NAME: T/S: TANK CAPACITY: PRESSURE/SUCTION/GRAVITY: 1 TANK CONSTRUCTION MATERIAL: PIPING CONSTRUCTION MATERIAL: TANK MONITOR: PIPING MONITOR: 1 MONITORING OPTION: VIOLATIONS: _ OTHER: 9ICA TANK ID: FAC. TAMC ID: DATE INSTALLED: STORED: CAS NAME: T/S : _ 1 TANK CAPACITY: SSURE/SUCTION/GRAVITY: TANK CONSTRUCTION MATERIAL: PIPING CONSTRUCTION MATERIAL: J TANK MONITOR: 1 PIPING MONITOR: MONITORING OPTION: 1 VIOLATIONS: OTHER: HCA TANK ID: FAC. TANK ID: DATE INSTALLED: 1 STORED: CAS n: NAME : T/S: TANK CAPACITY: PRESSURE/SUCTION/GRAVITY: TAMC CONSTR ION MATERIAL: PIPING CO TRUCTION MATERIAL: 1 TANK M ITOR: PIPI MONITOR: MO ITORING OPTION: iVIOLATIONS: OTHER: J NSPECTOR (I: ? S 1 GNATURE: r(��GYyl�1.I�/ ECI ✓K DATE : L� RECE I VIED SY: i//-�.a2�l�i (J� i// ,�.e DATE: 1 ' PAGE 2 ENV Ii -'MENTAL HEALTH ( 714 ) 834-8175 r 1725 :ST 17TH STREET, P.O. BOX 335 SANTA ANA, CA 92702 UNDERGROUND TANK INSPECTION FORM �C I I-I TY ACCOUNT NO. _I - &y PERM I T NO. ' VIOLATION DESCRIPTIONS �3 OPERATING UNDERGROUND STORAGE TANKS (UST) WITHOUT A PERMIT - SECTION 25284(a), HSC 0 UNREGISTERED UST FOUND ON SITE - SECTION 13173 WATER CODE 13 FAILURE TO REPORT THE CHANGE IN OWNERSHIP WITHIN 30 DAYS - SECTION 2712(f), CAC I0 FAILURE TO REPORT THE CHANGES IN THE USAGE OF UST WITHIN 30 DAYS - SECTION 2712(a) , CAC 25 FAILURE TO REPORT UNAUTHORIZED RELEASE - SECTION 2650(b) , cAc 30 FAILURE TO DEVELOP A RESPONSE PLAN TO REMOVE THE UNAUTHORIZED RELEASE FROM THE SECONDARY CONTAINER - SECTION 2632(d)(2) , cAc 5 FAILURE TO ENTER INTO A WRITTEN CONTRACT BETWEEN OWNERS AND OPERATORS TO MONITOR �— THE UST - SECTION 2610(b), cwc D INPUT AND OUTPUT METERS NOT INSPECTED BY THE COUNTY DEPARTMENT OF WEIGHTS AND MEASURES OR A DEVICE REPAIRMAN - SECTION 2644(b) , cAc 43 FAILURE TO MONITOR THE FACILITY USING THE METHOD SPECIFIED ON THE PERMIT - SECTION 25293, Hsc '0 FAILURE TO MAINTAIN THE WRITTEN RECORDS OF ALL MONITORING PERFORMED ON SITE FOR AT LEAST 3 YEARS - SECTION 2712(C), CAC 1 5 FAILURE TO MONITOR MANUALLY AT REWIRED FREQUENCY - SECTION 2642(c) , CAc 0 FAILURE TO SECURE THE MONITORING WELLS - SECTION 2648(7), CAC S CONTINUOUS MONITORING DEVICES INOPERABLE - SECTION 2632(c)(2)(A) , CAC 70 -- FAILURE TO CORRECT PREVIOUS VIOLATIONS WITHIN 30 DAYS - SECTION 2712(8) , GAG ,5 FAILURE TO PROPERLY HANDLE, STORE, OR DISPOSE OF A HAZARDOUS SUBSTANCE - SECTIONS 25154 a 25189, Hsc, 66300, cAc Arrc FAILURE TO CLOSE UST PROPERLY - SECTION 2670-72, GAC 80 FAILURE TO REPAIR UST PROPERLY - SECTIONS 2660-63, CAC WATERTIGHT COVER NOT PRESENT - SECTION 2635(c) (f) , CAC— — — — — — OTHER (/_7 tilIE""IT-lo �2 CDt-ojs e,&d1V eXQ 411 /Ir/71- -Fn r -J aYLu — o h r Ice o0 llnc. nlc��r Ur, ia >Prr rulldnux 4--Np Gt(( ocv"(2 ACL -k � _ _ _—h 3 V�7 �qj P c4lL'-t ,/(:a Tl cxfi O /j_ 1 \ C LECTOR IF: 1''7 SI ,�SSS�II GJJNATURE: DATE: �E I VED BY: // /CC.i'C2 �I DATE: PAGE 3 �09/2S/tt THIS PERM[- UST BE POSTED IN A CONSPICUOUS' ;ATION ORANGE COUNTY HEALTH CARE AGENCY PUBLIC HEALTH / ENVIRONMENTAL HEALTH PERMIT TO OPERATE UNDERGROUND STORAGE TANKS PERMIT NUMBER NUMBER OF TANKS OPERATED ISSUANCE EXPIRATION 'RJfiGt4-i UNDER THIS PERMIT i DATE 11 12-87 DATE 11-12.-92 ' SOLAG DISPOSAL INC St`LAG DISF'?+SAL TONY Ki?N 'L . S 31731 PASEQ ADELANTO P E Ov i 1:J5J SAN JUAN CAPISTPANO. S J !-API'3TRr.NO. _-ii '726 ' 92675 _,t? vr,dF•r Ur c-und ,ragY_ 7. riI+� .:r_ tc`d at i t S- f3i-:ils'_ arazper mittr`� L- _cerate orcvided the foll`.winc =unditicns-ar- Comclied with ! r . 1 . ,The followird chane sn-ttr iasaec of lin underor and ae tank must be reoorted withirl,.tpirtg '3,5)T-da, %the Uncieetg de Tank A. T.he ci;r:r3C:•,',Csii new nam aFdC.15 s.lL tet,ar,r e5. critorincior :edures '. ' C. The ra T Fnt or reuair of "alI 'or p' + h c cern_ ar, of any'undFrarr, r:j stnracF tank. _r ationner_t d -thereto. + �r.Y CI 2 . All urla,lthlrf,y ied releases must be reported withi ii,_Z hours o t4 ^I ' Program . V . Written r dsrtE ail" monitorinc-Derforrned"s`aI: be ;uaz naaTned\c It for a peri_4af at: least 3: years from the date the, monit rine was- oerafcrrned. The a,i^ltter rekcrds of all monitoring rf"rmed ir"tF� st .i ,jesrs shall be shown to tn� , - Pr"-am Staff ?DrssentatiI es f`111e USI Proor-- � , s4te ' sw -urx,n reyQest � r:r:.; any _ inspect;t:n. 4. . 'f �wnershio 'of' tha r�nder,�^:�..:;,� -,ar,k( is '.^=-.s. .. . the -:aw- �y ser a- `a r : r t•r' r�7. C _ J - C-♦I St r _ an. Pr:c, ,a, ithi., r,y _ c: nano_ -. -t ...r : s t or ,r.k our;e x. the _nc - c.qr_r, - �.._-uit r _n_. �t. as, ,.P:, _�;� for _zairar, i .n _i Derrrrt , ' Sec t.ior, =52-99 ; ?.r,:. -IS 1ifor-�ia Heaitn arid Ssfst`_ rode states that vTnc_r= and oc,eratt ors c,f trader 7m1 e• ?C - r: - i. per._.1t ;mss r::t less than F4 ve H'k, - � __ - _ 'h?-i,JJ? f'n:r.5 �'3Ci :'lYe .-._ i7 ��' _r v 1s r : _ rird tions :,F t4 . other or .vi i- r., •. f r r _�. !, y t s i4-yl1(11 .^!V'C:`ITt:� TG.0 :¢C ' UNDERGROUND STORAGE TANK PROGRAM OFFICE ADDRESS: 1725 W. 17TH STREET, SANTA ANA, CA ' MAILING ADDRESS: P.O. BOX 355, SANTA ANA, CA 92702 TELEPHONE (714) 834-8174 FO'P2-H.t 628,t TOM URAM ' DIRECTOR Q � COUNTY OFFtANGE L. REX EHLING, M.D. O HEALTH OFFICER 2.. \ s ' SAWEST 17TH STREE HEALTHCARE AGENCY •�� SANTA ANA, CA 13]0{9 TELEPHONE: 714/034-7 ' MAILING AOOR ESSi P.O. BOA 293 SANTA ANA: CA 92703 PUBLIC HEALTH ENVIRONMENTAL HEALTH ' APPLICATION FOR: PERMIT TO OPERATE/INSTALLATION (Check One) (COMPLETE PaGE 1 & 2) DATE: tl 2 3 777 ll FACILITY MODIFICATION t (COMPLETE PAGE 1 ) ' FACILITY INFORMATION TYPE OF CONSTRUCTION NAME: Drs AeSle 1 �•N r i ND 1 CATE NO. OF TANK(S): STREET AID`DRESS: 3/73, f1Y1hs �.Ir l /1 I INSTALLATION(S) (COMPLETE PAGE 2 ) ' CITY: '�4.�..,,, �i9�s/•�Sb�ra' yE�- I j REPAI R(S)/REL INE(S) Cl.T 07Y TOTAL N1�MBER ppFF TT AFTER CLOSURES)/REMOVAL(S) INSTALLATION/RErdOV I14`TMIS LOCATION _ - TYPE OF BUSINESSS: GASOLINE STATION SYSTEM MODIFICATION (E.G. . REPIPE) a FARM OTHER (SPECIFY) GOVERNMENT x OTHER ' DEPTH TO FIRST GROUNDWATER FT. a ' TANK OWNER 24 HOUR EMERGENCY CONTACT PERSON NAME (COPR. , I ND II V I DUAL, PUBLIC AGENCY) : I DAYS: A^fjlZGM/5 71Y y.(VafYVT yCPHOINK ' /J NIGHTS: STREET ADDRESS: �i/�3r /��52/0 �G'-rI�U- NAmZ TELEPHONE MAILING ADDRESS' ,J ' CITY: Lf'I7 ,¢(✓ ., moi'&-7} APPL t CANT 7L,& - L •� NAME : x G--'r STATE: ZIP: 77 rr�/ //// L ' ?FiCX.1T= ice. : 7/SCS p` T� `Q 76T I SI C7•WTURE: COMPANY NAME? FAC 1 L 1 TY OPERATOR (CONTACT PERSON) PfIO'E NO. : -7i V NAME: m•.1 HnL 1,y G✓l�, [is r/ 7 1 BUS I NESS PHONE NO. : 1V' �Q ' 0 7�rf . AT I NOTE: MOOff BE D PRIOR TO THE IN1TFA ION OF ANY POOIISTRUPYSTEM CT ON�aRIV 8=CII�ATIF �PL OFFICE USE ONLY ' FACILITY PERMIT NO. : PLAN APPROVAL DATE: BY: NO. : PLAN CHECK NO. : FEES: FIELD INSPECTION DATE: NUMBER OF TANGS TO BE BILLED: SURCHARGE BILLING: REV. 10/09/87 T A N K I N F 0 R M A T I ' 11 , TANK I. D. #1 #2 #3 #4 IF MOTOR VEHICLE ,AA 7S7�� FUEL, PLEASE PROPOSED ' E O SPECIFY THE RI E GRADE CURRENTLY DIE'Sr/ L D CAS NO. ( IF TRADE SECRET, S PLEASE STATE) r'Ir3" ' TYPE TANK, SUMP OTHERS 'IAN j( C DOUBLE WALL SINGLE WALL �N I,( ' YEAR MANUFACTURED INSTALLED Lw. O VAULTED NOT VAULTED pf ppu ' N MANUFACTURER T P CAPACITY GALLON & bsp M CONSTRUCTION MATERIAL .S TKe ' A Y THICKNESS UNITS 1 LINING/COATING �7fy�or7 1 EXTERIOR INTERIOR TOi Clad ' N MANUFACTURER N E COE CAPACITY (GALLON) ' DN CONSTRUCT1CN MATERIAL N /} R Y THICKNESS UNITS ' LINING/COATING _ (EXTERIOR/INTERIOR) N TYPE OF LEAK DETECTION AND MANUFACTURER p LOCATION (UNDER/ABOVE _ GROUND) &"4 I SUCTION/PRESSURE ' GRAVITY/Uh84VOWN 5 �`h P CONSTRUCTION PRIMARY MAYER i AL ' I MANUFACTURER CONSTRUCTION N MATERIAL SECONDARY ' G MANUFACTURER TYPE OF LEAK DETECTION AND MANUFACTURER ' OVERFILL/SPILL CONTAINMENT, PROTECTION TYPE FOR TANKS INSTALLED PRIOR S /tiCl�r tms/ TO 1 / 1/84 SPECIFY THE MONITORING ;y7 LIN 1 ' SYSTEM I 2a8- /f7IY}ri( ATTACH A DIAGRAM 18 1/2' ' X 11' ' ) INCLUDE THE LOCATIONS OF THE UNDERGROUND STORAGE TANK(S) , PIPING, AUXILIARY EQUIPMENT, BUILDINGS AND OTHER LANDMARKS. Lill ' �1EAL111 C, h'c ,;Gtiv r Erv:rcCTcc AJ Heath UTOM URAM DIRECTOR COUNTY OF RANGE L. REX EHLING, M.D. O HEALTH OFFICER e \ KY HEALTH CARE AGENCY J2S wE3TSANTA ANAA..C7THA, C RE92J0404 ,\ TELEPHONE: 7141934.7201 MAILING ADDRESS: P.O. 30% 233 SANTA ANA;CA 92702 PUBLIC HEALTH ENVIRONMENTAL HEALTH 'PLICATION FOR: PERMIT TO OPERATE/INSTALLATION (Check One)' C _ /] (OOAPLETE PGE I $ 2 ) DATE:(x\ FACILITY MODIFICATION (COMPLETE PAGE 1 ) FACT L1TY INFORMATION TYPE OF CONSTRUCTION NE: SO�h�� s. gl SAI?Arco NO. OF TANK(S): , STREET ADDRESS: 1 �( .���1 1"Arco A3alynl-o INSTALLATION(S) (CO[.PLETE PAGE 2) ,ITY: .SSt.y+ciu��. - AEPAIR(S)/RELINE(S) TofAL N)MBER OF TAMS tAFTER INSTALLATION/ CLOSURE(S)/RIEMOVAL(s) REMOVAL) AT THIS LOCATION: SYSTEM MODIFICATION (E.G. , REPIPE) E OF BUSINESS: OTHER (SPECIFY) ' GASOLINE STATION FARM GOVEYINIM£Ni OTHER OBNER �j 24 HOUR EMERGENCY CONTACT PERSON INDIVIDUAL. PUBLIC AGENCY) DAYS: l�o.�fAS f`V�IS M E TELEP14ONN ET ADDRESS: SStbt CAnw•n0 CAfh-r�l^^J G NIGHTS: A TELEFRIME ITY: ..S S GP• I ATE: �.^ nnA ZIP: "12-G-7S APPLICANT TELEPHONE NO. : 7 0-YO — Q IV? NAME: 0 PLICASM PRINT I LL NG ADDRESS INFORMATION SIGNATURE: T1 LL TO NAME: COMPANY NAME: ILL TO ADDRESS: TELEPHONE: TY: ATE: 21P: FACILITY OPERATOR (CONTACT PERSON) TELEPHONE NO. : NAME: BUSS?I N ESMS�TELEPHON TETDILEPHONE : NOTE: e� w"��d"taR 7 L 1 w idN��F wrl�r c�f7s'1�Ru' rf& Bi§NUNDW ASN�M ' OR FIAT OFFICE USE ONLY ILITY PER MIT NO. : Soc-/ PLAN APPROVAL DATE: BY: ND. : 1N1 CHECK NO. : FEES: FINAL FIELD INSPECTION DATE: JMBER OF TA14 S TO BE ADDED TO B 1 LL I NG: NUMBER OF TANiCS�R €.1 WfLt 9:03/04/88 S ' (-' TANK I NFORMAT I Or -2- ' TANK I .D. #2 #3 #4 M 1F MOTOR VEHICLE CURRENTLY Df 1443 ' A FUEL, PLEASE ET SPEC 1 F.Y THE PROPOSED I GRADE PREVIOUSLY ' S CAS NO. ( IF TRADE SECRET, PLEASE STATE TYPE TAMC SUMP. OTFERS TANK ' DOUBLE WALL SINGLE MALL .Sln It 6� C UL NUMBER Iq ' YEAR INSTALLED at O VAULTED NOT VAULTED N V N MANUFACTURER q9 ' P T I CAPACITY GALLON OJl7Q A Y CONSTRUCTION MATERIAL ' THICKNESS UNITS 014 I INTERIOR LINING IM ' N I MANUFACTURER q 7 CAPACITY GALLON 4 7 E AR CONSTRUCTION MATERIAL q7 R Y THICK ESs UNITS g 7 CORROSION PROTECTION -I ' Z)XER7ETCZJ.Uf DETECTION (LIQUID, ^V ate /2 MANUFACTURER OF LEAK DETECTOR l 7 LOCATION (cm�R w•Iu1ABOVE P)GAR P tW 11r°NrOa M v 1 CONSTRUCTION PRIMARY MATERIAL t ' P MANUFACTURER q-1 I SECONDARY MATCONSTRERUCIAL TION W ' N f2 MANUFACTURER G VYPF OFELE DETECTION (LIQUID, Q 7 ' MANUFACTURER OF LEAK DETECTOR OVERFILL PROTECTION TYPE / 1 ' SPILL CONTAINMENT qy ATTACH A DIAGRAM ( 8 1/2" X II •' ) INCLUDE THE LOCATIONS OF THE UNDERGROUND STORAGE TANK(S) . PIPING, AUXILIARY EQUIPMENT, BUILDINGS AND OTHER LANINAARKS. OFFICE USE ONLY MONITORING SYSTEM ALTERNATIVE 51 1 v/na/2t /aa l a.:C'�r:I',li`v' -iF Cof�ANc18 / I--i'l-nL—TH ENVIRONMENTAL HEALTH ("4) 874-8175 1729 WEST 17TH STREET. P .O. Bi- IX 355 SANTA ANA. CA, 92702 IERGROUND TANK INSPECTION RUN DATE 18 AUG 1988 PAGE 1 IOUN? N0: .95$477 PERMIT: 95$4-$ LAST INSP DATE: 11/17!87 ILIT SOLRG DISFOSr1L INC EX .C:D: 1 STATUS: 1 PUB P.GC'Y: ......... (REBAY! ESS: 31731 FASEO ADELRNTO UST DISTRICT: 15 PROGRAMS: UST S J CAPISTRANO- CA 92675 IN3P. TYPE. ..... -91 Y: 119 7 SAN JUAN CAPISTRRANO REST CROSS STREET: DEL OBISPO MAP COORDINATE: 38-C1 LERJSUPV. : TONY KONTROULIS PHONE: 714-240-0448 OF TANKS THIS L'JCATION: 1 DEPTH TO WATER TABLE: ............ (FT) COMPLIANCE: $ ITE VARIANCE: C I TYPE OF BUSINESS: C 21 NOT A GAS STATION - 1 L - TO NAME: SOLAG DISPQSAL INC TO STREET: F0 BOX 1100 1 " L TO CITY: S _APISTRANO STATE: CA ZIP CODE: 92693 �K OWNER )BA: SOLAG DISPOSAL UT: PO BOX lIC40 S J CAPISTRA.NO STATE: CA 71- CODE: 92693 -ACT: BOB GOTTLIED PHONE! ...............-............ .................. ,E.. �.":�C•i F'EFi^O J'= , , ?: Ti�t�.' .<ONTRiiULI - -'IiNC_. 714-24YJ-63448 ......................_............ FHONE. ............ — — ...................................................................................... ,STPNDING FACILITY 'VIOLATIONS DOTE INSP BY TYPE TANK ID VIO CODE DESCRIPTI"IN ABATED FSED TIME ....... .....-..(MIN) .-PECTOR #: " ../. .�/............ �.. ... SIG�NJATU/RE:� / .................................. DATE: ...�. j...... ......_ ,.. ..rV.. _VFD 5Y: DATE! .............. F( ' ENVIRCiNMENTRL HEALTH (714; 8-14--3175 1729 WEST 17TH STREET. F.O. EiCIX 7155 SANTA ANA, CA. 9^702 URGROUND TANK INSPECTION RUN DATE 18 AUG 1988 PAGE 2 PUNT NO: 9504 SOLA.!, DISPOSAL INC LIST INSP DATE: 11/1%87 TANK ID: 001 FCLTY TRNIF; ID! .............._............................. YcRR INSTALLED. .....I.... TYPE: 2 ■tTCIRED: DOT1993-FO NAME: DIESEL FUEL K-FUEL OIL T/S: C 7 TANK CAPACITY: 10000 (GAL) SUC?ION=1/GRA'VITY=2/PRESSURE=17 : C 11 TANK CONSTRUCTION MATERIAL: 11 1 STEEL ,'IPING CONSTRUCTION MATERIAL: 11 1 STEEL ANK MONITOR: E2 7 INVENTORY RECONCILIATIAN PIPING MONITOR: C97 1 NOT APPLICABLE MONITORIN- OFTiON: C5 1 INVENTORY RECONCILIATION. TAW, TE REPAIR DATE: .........../.........../........... t!LAT I nNi: ..._................................_............................................._.._............... 07HER: TANK ID: .................................... FCLTY TANK_ID: ..................... YEAR INSTALLED ............ TYPE ...... -Tl RED: NAME! ................................................................................................................................TIS: .................. TANK CAPACITY: ........................................................................(GAL) SUCTION=1/GRAVITY=Z/PRESSURE=3 ANK CONSTRUCTION MATERIAL: C 7 .............._........................................................................................ .................................._...._. FING CONSTRUCTIONMATERIAL: C 7 _.......................................................................................... TANKMONITOR: C I ......................................-.............................................................................................................................................. IPINGMONITOR: C 7 ..................................................................................................................................................................................... C:NIT!ORING OPTION: CI.. . ..... REPAIR DATE: .........._/.........._ ........_. / : ......................................................................................... PLAT I ONS: ......................................................................................................... OTHER: ......................................................................................................... tTANK ID:' ...................................:... FCLTY TANK ID: ..................... YEAR INSTALLED ............ TYPE ...... STORED: _........................................... NAME: ._T/S: �AN1< CAFACITY: ................:......................................................ttsRL) SUC:TION=1/GRRVITY= !PRESSURE=, :..........._....................... ANKCONSTRUCTION MATERIAL: C 7 ................................................................................................................................................... rIPING CONSTRUCTION MATERIAL: E 7 ................................................................................................................................................... ANKMONITOR: C 7 ........................................................ ....................................................................................... .............................. :PIN'G MONITOR: C 7 ............................................................................................ . .................................................................................... ONITORING OPTION: C7.................................................................................................. REPAIR DATE: ............/............/............ LRTiONiS: ........-.._......... OTHER, �� :R TANK ID: ....................................... FCLTY TANS: ID: ..................... YEAR INSTALLED ............ TYPE "LORE": ........................... ............................................. NAME T; ................................................................................................... : .................. . . ANK CAPA_ITY: ......................................_............................_(GAL) St!CTION=1!GRR'•1'_TY=2/F'RESS:;RE=' ........ ANK CONSTRUCTION 7! ...-...................................................... PIPIN3 CONSTRUCTION MATERIAL: C ] .......................................................................................................................................:........... ANKMONITOR: C 7 .................................................................................................................. .............................................._.................... IPINIGMONITOR: C 7 ....................................................................__............................................................................................................... MONITORING OPTION: C 7................:.................................................................................. REFA.IR DATE: ............ ILATIONS# ................................ OTHER: ......................................................................................................... 1 lPECTOR #: ...L.../.L............. SIGNATURE: J.�Jjj.._..._........................... DATE: / 'FINED $Y: _........ ar. ._.... . .. DATE! �J....(/_3. 400 r Efl'..I��!NMENTf!l. f�ERLTH (7'.4i 8�4-8i�5 !JE.=T 17TH STRE7 . F'.ij, HiiX 'S5 St-)NTA ANA. CO. 72702 tEfiCnUUND TANhi I`dfF'ECTi>>nl RUN PATE 18 AUG 1588 F'AGE r rVIOLATION DESCRIPTIONS CILTTY r_ M OPEtJ TING UPLER6n+TJM) STORAGE TANKS (USM WITHOUT A PERMIT - SECTIO,N 25284(a), HSC 115 FAILURE TO FORT THE CHkNGE IN OWN'E,SHIP WITHIN 39 'JAYS - SECTION 2712({). CCR 139 FAILURE TO DEVELOP A RESPONSE PLAN TO RFV'rt TIE UNAUTHORIZED RELEASE FROM THE SECONDARY CONTAINER - SECTION 2632(d)f2)., CCR 135 FAILURE TO ENTER INTO A WRITTEN CONTRACT BETWEEN OWNERS AND OPERATORS TO MONITOR THE UST - SECTION 2618(b), CCR 149 ME?ER3 NOT INSPECTED BY THE COUNTY DEPARTMENT OF WEIGHTS AND MEASURES OR A DEVICE REPAIRMAN - SECTION 2644(b) 145 FAILURE TO (MONITOR THE TFMS USING THE }ETiKD SPECIFIED ON THE PERMIT - SECTION '5293. HSC r159 FAILURE i0 MAINTAIN 5iE WRITTEN RECORDS OF ALL MONITORING PEnrOnMED ON SITE - SECTION 2712(c). CCRR 160 FAILIFE TO SECURE THE MONITCRING 'JELLS - SECTION 2648(i). CCR 179 FAILURE TO CORRECT PREVICe1S VIOLATIONS WITHIN 38 DAYS - SECTION 2712(h), OCR _ '9a FAILURE TO SUBMIT IN'VE":TORY RECONCILIATION QUARTEKY REPORT - SECTION 2644(e) CCR. 1?6 FAILURE TO SSJ:MIT A "PEP.MIT TO OPERATE" APPLICRT;ON FOR TFE USTS AT THE SITE - SECTION 25,286 H L S r120 FAILURE TO REPORT THE CF:R\GES IN TIC 'JSAGE OF UST WITHIN 39 DAYS - SECTION 2712(a). CCR 125 FAILURE TO n^E-•ORT k%%TKC-.,317ED RF EASE - SECTION 2658(b), CCR r155 FAILURE TO ?MONITOR VISNA' LY AT AEOUIRED FRE;1<JENCY - SEC?ICrti 2642(c), CIR _ 165 CONTINUOUS i1CNIjORING DEVICES INOPERABLE - SECTION 2632(C)(2)(A) _._ 189 FAILURE TO Atw'"A1RIlY TES? F;PELIPE LEAP DEMTORS - SECTIO`! 25292 HLS 185 FAILURE TO SUEMIT TANK INTEGRITY TEST RESULTS WITHIN 30 DAYS CF TEST MMPLEfION - 3ECTi0N 2629L.'n3S. 1195 FAIL'UREE TO FOLLOW THE PROCEDURE IN SECTION 2644(f) WHEN !MJE:TORY RECONCILIATION EXCEEDS THE ALLOWA=LE 'VARI"nTION. _ 2"o FAILURE TO REPORT CHA,NGE3 IN MIONITORING ALTERYIT2'VE PRC-M)URES WITHIN 38 DAYS - SEC(MN 2712(a) CCt, 5 PAI+Un- TO 1 13T PnlPEti - EC i i 2-671-7-, n Fp'"w) nr _- " TCz nn R FfK- it N 2660-6 'wi 36 AiL'SC -0 tih« ti_ P-a ) . dr .& .RILE _oT O TPw--iPIFEL:NE3 - SECTION '<5272 H C S 2S7 GT,_.. tIEN"'; �?.Q) /\.t! en... .._.L�.IL......:ZoVCN40". �C,?o.. 7 .- ``......_.�f 9. 0_.....__....f!.. �ANf(L....._...If1.rte..........�t.te...................."........................................................................................ U�....._ .At.t.........la.._._. ...S.J. .r,t.f......_.. ..........QJNJPN}„i/..........ECGar.4t��A.f .."........... r?QYi1 r�... ... ........... � ..�1f�. ..._..._...���s..,. .....:................Lt_........ .......... P�........... .........E ............!y......R��,rt..... ... ................. ��.✓. . ........ _ ...... _ . r ............. .. . . . .. .................... ..................... ... ........ ........................ IFE; TOR #: �. .'....... SIGNATURE: .... .. V..�/ V Dfl?c: .....I......�.5.. ... ........ ... 01,r I',.'E:. BY a Q .. ........ .........�......�!.-..... .. ... .. .... .... .. DATE: .�...;I�B� r� YYY _ ' HEKIMIAN & ASSOCIA fES, INC. (657( Gemini Lane Huntington Reach,CA 92647 (714) 841-6288 ENVIRONMENTAL F_NGINEERS I CONTRACTORS FAX (714)848-2603 ' FILE NO. 86-683 October 18 , 1988 SOLAG DISPOSAL P .O. Box 1100 San Juan Capistrano, CA 92693 ' Attention : Mr . Bob Gottlieb Subject : UNDERGROUND TANK TESTING AND CERTIFICATION AT 31731 PASEO ADELENTO, SAN JUAN CAPISTRANO, CALIFORNIA Mr . Gottlieb : ' In accordance with your P.O. #BOBG, we arrived at the subject facility on October 12, 1988 to test one ( 1 ) underground tank system using the Horner Ezy-Chek Leak Detection Equipment. A full systems test was performed on one ( 1 ) 10, 000 gallon diesel tank. The system was certified with a test result of -0.0283 gallons per hour. The test result for this system is within 44 percent of the State standard of -0.05 gallons per hour. Hekimian & Associates, Inc. suggests that you monitor this tank closely for possible ' leakage . The following information is included in this report as a requirement of the regulatory agency : * The tank was filled for testing on October 10, 1988 . ' The tank is constructed of steel. * The type of pump is suction pump . ' The distance from grade level to product level was 6 inches above grade. Enclosed is a copy of the pertinent worksheet. If you have any questions, please call. ' Very truly yours, �\� TTAN/( NK TFS SN F,� r HE MIA & OC 0,`� C. ' xY z6 d o. A0050 z nneth K. Hekimian, D. , P.E. President L KKH/ttd-1 �PFgQV PR�OJ ' Enc . _ (714) 941-62:26 FAX (714)848-26t CLIENT NAME OF SUPPLIER, G� - '• -'- OWNER OR DEALER. �olm4 �•S9oS�.0 8— t- DATE OF TEST ADORESS(NO. 6 STREET) WEATHER TEMPERATURE " .CITY AND STATE Q La m4 O�'S PM o - • • ;. ,.- TANK INFORMATION AA N ,p CAPACITY(NOMINAL) (0 GALS. SIZE OF FILL OR TEST OPENING T IN. CONTENTS(PRODUCT) CAPACITY(CHART) GALS. TOP OFF TIME— GALLONS TANK MATERIAL 5 0"tENS10NS: DIAMETER NUMBER OF GALLONS AD ED TO START TEST o APPROX.AGE LENGTH TANK NO. PUMP SYSTEM(TYPE) Su INCHES OF WATER - BEFORE TEST cJ •• AFTER TEST o •• Type of Phase II' - - -TEST CALIBRATION - - TARK LAYOUT \Vapor Recovery Sys. K,L SIZE OF CAL, BAR OR MCS ADDED ,O'rjC al _ 57 F,p00 9 (ALM{ tFAC1OR A) •. . LINE MOVEMENT I Q5 (a 37 _ 58 LINES - 2 a 2 to _ 57 LINES 3 qo to St, = —LINES - TOTAL LINES : 3 = LINES .. NLAq END OF TEST CALIBRATION _ SIZE OF CAL. BAR OR ML'S ADDED - (ALM) (FACTOR At ' LINE MOVEMENT 1 -10 - LINES 2 (o LINES 3 (G LINES TOTAL LINES - 3 = LINES (ALM) M_, iURED API SPECIFIC GRAVITY PRODUCT TEMPERATURE 7 �1= API SPECIFIC GRAVITY m 60°F (FROM TABLE A) , COEFFICIENT OF EXPANSION!_�, r 1( (a (FROM TABLE B) C.o.F x TOTAL CAPACITY IGAL.) wL.CwwGFr F(FACTOR B) PRODUCT LINE TESTING SYSTEM TANk Tme Readkq PRODUCT MONIMAING 08 LL Proaua Serial Number N I"tigl i No. Slav End Gm K Faw A ;Gaift Lass .00 Y .003 O0050 Z .003 ( o e"L 2 TECHNICIAN( ti DA1. DATA CHART FOR TANK SYSTEM TIGHTNESS TEST (EZY CHEK) ReN jrj PRODUCT MONITORING ON lLR PlpdUp TEMPERATURE COMPENSATION A TEMPERATURE COMPENSATION 8 NET VOL.CHANGE No. Sun End ♦Gain +Gain ♦Gain a6 esion ♦Gain +Ea anion _L� x Fads A doss Sian End _L X Fano IT -Conuagion Sian End -Loss X Fam 8 -Conoaebn LIR i 3411 -3 0009 -•0-27 73d -70-1 -� jos -uoS 6 0029 Q 31 2 - 3 4 -oo4T 7Qq 74y it. It ro -0027 23 25 -3 4 -.0047 79- 7U -eol t -oor6 65 60 -0045 728 728 ±v Y -0or9 728 728 +0 y Zo -w0s Q 58 _, - - -728 72y -roo f 1, i.004C -Coss 513 56. -2 r, -:0018 7121 -MIT -,I-o y fo 5 s S 3 -t V -0005 729 729 '*0 ef :tn -Duos `1 5S sS4T -I ` -oa�g 729 729 1 f v y :Lc ��oy .. . 11 �2 _ t 4 -Ooo`3 72 730 +004 r, ; . ZIT - 4 730 -731 +001 y cOarrG -Carr 730 fo y to _ooac- 1 T► 50 -t y -o��y 730 7 O 3� ,. *o —000S 14 30 49 — I -0009 7 o -73 too( ro04C -�(i A. Tank Bol. to Grade 1212 H �� -" Send Report to: S 1 g D B. Tank Top to Grade ��---- Client 6 t�� C. Tank Diameter �" , oTti Co PTGa TrmJU 0. Address D. Test Level above grade n City, State 6 a E. Depth of water in tank Phone ( ) F. Depth for taking sample Attn: H G. Temp. Probe depth (connector) " CEHTIFICATION Me y beend,T.I Tn una sesHm.a.Jested A H. Test level to Tank Bot. " 441*SI .,TIW..VM ,,.d gM Tet'the emina e{ubLPga I. Groundwater above lank bottom - by bey Nalidn.I r.e P,d,,0"A..xalgn P..",329. C J. Product Pressure per 1" height •o3"L PSI Tank No. ER Test Pressure Formula Tight `/ES TH G E _x—_ 036 _ 4.OS6' Leakage Indicated - . o 283 (—x )- Technician A> H J I NET TEST C.Q Pn, EsT Date Tested to. IQ,1g$8 ' CHECK LIST ' I MONITORING ALT #5 Number of Tanks Under This Monitoring Method. ' Identify Tanks: Product Stored Size 2. 3. 4. Status: 1 Permit has been issued. ' Tanks have been removed. Need to inspect. Awaiting more information. Required Information: 1. Application for "Permit to Operate" completed and signed ' by the owner of the tank(s) . ' 2. "FMA" completed and coded by inspector with tank details ✓ q/ g (note computer input date) . ' 3. Detailed inventory reconciliation procedure received which incorporates Section 2644 & 2641(5) . (indicate if in Major's file) . ' 4. Integrity test completed for tank(s) and piping with ' in the last 12 months (note date of test) , 5. Other years integrity test completed (note year - for information only) . ig 3° 1oi?/ S S 6. Pumping System ' a. Pressurized System 1. Documentation made/received for installation of pressure loss device. 2. Annual pressure loss device certification date. (device must be tamper proof) . Suction System 1. Britten description of warning signs received. 1 ' 7. Dispenser(s) calibrated within last 24 months ' S. UST Plot Plan on file. 9. Owner/Operator agreement on file. M A ' (Indicate if in Major 's file) . ' 10. Other Information 1 — Coin of Orange/Health Care Agency ' Env . . anmental Health (714) 834-8175 1719 West 17th Street, P. 0. Box 355 Santa Ana, CA 92702 ' UNDERGROUND STORAGE TANK QUARTERLY INVENTORY RECONCILIATION REPORT ACCOUNT NO. : DATE: .3 '0ti/ONe'er FACILITY NAME AND LOCATION: MAILING ADDRESS: q.2-4 43 Title 23, California Administrative Code (CAC) , Section 2644(e) requires the owner or oper- ator of an underground storage tank utilizing inventory reconciliation as part of the re- quired monitoring and leak detection system to submit on a quarterly basis a statement to the local agency under penalty of perjury, that either: the inventory reconciliation data is within allowable variations or a listing of the dates and variations that exceed the ' allowable variations. This form or a reasonable facsimile, when completed,, will satisfy the quarterly reporting requirements. Please return a copy of this form to the Underground Storage Tank Program within thirty (30) days of the end of each calendar quarter (March 31 , June 30, September 30, and December 31) . For the calendar quarter ending 3 o tvv at the facility indicated above, ' records for all underground tanks monitoret by inventory reconciliation indicate that: a. All inventory variations were within the allowable limits of Section 2644 , CAC'.` ' b. Inventory variations in excess of the allowable limits of Section 2644 , CAL have occurred cn the foll_Wing days , in the listed amounts , for the following underground stcrage tank� , .(pse back side of report if additional space is needed ' Tank Tank Size I .D. (Gallon) /l)//l ' Example: Dates 01/30/87 02/09/87102/28/87 03/07/87 #000 10,000 Vari- ' Unleaded ation +125 -130 +150 +175 Dates #001 Vari- ation Dates #002 Vari- ation Dates ' #003 Vari- ation I certify, under penalty of erjur that all variations (if any) exceeding allowable limits for the quarter ending No l � are indicated above and were investigated in accor- dance with the requirements df Title 23 , CAC, Section 2644. anc Facility Owner/Operator ,ljs:06/17/87 Cou of Orange/Health Care Agency('- Env , imental Health (714) 834-8175 . 1719 West 17th Street, P. 0. Box 355 Santa Ana, CA 92702 ' UNDERGROUND STORAGE TANK QUARTERLY INVENTORY RECONCIL TION REPORT ACCOUNT NO. : e/-fdcr DATE: /51 FACILITY NAME AND LOCATION: MAILING ADDRESS: n e Title 23 , California Administrative Code (CAC) , Section 2644(e) requires the owner or oper- ator of an underground storage tank utilizing inventory reconciliation as part of the re- quired monitoring and leak detection system to submit on a quarterly basis a statement to the local agency under penalty of perjury, that either: the inventory reconciliation data is within allowable variations or a listing of the dates and variations that exceed the ' allowable variations. This form or a reasonable facsimile, when completed., will satisfy the quarterly reporting requirements. Please return a copy of this form to the Underground Storage Tank Program within thirty (30) days of the end of each calendar quarter (March 31 , June 30, September 30, and December 31 ) . For the calendar quarter ending _ at the facility indicated above, ' records for all underground tanks monitored by inventory reconciliation indicate that: a. x All inventory variations were within the allowable limits of Section 2644 , CAC'. ' b. T Inventory variations in excess of the allowable limits of Section 2644, CAL have occurred cn the following days, in the listed amounts, for the following underground storage tanks (use back side of report if additional space is needed ' Tank Tank Size / I.D. (Gallon) J ' Example: Dates 01/30/87102/09/87 02/28/87 03/07/871 #000 10,000 Vari- ' Unleaded ation +125 -130 +150 +175 Dates #001 Vari- ation Dates ' #002 Vari- ation Dates ' #003 Vari- ation I certify, under penalty of p r-jury, that all variations (if any) exceeding., allowable limits ' for the quarter ending / -1, , are indicated above and were investigated in accor- dance with the requirements ot 9 Title 23, CAC, Section 2644. ' / Tank Vacility ner/Operator 1js :06/17/87 UNDERGROUND STORAGE --VK QUARTERLY INVENTORY RECONCIr 'TION REPORT 1 ACCOUNT NO. : 9,5o d DATE: 3! Ina,, ge, 1 FACILITY NAME AND LOCATION: MAILING ADDRESS: 4;�/'�j cr Di s,pvs y I :.. c SaI rsOc S9� lrrc ' sz�ai C,C2171G1! y �� � do B� iio�' •. `fc�.« �� -�C��fd %1G�3 s9w ?vt�„ C 9�',s7 tf vp e ;L 7Z 93 1 Title 23, California Administrative Code (CAC) , Section 2644(e) requires the owner or oper- ator of an underground storage tank utilizing inventory reconciliation as part of the re- 1 quired monitoring and leak detection system to submit on a quarterly basis a statement to the local agency under penalty of perjury, that either: the inventory reconciliation data is within allowable variations or a listing of the dates and variations that exceed the allowable variations. This form or a reasonable facsimile, when completed, will satisfy 1 the quarterly reporting requirements. Please return a copy of this form to the Underground Storage Tank Program within thirty (30) days of the end of each calendar quarter (March 31, June 30, September 30, and December 31). (For the calendar quarter ending 3; /7fgi� ���' at the facility indicated above, records for all underground tanks"monitored by inventory reconciliation indicate that: 1 a. All inventory variations were within the allowable limits of Section 2644, CAC. b. Inventory variations in excess of the allowable limits of Section 2644, CAC 1 have occurred on the following days, in the listed amounts, for the following underground storage tanks (use back side of report if additional space is needed). 1 Tank Tank Size I.D. Gallon (Example: Dates 01/30/87102/09/87102/28/87 03/07/87 #000 10,000 Vari- Unleaded ation +125 -130 +150 +175 1 Dates #001 Vari- ation N `g 1 Dates #002 Vari- ation Dates #003 ar - ation II certify, under penalty of perjury that all variations (if any) exceeding allowable limits for the quarter ending 3,;P%vve`//irk , are indicated above and were investigated in accor- 11ance with the requirements o it e , CAC, Section 2644. 1 /Tank Pace ity Owner/Operator IIis:06/17/87 1 UNDERGROUND STORAGE ,' VK QUARTERLY INVENTORY RECONCI(_'TION REPORT (ACCOUNT NO. : �S� DATE: o FACILITY NAME AND LOCATION: MAILING ADDRESS: So//�CT D/S�f10S9 I i✓L,( �S_O�/tO /�/SI�PI �� Zws h/w, VCLf�" CL�jfGji/�iJy(� %iL�7 S9W ��.'Q"7r ���i5?df�� C.Q - lLG93 'Title 23, California Administrative Code (CAC) , Section 2644(e) requires the owner or oper- ator of an underground storage tank utilizing inventory reconciliation as part of the re- quired monitoring and leak detection system to submit on a quarterly basis a statement to the local agency under penalty of perjury, that either: the inventory reconciliation data is within allowable variations or a listing of the dates and variations that exceed the allowable variations. This form or a reasonable facsimile, when completed, will satisfy the quarterly reporting requirements. Please return a copy of this form to the Underground Storage Tank Program within thirty (30) days of the end of each calendar quarter (March 31, June 30, September 30, and December 31) . 'For the calendar quarter ending c, " / V7 , at the facility indicated above, records for all underground tanks monitor by inventory reconciliation indicate that: a. All inventory variations were within the allowable limits of Section 2644, CAC. b. Inventory variations in excess of the allowable limits of Section 2644, CAC ' have occurred on the following days, in the listed amounts, for the following underground storage tanks (use back side of report if additional space is needed). ' Tank Tank Size I .D. (Gallon) 'Example: Dates 01/30/87 02/09/87 02/28/87 03/07/87 #000 10,000 Vari- Unleaded ation +125 -130 +150 +175 Dates #001 Vari- N ration Dates #002 Vari- ation ' Dates #003 art- ation 'I certify, under penalty of perjury, that all variations (if any) exceeding allowable limits for the quarter ending )! are indicated above and were investigated in accor- Idance with the requirements o it e CAC, Section 2644. Tran aci ,ty ner perator '1js :06/17/87 UNDERGROUND STORAGE "' 'iK QUARTERLY INVENTORY RECONCIt—'TION REPORT 'ACCOUNT NO. : 950 DATE: FACILITY NAME AND LOCATION: MAILING ADDRESS: o �c.�. ^ �� i-/CJ�1d !/1 %lL/�7 s9r✓ �vcc,. C;7�,s>�.f v0 C4 _5 Z e 93 'Title 23 , California Administrative Code (CAC) , Section 2644(e) requires the owner or oper- ator of an underground storage tank utilizing inventory reconciliation as part of the re- quired monitoring and leak detection system to submit on a quarterly basis a statement to the local agency under penalty of perjury, that either: the inventory reconciliation data is within allowable variations or a listing of the dates and variations that exceed the allowable variations. This form or a reasonable facsimile, when completed, will satisfy 'the quarterly reporting requirements. Please return a copy of this form to the Underground Storage Tank Program within thirty (30) days of the end of each calendar quarter (March 31 , June 30, September 30, and December 31). 'For the calendar quarter ending 3 Q at the facility indicated above, records for all underground tanks monitoPed by inventory reconciliation indicate that: ' a. k<� All inventory variations were within the allowable limits of Section 2644, CAC. b. Inventory variations in excess of the allowable limits of Section 2644, CAC ' have occurred on the following days, in the listed amounts, for the following underground storage tanks (use back side of report if additional space is needed) . ' Tank Tank Size I .D. (Gallon) 'Example: Dates 01/30/87 02/09/87 02/28/87 03/07/87 #000 10,000 Vari- Unleaded ation +125 -130 +150 +175 ' Dates #001 Vari- ation N4 ' Dates #002 Vari- ation ' Dates #003 ari- ation certify, under penalty oferjur,J , that all variations (if any) exceeding allowable limits for the quarter ending ;?C; , are indicated above and were investigated in accor- �ance with the requirements oor Title Z3, CAC, Section 2644. —�—' Tank-Facility ner perator 'is:06/17/87 ' HEKINIIAN & ASSOC:IATES, INC. 16571 Gemini Lane Huntington Reach,CA 92647 (714) 841.6288 EAI/ROAMEN7.4L CAM.\7ERS: CONIRAC7OR.S _ F.-v\ (714)848.2603 ' CACOYTRAC70R'.SLICC%SE=?000 0.+ FILE NO. 86-683T ' October 24, 1989 SOLAG DISPOSAL P,O. BOX 1100 ' San Juan Capistrano, CA�2�3 Cjc tV-7 5 Attention: Mr. Bob Gottlieb Subject: UNDERGROUND TANK TESTING AND CERTIFICATION AT 31731 PASEO_::_ ' ADELANT0, SAN JUAN CAPISTR NO, CALIFORNIA Dear Mr. Gottlieb: ' In accordance with our verbal agreement, we arrived at the subject facility on October 11, 1989 to test one (1) undereround tank system using the Horner Ery-Chek Leak Detection ' Equipment. A full systems test was performed on one (1) 10,000 gallon diesel tank. The system was ' certified with a test result of -0.0243 gallons per hour. The following information is included in this report as a requirement of the regulatory agency: * The tank was filled for testing on October 10, 1989. t * The tank is constructed of steel. ' * The type of pump is suction. * The system was tested at grade. Enclosed is a copy of the pertinent worksheet. If you have any questions, please call. ' Very truly yours, CEO TANK T HE & A C �sf 2� z t z 10 neth K. Hekimian, P.E. President ' KKH/tae-1 C�F�rIVE PROS DATA CHART FOR TANK SYSTEM TIGHTNESS TEST (EZY CHEK) TE REEddv PRODUCT MONITORING ON LLR prodW TEMPERATURE COMPENSATION A TEMPERATURE COMPENSATION B I NET vDL.CHANGE IwN+ryl No $W End X Fam A -LWSIM Erb -UmX Fuw B y-CmNliao Sun Eno loss X F&m B � W LLR -LMIa� -23 .Got7 _.ob91 ri._ 7 so -1 -testi 41?R 425 1003 N -.0112 -.0157 3 80 65 -15 F -.oQ55 425 422 -003 ' Y -.Jt3't- -.0123 5 419 -tel 0ok -0041 6 n2I 7S - t -D06$1 4r8 It 17 7 -78 - L -00 17 4116 -.701 A -0344 -a02T� 74 1 71 1 -3 -ooS( ' 416 . 415 -a01. w -0044 -0007 4 71 69 -2 -0034 415 4 v -OD3'4 to U1, 0 2 L •bo34 415 415 +o w :0034 tl 7 6E - 3 1)051 4/s 414 -Co( E -0044 -0007 19 6 0 -Lt -0053 414 413 -ool P -0o44 _Lx�2c 13 66 5C - + -W68 1113 412 -071 w -0044 -0024 ly 5 52 -[ - 68 412 41 -ooi t -0044 X34 i I I I I A. Tank Bot. to Grade h / O 8. Tank Top to Grade Send Report to: (mq GRADE C. Tank Diameter . Client Address D. Test Level above radeCity, 17 3 1 SCO g o hnale e E. Depth o1 water in tank Phone G Poe F. Depth for taking sample Attn: CA C1 a 675 F H G. Temp. Probe depth (connector) ' CEIITIFIWgN ThyrpcsMT+na+ws NN sh�m.Y Ny4a A H. Test level to Tank Bot. l �,ww,,,,,•, Thn.nesawe^7qu"myM o1)auo..woyyn.o 1. Groundwater above lank bottom ate.Nn wW F..PiaNncn NwwNon hmp M]A - 1_ _ C J. Product Pressure per t' height T PSI Tank No. I i ca 0243 WATER Test Pressure Formula 7,515 Tight Leakage Iny dicated DEPTH E _x—_(—x .036 )= Technician N J I NETTE5T PAESSU Dale Tested R(]7Jc�+U PqT C`I IJ (1 1 9 i DATA CHART FOR TANK SYSTEM TIGHTNESS TEST (EZY CHEK) Tone AeadN PROOUCT MONITORING ON LLR Plo" TEMPERATURE CONPENSATON A TEMPERATURE COMPENSATION a NET TOL.CNANGE tMeaaryt No Sort Eno sGL" xFaclaA +Gain Sun End 4GiF' %Fm9 aExp�Mion Sun End -Las %F&MB ♦Expansion LLA AM .-Loss -loss -Caurusion -cmnact" 1 ?7 -23 I.CXA7 0391 4'1B 4.896 2 7 80 -( c 75?184 42g 425 -003 11 3 So65 -15 a -,04255 425 422 -6034 -•0tdti 0123 i30 7 -i3 U -.0221 ,r22 Lill -001 r -b(32, t 5 X7 $2 -C r -.0685 119 LTI8 -co( r _004 X41 G TL 78 r -Do68 IS ! 17 -0oI r �0y4 -00Q 7 t 78 7q - 4 -006 17 416 -001 r -1004tr k1 -74 71 -3 4 -0051 416 415 7001. 4 --o 0" -000-7 9 71 89 -2 -L9p3G 1116' 415 r a 4 l0 Cq 67 2 L -bo34 415 415 3o y 11 G7 - 3 4 -v^0�51 415- 414 -ool E _0044fO�7 19 & o -4 L�wp 414 443 -fit r -Oo4 ��� IS 60 56 4 -W68 443 412 _WI r -0044 14 5 'S2 -I -w68 410 !// -001 V I ' I A. Tank Bot. to Gradeg�oSm Q �I ID B. Tank Top to Grade Send Report to: R �1 Client GRAOE C. Tank Diameter • Address Address 317 b I �6r co D. Test Level above grade o City, State - a , Cca St'f e E. Depth o4 water in tank Phone ( ) � F G F. Depth for taking sample Attn: CA q n 675 R G. Temp. Probe depth (connector) cEmElcAraN T�.4mx.w w„a�,en, ,,,•x�e A H. Test level to Tank Bol. —” mawro . Tn,a..+x,wa-rya'-m..rwwro.wwMa 1. Groundwater above tank bottom W ur ka 'r F..P,auabn""°"W P&-* da.. c J. Product Pressure per 1' height m PSI Tank No. I Tight yES WATER Test Pressure Formula � o Leakage Indicated DEPTH E x.--(—x .036 )_ S�SJ ��r 9 !n1 -E�oGsl Technician (�Q7,jc1iJu P.ek C� H . , r NET rear Date Tested O PAESSUAE (0 , 11 19 U�+ / � DATA H F TA�SY M TIGHTNESS T H�AN�7cc�emini�� ne (EZY CHEK) llunlinglon Beach,CA 92647 (714)841-6288 FAX (714)848-2603 CLIENT NAME OF SUPPLIER, OWNER OR DEALER DATE OF TEST `D•11. 1 a" I ADDRESS(NO.6 STREE 3Tj I asco c La. o . CWEATHER ,;U NST L TEMPERATURE CITY AND STATE. ' ID rz(QA t' 0 d7� TANK INFORMATION CAPACITY(NOMINAL) 1030,> GALS. SIZE OF FILL OR TESTPENING ¢ IN. CONTENTS(PRODUCT) CAPACITY(CHART) OD J GALS, TOP OFF TIME__ 4d. lo, d 9 GALLONS TANK MATERIAL S -R — DIMENSIONS: DIAMETER NUMBER OF GALLONS ADDED TO START TEST �® APPROX.AGE LENGTH .TANK NO. - 1 PUMP SYSTEM(TYPE) Sly U O(, ( INCHES OF WATER – BEFORE TEST AFTER TEST TEST CALIBRATION O,] _ ^ •/ = 1 ^ _ 1-7TANR LAYOUT SIZE Of CAL.BAR OR ML'S ADDED � •G L7 l� (ALMI U (FACTOR Al NE MOVEMENT q � I � -- 1to O LINES --� to�— _ LINES 3 3 to 41 LINES TOTAL LINES _ 3 = LINES (ALM) END OF TEST CALIBRATION SIZE OF CAL BAR OR ML'S ADDED _ LINE MOVEMENT (ALMI = (FACTOR Al 1 to LINES Z to LINES 3-10 —LINES TOTAL = LINES _ 3 = LINES (ALMI MEASURED API SPECIFIC GRAVITY 3 U 1 PRODUCT TEMPERATURE •"� L I API SPECIFIC GRAVITY O SO-F – (FROM TABLE A) �,. COEFFICIENT OF EXPANSION - 30. I O (FROM TABLE B) C.O.Ex I'J06D .V �}' 3qC (FACTOR B) . TOTAL CAPACITY IGALI NTL.CHANGEPF PRODUCT UNE TESTING SYSTEM ime Resd PRODUCT MONIIDRING ON LL Pmd ct TA (Ms ng +GainSerial Number ,� N K N F nary) No. Sun EM F� ix.00 xtpA doss Q- •� LT I.003 Y oD I' jfUC G 1D°I'cro Zz TECHNI I N(S) DATE ���gTlVE PR��J� COIL OF ORANGE/HEALTH Ci*" AG� trIVIRONMENTAL HEALTH DIVISION 2009 EAST EDINGER, P.O. BOX 355 SANTA ANA, CA 92702 (714) 667-3700 ACCOUNT NO.: �Lt, �� UNDERGROUND TANK INSPECTION FORM 1 FACILITY NAME:__ G 791 (-7 _T�A 5fs5AL_ INSPECTION DATE: l l3 / 7 'STREET: 3)x-31 C LSiE 7 � ( -�I-r-r) MAP COORDINATES: $ _C c � t CITY: [ 1 ) ��t)� �1(PnJ\ 1 - t�ZIP:: i 1( �r DISTRICT: NEAREST CROSS STREET: � ti �7C Lit (T1JO PHONE: ( I�) 4 - 'o 4 4 b EX CODE: STATUS: PUBLIC AGENCY: INSPECTION TYPE: / Iou,.G•wnres: k•1��cisr COMPLIANCE: UNDERGROUND: 1. GA ATION / OT GAS STATION 'DEALER/SUPV.: 'NUMBER OF TANKS CTHIS ^LOCATION: I BILL TO NAME: �� �f'clC �i S 'b SA'L._ _tik�_C 'STREET: CITY: �(L{1'1� C±Y'l51-W-A-1L o STATE: CIA- ZIP CODE: -1 ,TANK OWNER (MAILING ADDRESS) 37 \\ 41 2� ,NAME: `Tit1 L 't-o V,l PHONE: ( ) STREET: CITY: STATE: ZIP: EMERGENCY CONTACT 'DAY: cm_v PHONE: q( 'NIGHT: S /Ilv,. /i.'.. PHONE: (-)IV '7&7Z- INSPECTOR 7&7ZINSPECTOR#: /�/ - SIGNATURE: �I`'L. DATE: 1�z RECEIVED BY:� 4, / y /�/.ry DATE: /?- LAPSED (MIN.) ENTERED DEC 2 8 1989 W F272-9.1511(809( PAGE 1 ' COL(_. OF ORANGE/HEALTH CP(_ AG4 ENVIRONMENTAL HEALTH DIVISION U 2009 EAST EDINGER, P.O. BOX 355 ' SANTA ANA, CA 92702 - (714) 667-3700 (( �\ { UNyDERG OUND TANK INSPECTION FORM HCA TANK ID: W 1( `� `y F� TANK ID: DATEINSTALLED: ' STORED: CAS#: 1°l 3- Fo NAME: TIS: TANK CAPACITY: 10 j wtm PRESSURE/!/GRAVITY: TANK CONSTRUCTION MATERIAL: [ ( ] 5ileerL ' PIPING CONSTRUCTION MATERIAL: ( I ] S-reset_ TANK MONITOR: [ a ] I N PIPING MONITOR: [ 9_� ] rI/�4 /T k�x�br l ' MONITORING OPTION: [ !j ] VIOLATIONS: OTHER: HCA TANK ID: FAC. TANK ID: DATE INSTALLED: STORED:CAS#: NAME: vs._ ' TANK CAPACITY: PRESSURE/SUCTION/GRAVITY: TANK CONSTRUCTION MATERIAL: [ ] PIPING CONSTRUCTION MATERIAL: [ ] ' TANK MONITOR: [ ] PIPING MONITOR: [ ] MONITORING OPTION: [ ] VIOLATIONS: OTHER: HCA TANK ID: FAC. TANK ID: DATE INSTALLED: STORED: CAS#: NAME: T/S: TANK CAPACITY: PRESSURE/SUCTION/GRAVITY: TANK CONSTRUCTION MATERIAL: [ ] PIPING CONSTRUCTION MATERIAL: [ ] TANK MONITOR: [ J PIPING MONITOR: MONITORING OPTION: [ ] VIOLATIONS: OTHER: HCA TANK ID: FAC. TANK ID: DATE INSTALLED: ' STORED: CAS#: NAME: T/S TANK CAPACITY: PRESSURE/SUCTION/GRAVITY: TANK CONSTRUCTION MATERIAL: [ ] PIPING CONSTRUCTION MATERIAL: [ ] TANK MONITOR: [ ] PIPING MONITOR: [ ] MONITORING OPTION: [ ] ' VIOLATIONS: OTHER: ' INSPECTOR#: a a�L SIGNATURE: /Lr �r�c� DATE: RECEIVED BY: / /�� /�/r'�/�r� DATE: /L //3 1 `1 ' b F272 9.1541(9189) PAGE 2 COC. Y OF ORANGE/HEALTH C� AG! f ENVIRONMENTAL HEALTH DIVISION 5� Lp� 2009 EAST EDINGER, P.O. BOX 355 ' SANTA ANA, CA 92702 (714) 667-3700 UNDERGROUND TANK INSPECTION FORM VIOLATION DESCRIPTIONS ' FACILITY 105 Operating Underground Storage Tanks (UST) Without a Permit- Section 25284(a), H&S 115 Failure to Report the Change in Ownership Within 30 Days-Section 2712((), CCR 130 Failure to Develop a Response Plan to Remove the Unauthorized Release From the Secondary Container Section 2632(d) (2), CCR 135 Failure to Enter Into a Written Contract Between Owners and Operators to Monitor the UST-Section 2610(b),CCR 'JL-� 140 Meters Not Inspected b a Device Repairman - Section 2644(b),CCR LA 5-r w*s 1A21 / % -� 145 Failure to Monitor the Tanks Using the Method Specified on the Permit-Section 25293, H&S '__LL 150 Failure to Maintain the Written Records of All Monitoring Performed On-Site - Section 2712(c), CCR 160 Failure to Secure the Monitoring Wells -Section 26480), CCR 170 Failure to Correct Previous Violations Within 30 Days-Section 2712(h), CCR 190 Failure to Submit Inventory Reconcilliation Quarterly Report-Section 2644(e), CCR <- 196 Failure to Submit a"Permit to Operate"Application for the USTs at the Site - Section 26286, H&S TANKS 120 Failure to Report the Changes in the Usage of UST Within 30 Days - Section 2712)a), CCR 125 Failure to Report Unauthorized Release -Section 2650(b), CCR 1155 Failure to Monitor Visually at Required Frequency - Section 2642(c), CCR 165 Continuous Monitoring Devices Inoperable -Section 2632(c) (2) (A), CCR 180 Failure to Annually Test Pipeline Leak Detectors -Section 25292, H&S L�� 185 Failure to Submit Tank Integrity Test Results Within 30 Days of Test Completion -Section 2643(e), CCR 195 Failure to Follow the Procedure in Section 2644(f), CCR When Inventory Reconciliation Exceeds the Allowable Variation 270 Failure to Report Changes in Monitoring Alternative Procedures Within 30 Days- Section 2712(a), CCR 275 Failure to Close UST Properly - Section 2670-72, CCR 280 Failure to Repair UST Properly - Section 2660-63, CCR 286 Failure to Annually Perform Tank Integrity Test of Tanks/Pipelines -Section 25292, H&S ' 290 Other lo(}l g} 'COMMENTS: L-(` IN S PCNL l 1 -)--vim , f 'tD Pecs >✓ tFaVti�o 1 /� 2G-�°c� t�r1 I�1sc'� P�ts� CA tit VA-rte �yuy . ��. �t��S-t4 30VL_ Tl+s T— t� —� � �— T-q-,��� M tse-�.�/fi,�s�Z � �l. f5'h-1 - St j->✓ t�! �zc ,INSPECTOR#: a a SIGNATURE: (C/��_ DATE: '�-� /d3_1_ _F1 /a" l� DATE: /?— F272-9.150(989) PAGE 3 Gd -R NUMBER: ' HEALTH INSPECTION REPORT (continued) Page of ORANGE COUNTY HEALTHCARE AGENCY ' - ENVIRONMENTAL HEALTH DIVISION Mailing Address: P.O. Box 355, Santa Ana, CA 92702 Office: 2009 E. Edinger Ave., Santa Ana, CA 92705 Telephone 1714) 667-3600 ' DBA �+'� t`� ADDRESS CITY ITEM NO. vi t— M ts-h1T t `s 5A A�� A L.t_ �1ars-r- Tr-rc(.etit S PcVt ' �A YL , G-o �'f TFk "rttel- 5 1(E:-' R-T ' S-C> PM V-: 1 �a t5 /itx-, -r- -rte s -t-o Tti 1 LT 57- s 2 s R-I,ty t � s :9: s�� j s/ SPECIALIST G ( I AECEIVED BY DATE a i F 0272.9.373.5 OFFICE COPY COUNTY OF ORANGE UST CLEANUP HEALTH CARE AGENCY ENVIRONMENTAL HEALTH WASTE MANAGEMENT SECTION Q H.W. SITE CLEANUP ACTIVITIES REPORT Company Name: S �'l Ei �T't) 5P�lL_ Address: 31 -1- 3 r ' City: SPS ��f�NiST�2Wtle (iA �Z6�S ' Contact Person(s) : �� CnT'T-I- Phone: ` F4o - DY46 to Staff ACTIVITIES/COMMENTS P -ts sT� 19/�d� Lit Qurtso � cA,,�l s ,k JE-x�X5s5X F-U-10- +o��( e� > z4�g cbtu� Mrnl.�s (ALT. 5 ¢actcF,r -+'o IS-a-g �- �y/gP R f Lev�v v b 'P� n s 51 tJrc-9 �'h'r�9 ��38 Skrpi+,U P/4 A C.treYe 0191 g 9 (39 QuArn.T-6el) - o ems- 140 J F`N -M. ' -ri -r-. CZC—S K T 5 10/13 / SS 4- t o (z't $`) REV: 10/13/87 ' UNDERGROUND STORAGE/`NK QUARTERLY INVENTORY RECONCr -kTION REPORT ACCOUNT NO. : DATE: 'FACILITY NAME AND LOCATION: MAILING ADDRESS: Sol.9!r D1Soj sr/ L Sn/.moi+ Dis�oSc�/ l�vc C1 °l3 Z 93 'Title 23, California Administrative Code (CAC) , Section 2644(e) requires the owner or oper- ator of an underground storage tank utilizing inventory reconciliation as part of the re- quired monitoring and leak detection system to submit on a quarterly basis a statement to the local agency under penalty of perjury, that either: the inventory reconciliation data is within allowable variations or a listing of the dates and variations that exceed the 'allowable variations. This form or a reasonable facsimile, when completed, will satisfy the quarterly reporting requirements. Please return a copy of this form to the Underground Storage Tank Program within thirty (30) days of the end of each calendar quarter (March 31, tune 30, September 30, and December 31). or the calendar quarter ending 3i Van P9 at the facility indicated above, ,records for all underground tanks monitored y inveniory reconciliation indicate that: a. All inventory variations were within the allowable limits of Section 2644, CAC. b. Inventory variations in excess of the allowable limits of Section 2644, CAC have occurred on the following days, in the listed amounts, for the following underground storage tanks (use back side of report if additional space is needed). 1 Tank Tank Size I.D. Gallon �xample: Dates 01/30/87102/09/87 02/28/87 03/07/87 #000 10,000 Vari- Unleaded ation +125 -130 +150 +175 Dates #001 Vari- /V/#, ation Dates #002 Vari- ation Dates #003ari- ation certify, under penalty of perjury, that all variations (if any) exceeding allowable limits or the quarter ending 3J Dee. d"� are indicated above and were investigated in accor- ance with the requirements of Title 23, CAC, Section 2644. Tank Facility Owner/Operator js:06/17/87 RALPH RIGHT r ' PUMP CALIBRATION 12172 London Grove Ct. y Moorpark,CA 93021 y (805) 523- 1036 �nCr4 Q/S4Z3SA-c- 1� C IFow�ss �-��Y�YY ��An�e`,zA N '0 srwTION »Urw[w owrc/n� ll <w� wwnoa E tT o.sn.yr<»wurKw S•v. ti J J A J `.wy/S •V O ,d I J d `COM N T ANLL_ t7 W/M NOTIFIED 4-1 _ RED 4) '7 TAGGED GREEN tl MP: C-/,1�. i2�1 F-i �1 1 Q L A Z- BLUE 41 TAG / CALIBRATION: TALIZER FINISH Y.- __ a ii ____ CHECKED r ID o»s ..ST xow READINGS: START—_____-_—____ ADJUSTED To ".,»e. a ws •o. slaw _ TOTALIZER SEALED YES t7 NO t1 �ODUCT-__ � -�_ RETURN 10 STORAGE _ ( _ METER SEALED YES t] NO 47 a.0 o»s (RED <1 f TAGGED[GREEN t C 4L(r /4�� J � ut= / S IJ -T"1 Ste//._ l �MP: ..___�_�:.. .. BLUE tl TAG I Al � J 74-Z" A N p A .1-) cAIIBCHECKE: FINISH- _ CHECKED TOTALIZER "a"s' °•`""' ••s• xow �ADINGS: START .o ti '� U S; 0 O�ti 1 c �= / + F S ADJUSTED TO n I •>r A AST S. 4 LJ /-L C_ F=7-S- TOTALIZER SEALED YES 4V NO 4uslow PRODUCT_____4 S�L RETURN TO STORAGE METER SEALED YES tl NO t1 a.uo»z RED 41 i TAGGED GREEN t1 MP: _ 2 /1 W • l J / C i BLUE t1 TAG E CALIBRATION: FINISH o eT- an.Os CHECKED •.e. TALIZER j I Q y.ow READING& START.6—_-.--_---___ ADJUSTED TO O.LLOM y.sr xow CETtTOTALIZER SEALED YES t1 NO tlIODUCT __-___ RETURN TO STORAGE 1R SEALED YES 41 NO tl O.LLO»y RED 43 I' TAGGED(GREEN h �MP:___-_---.::_ -- xn..»o..e. l BLUE. tJ TAG A_ i CALIBRATION: FINISH �_ CHECKED OTALIZER .a..y. c...os . .,• •m. yww ADINGS: START ADJUSTED TO .o»<. - °•"o"s TOTALIZER SEALED ,YES 47 NO h xow PRODUCT _._____ -- RETURN TO STORAGE METER SEALED YES tJ NO 47 (RED 41 4.1 PUMP: _ _ _ __— _ s•..` rys, TAGGED 1 BLUEN tl TAG / CALIBRATION: TALIZER FINISH CHECKED READINGS: START v__. __-..___._.-_-_-___-_ ADJUSTED TO MO»l♦ a.11 Wy I.S. xOM TOTALIZER SEALED YES 41 NO 4.1 DUCT ____-..._...-------.___ RETURN TO STORAGE METER SEALED YES t7 NO V (RED 41 P TAGGED( GREEN 41 41 TAG E ----- ----_- —'CALIBRATION: ALIZER FINISH _-_ CHECKED DINGS: SIARr .. _- _ ADJUSTED 10 -- slow TOTALIZER SEALED •YES 41 NO t 1 DUCT _ _.. . RETURN TO STORAGE _ __. __- METER SEALED YES 41 t I .1 UNDERGROUND STORAr-TANK QUARTERLY INVENTORY RECON" IATION REPORT i , ACCOUNT NO. : 950 : J DATE: .j/ /Wai el l q 9 0 n.. FACILITY NAME AND LOCATION:3 -r z,1 �;oMAILING ADDRESS: i .S%t* 215eo5ap/ svc g16°13 sew �4a„ �y�,sT�,f. a C� -IZC93 'Title 23, California Administrative Code (CAC) , Section 2644(e) requires the owner or oper- ator of an underground storage tank utilizing inventory reconciliation as part of the re- quired monitoring and leak detection system to submit on a quarterly basis a statement to the local agency under penalty of perjury, that either: the inventory reconciliation data is within allowable variations or a listing of the dates and variations that exceed the allowable variations. This form or a reasonable facsimile, when completed, will satisfy the quarterly reporting requirements. Please return a copy of this form to the Underground Storage Tank Program within thirty (30) days of the end of each calendar quarter (March 31, June 30, September 30, and December 31) . 'For the calendar quarter ending 3/ �'A�Cf//Q90 , at the facility indicated above, records for all underground tanks monitored by inventory reconciliation indicate that: ' a. All inventory variations were within the allowable limits of Section 2644, CAC. b. Inventory variations in excess of the allowable limits of Section 2644, CAC have occurred on the following days, in the listed amounts, for the following ' underground storage tanks (use back side of report if additional space is needed). ' Tank Tank Size T.D. Gallon ,Example: Dates 01/30/87 02/09/87102/28/87 03/07/87 #000 10,000 Vari- Unleaded ation +125 -130 +150 +175 Dates *V/# #001 Vari- ation Dates #002 Vari- ation Dates #003vari- ation kicertify, under penalty of perjury, that all variations (if any) exceeding allowable limits or the quarter ending .31 0*0#10 x/ , are indicated above and were investigated in accor- dance with the requirements of TiT23, CAC, Section 2644. an aci 11ty ner perator �js:06/17/87 HEKIMIAN & ASSG-[ATES, [NC_ 16;71 con,n,i Lnnc 11un(in'ton Beach. CA 92647 (714) 841-6288 LA M0.wtcATAI. LA(;ISCEaSiCu,v(RA( Zfur COW/•'AC'TOR c/10EA:Sl- FAX (7141848-2601 C-l FILE NO. 86-683 ' October 24, 1990 SOLAG DISPOSAL P.O. Box 11.00 San Juan Capistrano, CA 92693 ' Attention: Cameron Spicer Subject: UNDERGROUND TANK TESTING AND CERTIFICATION AT 31731 PASEO ADELENTO, SAN JUAN CAPISTRANO, CA Dear Mr. Spicer: In accordance with our agreement, we arrived at the subject facility on October 12, 1990 to tc,t one (1) underground tank system using the Horner Ezy-Chek Leak Detection Equipment. A full system test was performed on one (1) 10,000 gallon diesel tank. The system was certified with a test result of -0.0143 gallons per hour. ' The following information is included in this report as a requirement of the regulatory agency: * The tank was filled for testing on October 19, 1990. * The tank is constructed of steel. * The type of pump is suction. * The distances from grade level to product level was 12 inches above grade. ' Enclosed are copies of the pertinent worksheets. If you have any questions, please call. Very truly yours, HEKI A IATES, INC. .-. r ' nneth K. Hekimian, Ph.b, P' President KKII/tpn 1i�f CkLR(-1171 Enc: Worksheets gT1VEP� _ m m m m = = = = = = M I = = = = = �. DATA CHART FOR TANK SYSTEM TIGHTNESS TEST (EZY CHE10 CLIENT NAME OF'SUPPLIER, OWNER OR DEALER L2 ` I i 4�a a C_ DATE OF TEST__. O' ?U - 96 ADDRESS(NO,b STREET) WEATHER____ TEMPERATURE ATY AND STATE TANK INFORMATION CAPACITY(NOMINAL) UI L'UO GALS. SIZE OF FILL OR TEST OPENING :___._ IN. CONTENTS(PRODUCT) — CAPACITY(CHART) GALS. TOP OFF TIME 1&— (2- 9 D GALLONS TANK MATERIAL te e I DIMENSIONS: DIAMETER NUMBER OF GALLONS ADD)D TO START TEST__ APPROX.AGE LENGTH TANK NO. 1 c r�L UQ PUMP SYSTEM(TYPE) INCHES OF WATER - BEFORE TEST AFTER TEST Ph" I 1101FOr' Ul "" A cN TEST CALIBRATION _ uINK LAYOUT SIZE OF CAL. BAR OR ML'S ADDED ` - 3 y � OU 1 (ALM) (FACIOn A) _INE MOVT W to L o _ 3 LINES — L( to ti y - S LINES 13 to (z R = 'i LINES TOTAL I 0l- LINES _ 3 = S _—LINES (ALM) END OF TEST CALIBRATION .. ... SIZE OF CAL. BAR OR ML'S ADDED (ALMI (fACIGN AI LINE MOVEMENT 1 to = LINES 2 to = LINES J to = LINES TOTAL LINES _ 3 = __LINES / IAIMI MI RED.API SPECIFIC GRAVITY -- PR000CTTEMPERATURE ' API SPECIFIC GRAVITY O @O'F P# (FROM TABLE A) - COEFFICIENT OF EXPANSION ' ')U��'! (FROM(ABLE B) - - (I X ! ;%,J ;Jt�S i, �"I''•) ' (FACTOR B) G.O.E TOTAL CAPACITY IGALII VOL CIANGErF PRODUCT UNE TESTING SYSTEM - T— PROOUCTMONITORINGONLL Pmdct Serial Number Tme Reath.' +Gril (M&4M Na 'SII End . . �lM XFxforA -LIM \ .003lu / DO i)U� No. CAO DO .003 ---�—�-/— it HNICIAN(S ,. �-, ; �[ Q 1 l 7 DATE DATA CHART FOR TAIW*SYSTEM TIGHTNESS TEST (EZY CHEK) I „ T.Rr Arad.g PAODllLraIQAORW CW I IAJ P,&�%d TEWEAATURE COMPENSAWN-A TEMPERATURE COMPENSMION B NETVOL.CwU6E _ lu.daa:il 1k sut ' nd tGan• XFanaA EGM slad End rGan IFMIar0 EE.panson Skin — _-_End rGain XFacbre rEap own LLA F _Lott -Loss -Lois -Conuacton -L055 {onlatlgn � T •(J(J, ai,1' Z 2$ O 0 Z •r.A ! 3 e 9 2. 2, 0 o' Z P 'I Z ca 92 • 2 0 _�_ r• c; , , � o 0 d It, r . I ; ) er ,� ir — f - 0t7 ♦ 12. r $ �. tl - - --_ .•((/T .. 12 0 �J A. Tank Got. to Grade D B. Tank Top to Grade —_— - Send Report to: � GRADE C. Tank Diameter _ Client - ' Address D. Test Level above grade City. State a E. Depth of water in tank —.. Phone ( ) F. Depth for taking sample —_._ .Attn: H G. Temp. Probe depth(connector) CEfIs1FIGr10N TTs•q nnM mY Ib�aN Mum.aa Maw A H. Test level to Tank Got. — ._—" a.+ .nb..:m"H..-rV.-m...n.... ...�eE.n.a I. Groundwater above lank bottom °""'N~A F..P�Mw ft P*+ M. - 1. c J. Product Pressure per t" height_PSI Tank'No. WATER Test Pressure Formula Tight ' YCS J�. Leakage iindicated - • o l y J7 I T h DEPTH E x_-(_X .036 )_ Technician -TojNr,, N a r,El❑:st PRESSUOE Date Tested l 90 •1 il/ '- TOM URAM DIRECTOR CAROL D.KISER 4U NTY O F DIRECTOR OF ADMINISTRATION i 2 1 s 3 RAN G E HEALTH CARE AGENCY CUSTODIAN OF RECORDS 515 N.SYCAMORE AVENUE,SUITE 120 SANTA ANA,CALIFORNIA 92701 FAX(714)835-9312 ' (714)834-3446 ' CERTIFICATION OF NO RECORDS the undersigned, being the Custodian of Records for the County of Orange, Health Care Agency, certify that a thorough search of our files, ' carried out under my direction and control, revealed no Hazardous Waste ' records regarding 31731 Los Rios, San Juan Capistrano, CA. ' It is understood that such records could exist under another spelling, name, or classification, but with the information furnished our office and ' to the best of our knowledge, no such records exist in our files. The Health Care Agency may not be the only source of record. Please check with the Fire Department, the Water Quality control Board and/or the State Department of Health Services. �1 SIGNED: (� - � / ' ' qan-Marie Legacy / Custodian of Records / Itealth Care Agency ' DATE: May 9, 1991 ' JML/gb 0021h